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    Process for preparing linear α-olefins
    1.
    发明授权
    Process for preparing linear α-olefins 有权

    公开(公告)号：US09896391B2

    公开(公告)日：2018-02-20

    申请号：US13576414

    申请日：2011-01-13

    申请人： Karl Heinz Hofmann ,  Hans Jorg Zander ,  Anton Wellenhofer ,  Wolfgang Muller ,  Anina Wohl

    发明人： Karl Heinz Hofmann ,  Hans Jorg Zander ,  Anton Wellenhofer ,  Wolfgang Muller ,  Anina Wohl

    IPC分类号： C07C2/08

    CPC分类号： C07C2/08 ,  C07C11/02

    摘要： The invention relates to a process for preparing linear α-olefins, wherein ethylene 1a is conducted into the oligomerization reactor 2 in the liquid phase. The oligomerization reactor 2 has a mechanical stirrer 2a in order to ensure optimal mixing of the liquid ethylene and of the catalyst in the liquid phase. From the top of the oligomerization reactor 2, vaporized ethylene is drawn off together with light α-olefins and a small proportion of the organic solvent. The gas mixture drawn off from the top of the reactor 2 is condensed together with gaseous fresh ethylene 7 by means of heat exchanger 3 and separator 4. The liquid phase drawn off from the separator 4 is conducted by means of circulation pump 5a as liquid ethylene input 1a back into the oligomerization reactor 2. The liquid products of the oligomerization reaction are drawn off 8 laterally from the base of the reactor 2.

    PROCESS FOR PREPARING LINEAR alpha-OLEFINS
    2.
    发明申请
    PROCESS FOR PREPARING LINEAR alpha-OLEFINS 有权
    制备线性α-烯烃的方法

    公开(公告)号：US20120330078A1

    公开(公告)日：2012-12-27

    申请号：US13576414

    申请日：2011-01-13

    申请人： Karl Heinz Hofmann ,  Hans Jorg Zander ,  Anton Wellenhofer ,  Wolfgang Muller ,  Anina Wohl

    发明人： Karl Heinz Hofmann ,  Hans Jorg Zander ,  Anton Wellenhofer ,  Wolfgang Muller ,  Anina Wohl

    IPC分类号： C07C2/08

    CPC分类号： C07C2/08 ,  C07C11/02

    摘要： The invention relates to a process for preparing linear α-olefins, wherein ethylene 1a is conducted into the oligomerization reactor 2 in the liquid phase. The oligomerization reactor 2 has a mechanical stirrer 2a in order to ensure optimal mixing of the liquid ethylene and of the catalyst in the liquid phase. From the top of the oligomerization reactor 2, vaporized ethylene is drawn off together with light α-olefins and a small proportion of the organic solvent. The gas mixture drawn off from the top of the reactor 2 is condensed together with gaseous fresh ethylene 7 by means of heat exchanger 3 and separator 4. The liquid phase drawn off from the separator 4 is conducted by means of circulation pump 5a as liquid ethylene input 1a back into the oligomerization reactor 2. The liquid products of the oligomerization reaction are drawn off 8 laterally from the base of the reactor 2.

    摘要翻译： 本发明涉及一种线性α-烯烃的制备方法，其中乙烯1a以液相方式进入低聚反应器2。 低聚反应器2具有机械搅拌器2a，以确保在液相中液体乙烯和催化剂的最佳混合。 从低聚反应器2的顶部开始蒸发的乙烯与轻质α-烯烃和少部分有机溶剂一起被排出。 从反应器2的顶部排出的气体混合物通过热交换器3和分离器4与气态新鲜乙烯7一起冷凝。从分离器4抽出的液相通过循环泵5a作为液体乙烯 输入1a回到低聚反应器2中。低聚反应的液体产物从反应器2的底部横向排出8。