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1.发明申请公开(公告)号：US20110207909A1
公开(公告)日：2011-08-25
申请号：US13033252
申请日：2011-02-23
申请人： Ji Su Jeong , Sujith Sudevan , Myung Ahn Ok , Sung Jae Na , Yong Gyu Han , Kwang Jin Chung , Bun Yeoul Lee , Kodiyan Varghese Jobi
发明人： Ji Su Jeong , Sujith Sudevan , Myung Ahn Ok , Sung Jae Na , Yong Gyu Han , Kwang Jin Chung , Bun Yeoul Lee , Kodiyan Varghese Jobi
IPC分类号： C08G65/26 , C07F15/06 , C07C221/00
CPC分类号： C07C251/24 , C07C2601/14 , C07F15/065 , C08G65/2603 , C08G65/266
摘要： This invention relates to a Salen type ligand including three or more quaternary ammonium salts of nitrate anions, to a trivalent metal complex compound prepared from this ligand and a method of preparing the same, to a method of preparing polycarbonate by copolymerizing an epoxide compound and carbon dioxide using the complex compound as a catalyst, and to a method of separating and collecting the catalyst from the copolymer after copolymerization. This catalyst used to copolymerize an epoxide compound and carbon dioxide can be more simply prepared, and has lower catalyst preparation and recovery costs, and higher activity, compared to conventional catalysts.
摘要翻译： 本发明涉及包含三种或更多种硝酸根阴离子的季铵盐的Salen型配体，由该配体制备的三价金属络合物及其制备方法，涉及一种通过使环氧化合物与碳 使用配位化合物作为催化剂的二氧化碳，以及共聚后从共聚物中分离和收集催化剂的方法。 与常规催化剂相比，用于共聚环氧化合物和二氧化碳的催化剂可以更简单地制备，并且具有较低的催化剂制备和回收成本，以及更高的活性。
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2.发明授权公开(公告)号：US08598309B2
公开(公告)日：2013-12-03
申请号：US13033252
申请日：2011-02-23
申请人： Ji Su Jeong , Sujith Sudevan , Myung Ahn Ok , Sung Jae Na , Yong Gyu Han , Kwang Jin Chung , Bun Yeoul Lee , Kodiyan Varghese Jobi
发明人： Ji Su Jeong , Sujith Sudevan , Myung Ahn Ok , Sung Jae Na , Yong Gyu Han , Kwang Jin Chung , Bun Yeoul Lee , Kodiyan Varghese Jobi
CPC分类号： C07C251/24 , C07C2601/14 , C07F15/065 , C08G65/2603 , C08G65/266
摘要： This invention relates to a Salen type ligand including three or more quaternary ammonium salts of nitrate anions, to a trivalent metal complex compound prepared from this ligand and a method of preparing the same, to a method of preparing polycarbonate by copolymerizing an epoxide compound and carbon dioxide using the complex compound as a catalyst, and to a method of separating and collecting the catalyst from the copolymer after copolymerization. This catalyst used to copolymerize an epoxide compound and carbon dioxide can be more simply prepared, and has lower catalyst preparation and recovery costs, and higher activity, compared to conventional catalysts.
摘要翻译： 本发明涉及包含三种或更多种硝酸根阴离子的季铵盐的Salen型配体，由该配体制备的三价金属络合物及其制备方法，涉及一种通过使环氧化合物与碳 使用配位化合物作为催化剂的二氧化碳，以及共聚后从共聚物中分离和收集催化剂的方法。 与常规催化剂相比，用于共聚环氧化合物和二氧化碳的催化剂可以更简单地制备，并且具有较低的催化剂制备和回收成本，以及更高的活性。
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3.发明授权Preparation of poly(alkylene carbonate) containing cross-linked high molecular weight chains 有权含有交联的高分子量链的聚（碳酸亚烷基酯）的制备公开(公告)号：US08785592B2
公开(公告)日：2014-07-22
申请号：US13226985
申请日：2011-09-07
申请人： Ji Su Jeong , Sung Jae Na , Sujith Sudevan , Myung Ahn Ok , Yong Gyu Han , Kwang Jin Chung , Bun Yeoul Lee , Anish Cyriac
发明人： Ji Su Jeong , Sung Jae Na , Sujith Sudevan , Myung Ahn Ok , Yong Gyu Han , Kwang Jin Chung , Bun Yeoul Lee , Anish Cyriac
CPC分类号： C08G64/34 , C08G64/0216
摘要： Provided is preparation of poly(alkylene carbonate) through alternating copolymerization of carbon dioxide and epoxide. According to the disclosure, by introducing a diepoxide compound to alternating copolymerization of carbon dioxide and epoxide compound using a metal(III) prepared with salen-type ligands containing quaternary ammonium salt as a catalyst, some of the polymer chains may be cross-linked to thus increase an average molecular weight of the copolymer and extend a distribution of molecular weight. A resin prepared according to this method may have high mechanical strength and rheological advantages.
摘要翻译： 提供通过二氧化碳和环氧化物的交替共聚制备聚（碳酸亚烷基酯）。 根据公开内容，通过使用由含有季铵盐的salen型配体制备的金属（III）作为催化剂，通过引入二环氧化合物以使二氧化碳和环氧化合物的交替共聚，一些聚合物链可以与 从而增加共聚物的平均分子量并延长分子量的分布。 根据该方法制备的树脂可具有高的机械强度和流变学优点。
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4.发明申请PREPARATION OF POLY(ALKYLENE CARBONATE) CONTAINING CROSS-LINKED HIGH MOLECULAR WEIGHT CHAINS 有权含有交联高分子量链的聚（亚烷基碳酸酯）的制备公开(公告)号：US20120065360A1
公开(公告)日：2012-03-15
申请号：US13226985
申请日：2011-09-07
申请人： Ji Su Jeong , Sung Jae Na , Sujith Sudevan , Myung Ahn Ok , Yong Gyu Han , Kwang Jin Chung , Bun Yeoul Lee , Anish Cyriac
发明人： Ji Su Jeong , Sung Jae Na , Sujith Sudevan , Myung Ahn Ok , Yong Gyu Han , Kwang Jin Chung , Bun Yeoul Lee , Anish Cyriac
IPC分类号： C08G64/34
CPC分类号： C08G64/34 , C08G64/0216
摘要： Provided is preparation of poly(alkylene carbonate) through alternating copolymerization of carbon dioxide and epoxide. According to the disclosure, by introducing a diepoxide compound to alternating copolymerization of carbon dioxide and epoxide compound using a metal(III) prepared with salen-type ligands containing quaternary ammonium salt as a catalyst, some of the polymer chains may be cross-linked to thus increase an average molecular weight of the copolymer and extend a distribution of molecular weight. A resin prepared according to this method may have high mechanical strength and rheological advantages.
摘要翻译： 提供通过二氧化碳和环氧化物的交替共聚制备聚（碳酸亚烷基酯）。 根据公开内容，通过使用由含有季铵盐的salen型配体制备的金属（III）作为催化剂，通过引入二环氧化合物以使二氧化碳和环氧化合物的交替共聚，一些聚合物链可以与 从而增加共聚物的平均分子量并延长分子量的分布。 根据该方法制备的树脂可具有高的机械强度和流变学优点。
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