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    Process for manufacturing a tertiary alkyl ether by reactive distillation
    1.
    发明授权
    Process for manufacturing a tertiary alkyl ether by reactive distillation 失效
    通过反应蒸馏制备叔烷基醚的方法

    公开(公告)号：US4847430A

    公开(公告)日：1989-07-11

    申请号：US171339

    申请日：1988-03-21

    申请人： Dang Vu Quang ,  Pierre Amigues ,  Jean-Ferdinand Gaillard ,  Jacques Leonard ,  Jean-Luc Nocca

    发明人： Dang Vu Quang ,  Pierre Amigues ,  Jean-Ferdinand Gaillard ,  Jacques Leonard ,  Jean-Luc Nocca

    IPC分类号： C07B61/00 ,  B01D3/00 ,  B01J8/04 ,  B01J31/10 ,  C07C41/00 ,  C07C41/06 ,  C07C41/42 ,  C07C43/04 ,  C07C67/00

    CPC分类号： C07C41/06 ,  B01D3/009 ,  B01J8/0453 ,  C07C41/42 ,  Y02P20/127 ,  Y10S203/06

    摘要： The invention concerns a process for manufacturing methyl tert-butyl ether (MTBE) by reacting methanol with an isobutene-containing hydrocarbon mixture.This process is characterized by the steps of:introducing the reactants into a reaction-distillation zone containing at least two superposed and non-contiguous fixed beds (2a, 2b) of catalyst of the sulfonated resin type, wherein passage-ways are provided for a vapor phase, at least one distillation tray (4a), at least one liquid redistribution tray (5),maintaining distillation conditions in said zone so as to have a descending liquid phase and an ascending vapor phase,maintaining a continuous liquid phase in the lower part of said beds,discharging a vapor phase containing a high proportion of unconverted hydrocarbons from the top (8) of said zone, andwithdrawing a liquid phase of high MTBE content from the bottom (10) of said zone.

    摘要翻译： 本发明涉及通过使甲醇与含异丁烯的烃混合物反应制备甲基叔丁基醚（MTBE）的方法。 该方法的特征在于以下步骤：将反应物引入含有至少两个磺化树脂类型的催化剂的重叠和不连续的固定床（2a，2b）的反应 - 蒸馏区，其中为 蒸气相，至少一个蒸馏塔板（4a），至少一个液体再分配托盘（5），保持所述区域中的蒸馏条件以具有下降的液相和上升的气相，将下一个液相保持在下部 所述床的一部分，从所述区域的顶部（8）排出含有高比例未转化烃的气相，并从所述区域的底部（10）排出高MTBE含量的液相。

    Apparatus for reactive distillation
    4.
    发明授权
    Apparatus for reactive distillation 失效
    反应蒸馏装置

    公开(公告)号：US5026459A

    公开(公告)日：1991-06-25

    申请号：US356087

    申请日：1989-05-24

    申请人： Dang Vu Quang ,  Pierre Amigues ,  Jean-Ferdinand Gaillard

    发明人： Dang Vu Quang ,  Pierre Amigues ,  Jean-Ferdinand Gaillard

    IPC分类号： B01D3/00 ,  C07C41/06 ,  C07C41/42

    CPC分类号： B01D3/009 ,  C07C41/06 ,  C07C41/42 ,  Y02P20/127 ,  Y10S203/06

    摘要： The invention concerns a process and apparatus for manufacturing methyl tert-butyl ether (MTBE) by reacting methanol with an isobutene-containing hydrocarbon mixture.This process is characterized by the steps of:introducing the reactants into a reaction-distillation zone containing at least two superposed and non-contiguous fixed beds (2a, 2b) of catalyst of the sulfonated resin type, wherein passageways are provided for a vapor phase, at least one distillation tray (4a), at least one liquid redistribution tray (5),maintaining distillation conditions in the zone so as to have a descending liquid phase and an ascending vapor phase,maintaining a continuous liquid phase in the lower part of the beds,discharging a vapor phase containing a high proportion of unconverted hydrocarbons from the top (8) of the zone, andwithdrawing a liquid phase of high MTBE content from the bottom (10) of the zone.

    摘要翻译： 本发明涉及通过使甲醇与含异丁烯的烃混合物反应制备甲基叔丁基醚（MTBE）的方法和装置。 该方法的特征在于以下步骤：将反应物引入反应 - 蒸馏区，该反应蒸馏区包含磺化树脂型催化剂的至少两个重叠和不连续的固定床（2a，2b），其中为气相提供通道 ，至少一个蒸馏塔板（4a），至少一个液体再分布托盘（5），保持该区域中的蒸馏条件以具有下降的液相和上升的气相，在 床，从该区域的顶部（8）排出含有高比例的未转化的烃的气相，并从该区域的底部（10）排出高MTBE含量的液相。

    Process for producing oxygen-containing compounds containing at least one oxygen atom bonded to two distinct carbon atoms which are not bonded together and not including a multiple bond
    5.
    发明授权
    Process for producing oxygen-containing compounds containing at least one oxygen atom bonded to two distinct carbon atoms which are not bonded together and not including a multiple bond 有权
    制备含有至少一个键合在两个不同的碳原子上的氧原子的含氧化合物的方法，它们不结合在一起并且不包括多重键

    公开(公告)号：US06486362B1

    公开(公告)日：2002-11-26

    申请号：US09606018

    申请日：2000-06-29

    申请人： Alain Forestiere ,  Jean-Ferdinand Gaillard ,  Michel Barraque

    发明人： Alain Forestiere ,  Jean-Ferdinand Gaillard ,  Michel Barraque

    IPC分类号： C07C4100

    CPC分类号： C07C41/09 ,  C07C41/42 ,  C07C41/56 ,  C10L1/02 ,  C07C43/04 ,  C07C43/303

    摘要： A process for producing oxygen-containing compounds containing at least one oxygen atom bonded to two distinct carbon atoms which are not bonded together and not comprising a multiple bond comprises a step a) for hydroformylation of a feed comprising at least one olefin containing four to seven carbon atoms to at least one aldehyde, in the presence of a catalyst and a synthesis gas under hydroformylation conditions, a step b) for hydrogenation of this aldehyde to at least one corresponding alcohol, and a step c) for transforming at least one alcohol obtained from step b) in the presence of a catalyst under conditions for producing a mixture containing at least one ether or at least one acetal.

    摘要翻译： 含有至少一个键合在两个不同的碳原子上并且不包含多重键的氧原子的含氧化合物的方法包括步骤a）用于加氢甲酰化含有至少一种含有4-7个烯烃的烯烃 在加氢甲酰化条件下，在催化剂和合成气存在下，将碳原子与至少一种醛反应，步骤b）将该醛氢化成至少一种相应的醇，和步骤c）用于转化至少一种获得的醇 步骤b）在催化剂存在下在产生含有至少一种醚或至少一种缩醛的混合物的条件下进行。