公开(公告)号：US5035781A

公开(公告)日：1991-07-30

申请号：US528664

申请日：1990-05-24

申请人： Jurgen Schmidt ,  Thomas Furche ,  Roland Erdmann ,  Marion Reichert ,  Ullrich Bayer ,  Peter Kurze ,  Thomas Schwarz ,  Joachim Schreckenbach ,  Hans-Jurgen Kletke ,  Andreas Hoffmann ,  Martin Heppner ,  Anja Hasse ,  Dorith Schmidt ,  Annette Klaus

发明人： Jurgen Schmidt ,  Thomas Furche ,  Roland Erdmann ,  Marion Reichert ,  Ullrich Bayer ,  Peter Kurze ,  Thomas Schwarz ,  Joachim Schreckenbach ,  Hans-Jurgen Kletke ,  Andreas Hoffmann ,  Martin Heppner ,  Anja Hasse ,  Dorith Schmidt ,  Annette Klaus

IPC分类号： C25D11/02 ,  C25D11/26

CPC分类号： C25D11/26 ,  C25D11/026 ,  Y10T428/12806 ,  Y10T428/12812

摘要： The invention relates to a cyanide-free electrolyte being harmless to the environment and to health which makes feasible the production of black surface layers on light metals or on alloys of the latter, preferably titanium, remaining deeply-black and adhesive even after extreme changes in the ambient temperature and having nearly equal values of the optical absorptivity of radiation and of the thermal emission capability (the .alpha./.epsilon.-ratio is about 0.95) by means of the anodic oxidation by spark discharge (ANOF-method). These layers are absolutely X-amorphous and show, hence, an ideal optically isotropic behavior regarding the reflection of radiation. Due to their minimum evolution of gases they offer a high thermovacuum stability. The electrolyte consists of an ammoniacal solution of K.sub.2 H.sub.2 PO.sub.4 potssium dihydrogenphosphate and K.sub.2 CRO.sub.4 potassium chromate. The homogeneity of the optically black layers is ensured by not using fluoride ions and employing acetate ions. Such layers comprise titanium, chromium and copper following ratios of CR:Ti=1:(1.9 to 2.2) and CR:Cu=1:(0.8 to 1.3).

摘要翻译： 本发明涉及一种对无环境和健康无害的电解质，这使得在轻金属或后者的合金（优选钛）上生产黑色表面层是可行的，即使在极端变化之后仍然保持深黑色和粘合 通过火花放电的阳极氧化（ANOF方法），具有几乎相同的辐射光吸收率和热发射能力（α/ε-比率约为0.95）的值。 这些层是绝对X非晶体的，因此显示关于辐射反射的理想光学各向同性行为。 由于它们气体的最小演变，它们提供了高的热真空稳定性。 电解质由K2H2PO4磷酸二氢钾和K2CRO4铬酸钾的氨溶液组成。 通过不使用氟离子并使用乙酸根离子来确保光学黑层的均匀性。 CR：Ti = 1：（1.9〜2.2）和CR:Cu = 1：（0.8〜1.3）的比例，这些层包含钛，铬和铜。

公开(公告)号：US5075178A

公开(公告)日：1991-12-24

申请号：US638288

申请日：1990-01-07

申请人： Juergen Schmidt ,  Thomas Furche ,  Roland Erdmann ,  Marion Reichert ,  Bayer Ullrich ,  Peter Kurze ,  Thomas Schwarz ,  Joachim Schreckenbach ,  Hans-Juergen Kletke ,  Andreas Hofmann ,  Martin Heppner ,  Anja Hasse ,  Dorith Schmidt ,  Annette Klaus

发明人： Juergen Schmidt ,  Thomas Furche ,  Roland Erdmann ,  Marion Reichert ,  Bayer Ullrich ,  Peter Kurze ,  Thomas Schwarz ,  Joachim Schreckenbach ,  Hans-Juergen Kletke ,  Andreas Hofmann ,  Martin Heppner ,  Anja Hasse ,  Dorith Schmidt ,  Annette Klaus

IPC分类号： C25D11/02 ,  C25D11/26

CPC分类号： C25D11/26 ,  C25D11/026 ,  Y10T428/12806 ,  Y10T428/12812

摘要： The invention relates to a cyanide-free electrolyte being harmless to the environment and to health which makes feasible the production of black surface layers on light metals or on alloys of the latter, preferably titanium, remaining deeply-black and adhesive even after extreme changes in the ambient temperature and having nearly equal values of the optical absorptivity of radiation and of the thermal emission capability (the .alpha./.epsilon.-ratio is about 0.95) by means of the anodic oxidation by spark discharge (ANDF-method). These layers are absolutely X-amorphous and show, hence, an ideal optically isotropic behavior regarding the reflection of radiation. Due to their minmum evolution of gases they offer a high thermovacuum stability. The electrolyte consists of an ammoniacal solution of K.sub.2 H.sub.2 PO.sub.4 potassium dihydrogenphosphate and K.sub.2 CrO.sub.4 potassium chromate. The homogeneity of the optically black layers is ensured by not using fluoride ions and employing acetate ions. Such layers comprise titanium, chromium and copper in ratios of Cr:Ti=1: (1.9 to 2.2) and Cr:Cu=1:(0.8 to 1.3).

公开(公告)号：US5225069A

公开(公告)日：1993-07-06

申请号：US884691

申请日：1992-05-18

申请人： Kerstin Haupt ,  Jurgen Schmidt ,  Ullrich Bayer ,  Thomas Furche

发明人： Kerstin Haupt ,  Jurgen Schmidt ,  Ullrich Bayer ,  Thomas Furche

IPC分类号： C25D11/04 ,  C25D11/16

CPC分类号： C25D11/04 ,  C25D11/024 ,  C25D11/026 ,  C25D11/16

摘要： A process for the production of white and black oxide ceramic surface films on silicon-containing light metal cast alloys by plasma-chemical anodic oxidation. An aluminum cast alloy is pickled with nitric acid and hydrofluoric acid and coated by plasma-chemical anodic oxidation in an aqueous electrolyte. Accordingly, a coating variant is provided particularly for construction parts of silicon-containing light metal cast alloys having complicated shapes which enables the production of uniformly thin oxide ceramic surface films in contrast to conventional coating variants.

摘要翻译： 通过等离子体化学阳极氧化在含硅轻金属铸造合金上生产白色和黑色氧化物陶瓷表面膜的方法。 铝合金铸造用硝酸和氢氟酸浸渍，并通过等离子体化学阳极氧化在含水电解液中涂覆。 因此，与传统的涂层变型形成对比，特别提供了具有复杂形状的含硅轻金属铸造合金的构造部件的涂层变型，其能够生产均匀的氧化物陶瓷表面膜。

公开(公告)号：US5094727A

公开(公告)日：1992-03-10

申请号：US691629

申请日：1991-04-25

申请人： Thomas Schwarz ,  Ullrich Bayer ,  Kerstin Haupt ,  Juergen Schmidt ,  Thomas Furche

发明人： Thomas Schwarz ,  Ullrich Bayer ,  Kerstin Haupt ,  Juergen Schmidt ,  Thomas Furche

IPC分类号： C25D11/04 ,  C25D11/14

CPC分类号： C25D11/026 ,  C25D11/04 ,  C25D11/14

摘要： By means of an electrolyte free of ammonia, cyanide, and fluoride, hence low in harmful substances and inoffensive to the environment, optically black coatings having a thickness of less than 10 microns and substantially equal optical absorption and thermal emission capability can be produced on light metals or alloys thereof by spark discharge anodizing. In comparison with prior art conversion coatings obtained by spark discharge anodizing, the coatings produced with this electrolyte have a substantially lower roughness of this electrolyte in spark discharge anodizing provides an alternative mode of coating particularly for structural components or subassemblies of complicated shapes having greater requirements for accuracy to gauge.

摘要翻译： 通过不含氨，氰化物和氟化物的电解质，因此有害物质低，对环境无害，可以在光照下产生厚度小于10微米，光学吸收和热发射能力基本相等的光学黑色涂层 金属或其合金通过火花放电阳极氧化。 与通过火花放电阳极氧化获得的现有技术的转化涂层相比，用电解质生产的涂层在火花放电中具有基本上较低的这种电解质的粗糙度阳极氧化提供了替代的涂层模式，特别是对于具有更大要求的复杂形状的结构部件或子组件 测量精度。

公开(公告)号：US20060172454A1

公开(公告)日：2006-08-03

申请号：US11334221

申请日：2006-01-18

申请人： Hans-Henning Reis ,  Thomas Furche ,  Klaus Andersson

发明人： Hans-Henning Reis ,  Thomas Furche ,  Klaus Andersson

IPC分类号： H01L21/00 ,  C23C14/32

CPC分类号： C22C27/04 ,  B22F2003/248 ,  B22F2998/10 ,  C23C4/08 ,  C23C14/3414 ,  B22F3/02 ,  B22F3/20 ,  B22F3/24 ,  B22F3/17

摘要： The invention relates to a molybdenum alloy that includes: 94 to 99 weight % of molybdenum; 0.5 to 6 weight % of niobium; and 0.01 to 1 weight % of zirconium. The invention also relates to metal substrates that include such a molybdenum alloy, and anode disks for rotating anode x-ray tubes that include the substrate. Also described are methods of preparing tubular-shaped and disk-shaped molybdenum alloy based sputtering targets.

摘要翻译： 本发明涉及一种钼合金，其包括：94〜99重量％的钼; 0.5〜6重量％的铌; 和0.01〜1重量％的锆。 本发明还涉及包括这种钼合金的金属基底和用于旋转包括基底的阳极x射线管的阳极盘。 还描述了制备管状和盘形钼合金的溅射靶的方法。

公开(公告)号：US20100028706A1

公开(公告)日：2010-02-04

申请号：US12535278

申请日：2009-08-04

申请人： Jan Hornschu ,  Andre Kabis ,  Thomas Furche ,  Henning Uhlerihut

发明人： Jan Hornschu ,  Andre Kabis ,  Thomas Furche ,  Henning Uhlerihut

IPC分类号： B32B15/01 ,  H05H1/24 ,  H05H1/48

CPC分类号： C22F1/00 ,  C23C4/02 ,  C23C4/10 ,  C23C4/11 ,  C23C4/18 ,  C23C24/04 ,  C23C28/321 ,  C23C28/322 ,  C23C28/34 ,  C23C28/345 ,  C23C28/3455 ,  C23C30/00 ,  Y10T428/12229

摘要： The present invention relates to blanks for workpieces composed of a base body, which comprises at least one refractory metal and an oxidation protection layer composed of at least one metal layer, and also processes for producing them.

摘要翻译： 本发明涉及由基体构成的工件坯料，该基体包括至少一种难熔金属和由至少一个金属层构成的氧化保护层，并且还涉及制造它们的工艺。