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    PREPARATION OF HIGH-QUALITY OXO PROCESS ALCOHOLS FROM INCONSTANT RAW MATERIAL SOURCES
    4.
    发明申请
    PREPARATION OF HIGH-QUALITY OXO PROCESS ALCOHOLS FROM INCONSTANT RAW MATERIAL SOURCES 有权
    从不合理原料来源制备高品质氧气工艺酒精

    公开(公告)号：US20150336861A1

    公开(公告)日：2015-11-26

    申请号：US14717183

    申请日：2015-05-20

    Applicant: Frank GEILEN ,  Katrin Marie DYBALLA ,  Dieter HESS ,  Stephan PEITZ ,  Robert FRANKE ,  Dirk FRIDAG ,  Dietrich MASCHMEYER ,  Helene REEKER ,  Guido STOCHNIOL

    Inventor： Frank GEILEN ,  Katrin Marie DYBALLA ,  Dieter HESS ,  Stephan PEITZ ,  Robert FRANKE ,  Dirk FRIDAG ,  Dietrich MASCHMEYER ,  Helene REEKER ,  Guido STOCHNIOL

    IPC: C07C29/14 ,  C07C69/80 ,  C08K5/12 ,  C07C67/08

    CPC classification number: C07C29/14 ,  B01J31/185 ,  B01J31/1885 ,  C07C2/24 ,  C07C29/141 ,  C07C45/50 ,  C07C67/08 ,  C07C69/80 ,  C07C2523/755 ,  C08K5/12 ,  C07C11/02 ,  C07C47/02 ,  C07C31/125

    Abstract: The preparation of high-quality oxo process alcohols from inconstant raw material sources is the technically demanding problem which is addressed by a process for continuously preparing an alcohol mixture, in which an input mixture which contains an olefin and has a composition that changes over time is subjected to an oligomerization to obtain an oligomerizate and at least a portion of the olefin oligomers present in the oligomerizate are hydroformylated with carbon monoxide and hydrogen in a hydroformylation in the presence of a homogeneous catalyst system to give aldehydes, at least some of which are converted to the alcohol mixture by subsequent hydrogenation. The process provides a constant plasticizer quality to be produced over a long production period and, optionally, a higher throughput with the same product quality. This is achieved a) by control of the temperature and/or the conversion of the oligomerization as a function of the current composition of the oligomerizate; and b) by control of the composition of the catalyst system and/or of the pressure of the hydroformylation as a function of the current composition of the aldehydes.

    Abstract translation: 从不定原料来源制备高品质氧化工艺醇是技术上要求苛刻的问题，其通过连续制备醇混合物的方法来解决，其中含有烯烃并且具有随时间变化的组成的输入混合物是 进行低聚以获得低聚物，并且在均相催化剂体系的存在下，在加氢甲酰化中，将低聚物中存在的烯烃低聚物的至少一部分与一氧化碳和氢气加氢甲酰化，得到醛，其中至少一些转化为 通过随后的氢化到醇混合物。 该方法提供了在长的生产周期内生产的恒定的增塑剂质量，并且可选地具有相同产品质量的较高产量。 这是通过控制低聚物的温度和/或转化作为当前低聚物组成的函数来实现的; 和b）通过控制催化剂体系的组成和/或加氢甲酰基化的压力作为醛的当前组成的函数。

    COMBINED PREPARATION OF AT LEAST BUTENE AND OCTENE FROM ETHENE
    5.
    发明申请
    COMBINED PREPARATION OF AT LEAST BUTENE AND OCTENE FROM ETHENE 审中-公开
    从乙烯组合制备最小的泡沫和硬度

    公开(公告)号：US20160207849A1

    公开(公告)日：2016-07-21

    申请号：US15000837

    申请日：2016-01-19

    Applicant: Guido STOCHNIOL ,  Stephan PEITZ ,  Dietrich MASCHMEYER ,  Helene REEKER ,  Joerg SCHALLENBERG

    Inventor： Guido STOCHNIOL ,  Stephan PEITZ ,  Dietrich MASCHMEYER ,  Helene REEKER ,  Joerg SCHALLENBERG

    IPC: C07C2/24

    CPC classification number: C07C2/24 ,  C07C2/10 ,  C07C7/04 ,  C07C2521/12 ,  C07C2523/755 ,  C07C11/08 ,  C07C11/107 ,  C07C11/02

    Abstract: A process for the combined preparation of at least butene and octene from ethane, proceeds by a) providing an inert solvent having a boiling point or boiling range below the boiling point of butene; b) providing a first feed mixture comprising at least the inert solvent and ethene dissolved therein; c) converting the first feed mixture in a first synthesis; d) in the first synthesis, oligomerizing at least a portion of the ethene present in the first feed mixture in the presence of a first heterogeneous catalyst and in the presence of the inert solvent to obtain a first reaction mixture comprising at least the inert solvent, butene, hexene and octene; e) working-up of the first reaction mixture and/or a substance stream based thereon into a low boiler fraction comprising the inert solvent, at least one C4-fraction comprising butenes, a C6-fraction comprising hexenes, a C8-fraction comprising octenes and into a C8+-fraction comprising hydrocarbons having more than eight carbon atoms; f) using at least a portion of the low boiler fraction for providing the first feed mixture; g) providing a second feed mixture comprising at least hexene and ethene dissolved in the hexene using at least a portion of the C6-fraction; h) converting the second feed mixture in a second synthesis, wherein the second synthesis is spatially separated from the first synthesis; i) in the second synthesis, reacting at least a portion of the ethene present in the second feed mixture with at least a portion of the hexene present in the second feed mixture in the presence of a second heterogeneous catalyst to obtain a second reaction mixture comprising at least octene; and k) joint working-up of the second reaction mixture with the first reaction mixture or with the substance stream based thereon.

    Abstract translation: 从乙烷中至少组合制备丁烯和辛烯的方法是：a）提供沸点或沸点低于丁烯沸点的惰性溶剂; b）提供至少包含溶解在其中的惰性溶剂和乙烯的第一进料混合物; c）在第一合成中转化第一进料混合物; d）在第一种合成中，在存在第一种非均相催化剂的情况下和在惰性溶剂存在下使存在于第一进料混合物中的至少一部分乙烯低聚，得到包含至少惰性溶剂的第一反应混合物， 丁烯，己烯和辛烯; e）将第一反应混合物和/或基于其的物质流加工到包含惰性溶剂的低沸点馏分中，至少一种包含丁烯的C 4馏分，包含己烯的C 6馏分，包含辛烯的C 8馏分 并进入包含具有多于8个碳原子的烃的C8 +分馏; f）使用低沸点馏分的至少一部分来提供第一进料混合物; g）使用C 6馏分的至少一部分提供包含至少己烯和溶解在己烯中的乙烯的第二进料混合物; h）在第二合成中转化所述第二进料混合物，其中所述第二合成在空间上与所述第一合成分离; i）在第二合成中，使第二进料混合物中存在的乙烯的至少一部分与存在于第二进料混合物中的至少一部分己烯存在于第二种非均相催化剂中，以获得第二反应混合物， 至少辛烯; 和k）第二反应混合物与第一反应混合物或其上的物质流的联合处理。

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