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公开(公告)号：US5080694A
公开(公告)日：1992-01-14
申请号：US445711
申请日：1989-11-17
申请人： Karl Knoblauch , Erwin Pilarczyk , Klaus Glessler , Hans Bukowski , Joseph S. D'Amico , Herbert Reinhold
发明人： Karl Knoblauch , Erwin Pilarczyk , Klaus Glessler , Hans Bukowski , Joseph S. D'Amico , Herbert Reinhold
IPC分类号： B01D53/04 , B01D53/047 , C01B23/00
CPC分类号： B01D53/0476 , C01B23/00 , B01D2253/102 , B01D2253/116 , B01D2253/25 , B01D2253/308 , B01D2256/18 , B01D2257/102 , B01D2257/7025 , B01D2259/40001 , B01D2259/4003 , B01D2259/40037 , B01D2259/40041 , B01D2259/40066 , B01D2259/40071 , B01D2259/404 , Y02C20/20 , Y02P20/156
摘要： A method is provided for the extraction of hellium of high purity, and high yield, with intermediate enrichment in refrigerating plants, from gases containing very low helium concentrations, by an alternating pressure adsorption process. the helium containing gas is fed cyclically in each of three adsorption stages into four adsorbers connected in parallel. First, higher hydrocarbons and other impurities are trapped in adsorbers (J, K, L, M) filled with activated charcoal in a preliminary filtering stage. Other gaseous components, for example nitrogen and/or methane are trapped in adsorbers (A, B, C, D and E, F, G, H) filled with carbon molecular sieves, in two subsequent adsorption stages. The helium is first enriched in stage (I) and then extracted in stage (II) as refined helium with a helium content of 99.9%. The gas used is preferably natural gas with a 2 to 10% helium content. The refined helium so produced can be used, for example as a blanket gas, a breathing gas for divers, a balloon gas and as a carrier gas in chromatography.
摘要翻译： PCT No.PCT / EP88 / 04440 Sec。 371日期：一九八九年十一月十七日 102（e）日期1989年11月17日PCT提交1988年5月19日PCT公布。 出版物WO88 / 09305 日期为1988年12月1日。提供了一种通过交替压力吸附法从含有非常低的氦浓度的气体中提取高纯度和高产率的富含中间富集的冷藏设备的方法。 将含氦气体在三个吸附阶段中的每一个周期循环进入并联连接的四个吸附器。 首先，在预过滤阶段，高级烃和其他杂质被捕获在填充有活性炭的吸附器（J，K，L，M）中。 在两个后续吸附阶段中，其他气体组分，例如氮和/或甲烷被捕获在填充有碳分子筛的吸附器（A，B，C，D和E，F，G，H）中。 氦首先在阶段（I）中富集，然后在阶段（II）中作为氦含量为99.9％的精制氦萃取。 所使用的气体优选为具有2至10％氦含量的天然气。 如此生产的精制氦气可以用作例如毯式气体，用于潜水员的呼吸气体，气球气体和作为色谱法中的载气。
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公开(公告)号：US5089048A
公开(公告)日：1992-02-18
申请号：US445716
申请日：1989-11-17
申请人： Karl Knoblauch , Erwin Pilarczyk , Klaus Giessler , Hans Bukowski , Joseph S. D'Amico , Herbert Reinhold
发明人： Karl Knoblauch , Erwin Pilarczyk , Klaus Giessler , Hans Bukowski , Joseph S. D'Amico , Herbert Reinhold
IPC分类号： B01D53/04 , B01D53/047 , C01B23/00
CPC分类号： B01D53/0476 , C01B23/00 , B01D2253/102 , B01D2253/116 , B01D2253/25 , B01D2253/308 , B01D2256/18 , B01D2257/102 , B01D2257/7025 , B01D2259/4003 , B01D2259/40041 , B01D2259/40071 , B01D2259/404 , Y02C20/20 , Y02P20/124 , Y02P20/156
摘要： A method is provided for extracting helium from a relatively helium poor gas mixture through a pressure swing adsorption process which adhieves an enriched product gas containing over 50% helium. The gas mixture to be enriched is fed cyclically to four adsorber vessels ranged in parallel which successively pass through a pressure build-up, an adsorptive and a pressure relief phase, with pressure build-up and relief being in part brought about by pressure compensation with any one of the other adsorbers. The pressure-build up and relief phases include a series of three and four, respectively, steps involving alternating pressure levels. As a preliminary treatment, the process may include an initial step wherein the unenriched gas mixture is first fed through a series of pre-filters filled with activated carbon for removing higher hydrocarbons.
摘要翻译： PCT No.PCT / EP88 / 00441 Sec。 371日期：一九八九年十一月十七日 102（e）日期1989年11月17日PCT提交1988年5月19日PCT公布。 出版物WO89 / 10810 日期为1989年11月16日。提供了一种通过变压吸附法从相对氦气气体混合物中提取氦气的方法，该方法对含有超过50％氦的富集产物气进行了补充。 要富集的气体混合物循环进料到四个平行流动的吸附剂容器，它们依次通过压力增加，吸附和减压阶段，压力积聚和释放部分是由压力补偿带来的 任何其他吸附剂。 压力增加和缓解阶段包括一系列涉及交替压力水平的三个和四个步骤。 作为初步处理，该方法可以包括初始步骤，其中未富集的气体混合物首先通过充满活性炭的一系列预过滤器进料，以除去高级烃。
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公开(公告)号：US5042811A
公开(公告)日：1991-08-27
申请号：US490369
申请日：1990-03-08
申请人： Joseph S. D'Amico
发明人： Joseph S. D'Amico
CPC分类号： A63B69/3632 , A63B53/14
摘要： A device for weakening the right hand grip on a golf club in order to allow better extension in a swing for the left arm and club shaft. A body has three identations, two to be gripped by the thumb and middle finger of the right hand and a third indentation disposed between the other two for accepting the width of the golf club shaft. The body is gripped by the thumb and middle finger of the right hand and the third indentation is placed against the club shaft. The resulting grip maintains the positioning of a standard grip while at the same time weakening the right hand strength.
摘要翻译： 一种用于削弱高尔夫球杆上的右手把手的装置，以便在左臂和杆杆的摆动中更好地延伸。 身体具有三个标识，两个由右手的拇指和中指夹住，另一个位于另一个之间，用于接受高尔夫球杆杆的宽度。 身体被右手的拇指和中指夹住，第三个凹痕被放置在球杆杆上。 所产生的握柄保持标准把手的定位，同时削弱右手强度。
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公开(公告)号：US5707425A
公开(公告)日：1998-01-13
申请号：US655872
申请日：1996-05-21
IPC分类号： B01D53/047 , B01D53/22 , C01B23/00
CPC分类号： B01D53/04 , B01D53/047 , B01D53/229 , C01B23/0052 , C01B23/0094 , B01D2253/102 , B01D2253/104 , B01D2253/106 , B01D2253/304 , B01D2256/18 , B01D2257/11 , B01D2259/404 , B01D2259/406 , B01D2259/41 , C01B2210/001 , C01B2210/0014 , C01B2210/0031 , C01B2210/0068 , C01B2210/007 , F25J2250/02
摘要： The present process is directed to the efficient recovery of helium gas from gas streams which contain about 25 percent by volume or more helium. The process comprises two stages of pressure swing adsorption, each stage being comprised of a plurality of interconnected adsorbent beds. In the first stage of pressure swing adsorption which is comprised of about five phases, the helium content of the gas stream is increased to 95 percent by volume or more. A secondary product gas stream from the first stage of pressure swing adsorption is fed to the second stage of pressure swing adsorption. The second stage of pressure swing adsorption increases the helium content of this primarily non-helium product gas to more than about 50 percent by volume. This gas now with a helium content of more than about 50 percent by volume is fed along with the gas stream as the input gas to the first stage of pressure swing adsorption.
摘要翻译： 本方法涉及从含有约25体积％或更多氦气的气流中有效地回收氦气。 该方法包括两个阶段的变压吸附，每个阶段由多个相互连接的吸附床组成。 在由五相组成的变压吸附的第一阶段中，气流的氦含量增加至95体积％以上。 来自变压吸附的第一阶段的二次产物气流被供给到变压吸附的第二阶段。 变压吸附的第二阶段使这种主要的非氦产物气体的氦含量增加到超过约50体积％。 现在具有大于约50体积％的氦含量的气体与作为输入气体的气流一起供入到变压吸附的第一阶段。
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公开(公告)号：US5632803A
公开(公告)日：1997-05-27
申请号：US517469
申请日：1995-08-21
IPC分类号： B01D53/047 , B01D53/22 , C01B23/00 , B01D53/47
CPC分类号： B01D53/04 , B01D53/047 , B01D53/229 , C01B23/0052 , C01B23/0094 , B01D2253/102 , B01D2253/104 , B01D2253/106 , B01D2253/304 , B01D2256/18 , B01D2257/11 , B01D2259/404 , B01D2259/406 , B01D2259/41 , C01B2210/001 , C01B2210/0014 , C01B2210/0031 , C01B2210/0068 , C01B2210/007
摘要： The disclosed hybrid membrane and pressure swing adsorption process can recover helium from source streams of about 0.5 to 5 percent by volume helium and concentrate the helium to a concentration of greater than about 98 percent by volume. The process comprises a membrane separation followed by two stages of pressure swing adsorption which are used in series. The source gas will primarily contain hydrocarbons but will contain some nitrogen. The membrane unit will contain a semipermeable membrane which is permeably selective for helium and will to the extent feasible reject hydrocarbons. The permeate gas will be increased in helium content by 2 to 10 times. Part of the residue gas is used in the regeneration of the adsorbent beds in the first stage of pressure swing adsorption. Each stage of pressure swing adsorption will contain a plurality of adsorbent beds, and will be cycled through multiple phases. In the first stage the adsorbent beds will sequentially undergo the phases of adsorption, recycle, depressurization, evacuation, helium pressurization and recycle feed pressurization. The product gas from the first stage is flowed to the second stage and in the second stage sequentially will undergo the phases of adsorption, depressurization, evacuation, purge, and helium pressurization. The offgas from the evacuation and purge in the second stage is flowed to input to the first stage. The process efficiently produces a product stream with a helium content of more than 98 percent by volume.
摘要翻译： 所公开的混合膜和变压吸附方法可以从约0.5至5体积％氦的源流中回收氦，并将氦浓缩至大于约98体积％的浓度。 该方法包括一个膜分离，然后是串联使用两个阶段的变压吸附。 源气体将主要含有烃，但将含有一些氮。 膜单元将包含半透膜，其对于氦具有可渗透的选择性，并且在可行的程度上将排除碳氢化合物。 渗透气体的氦气含量将增加2〜10倍。 在变压吸附的第一阶段，残余气体的一部分用于吸附剂床的再生。 变压吸附的每个阶段将包含多个吸附剂床，并且将循环通过多个阶段。 在第一阶段，吸附剂床将依次经历吸附，循环，减压，排空，氦加压和再循环进料加压的阶段。 来自第一阶段的产物气体流到第二阶段，并且在第二阶段中将顺序地经历吸附，减压，抽空，吹扫和氦气加压的阶段。 在第二阶段中排气和吹扫的废气流入第一阶段的输入。 该方法有效地产生氦含量大于98体积％的产物流。
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公开(公告)号：US5542966A
公开(公告)日：1996-08-06
申请号：US326917
申请日：1994-10-21
IPC分类号： B01D53/047 , B01D53/22 , C01B23/00
CPC分类号： C01B23/0094 , B01D53/04 , B01D53/047 , B01D53/229 , C01B23/0052 , B01D2253/102 , B01D2253/104 , B01D2253/106 , B01D2253/304 , B01D2256/18 , B01D2257/11 , B01D2259/404 , B01D2259/406 , B01D2259/41 , C01B2210/001 , C01B2210/0014 , C01B2210/0031 , C01B2210/0068 , C01B2210/007
摘要： The disclosed pressure swing adsorption processes can recover helium from source streams of less than about 10 percent by volume helium and concentrate the helium to a concentration of greater than about 98 percent by volume. Two stages of pressure swing adsorption are used in series. The source of the helium gas will be natural gas wells. The source gas will contain hydrocarbons but in most instances the primary gas other than helium will be nitrogen. Each stage of pressure swing adsorption will contain a plurality of adsorbent beds, and preferably about four. In each stage the adsorbent beds will be cycled through multiple phases. In the first stage the adsorbent beds will sequentially undergo the phases of adsorption, recycle, depressurization, evacuation, helium pressurization and recycle feed pressurization. The product gas from the first stage is flowed to the second stage and in the second stage sequentially will undergo the phases of adsorption, depressurization, evacuation, purge, and helium pressurization. The offgas from evacuation and purge in the second stage is flowed to input to the first stage. The processes using an adsorbent that adsorbs the gases other than helium produces a product stream in a high volume with a helium content of more than 98 percent by volume.
摘要翻译： 公开的变压吸附方法可以从小于约10体积％氦的源流中回收氦，并将氦浓缩至大于约98体积％的浓度。 串联使用两级变压吸附。 氦气的来源将是天然气井。 源气体将含有烃，但在大多数情况下，氦以外的主要气体将是氮气。 变压吸附的每个阶段将包含多个吸附床，优选约四个。 在每个阶段，吸附剂床将循环通过多个阶段。 在第一阶段，吸附剂床将依次经历吸附，循环，减压，排空，氦加压和再循环进料加压的阶段。 来自第一阶段的产物气体流到第二阶段，并且在第二阶段中将顺序地经历吸附，减压，抽空，吹扫和氦气加压的阶段。 在第二阶段排气和吹扫的废气流入第一阶段的输入。 使用吸附除了氦之外的气体的吸附剂的方法产生大体积的产物流，氦含量大于98体积％。
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公开(公告)号：US5536300A
公开(公告)日：1996-07-16
申请号：US326916
申请日：1994-10-21
IPC分类号： B01D53/047 , C10G5/02 , C10L3/10
CPC分类号： B01D53/047 , C10G5/02 , C10L3/10 , B01D2253/102 , B01D2253/116 , B01D2253/304 , B01D2256/10 , B01D2256/24 , B01D2257/102 , B01D2257/504 , B01D2257/702 , B01D2259/40003 , B01D2259/40015 , B01D2259/40032 , B01D2259/403 , B01D53/0476 , Y02C10/08
摘要： A natural gas feed stream containing significant quantities of nitrogen can be increased to a content of greater than 95 percent by volume of natural gas, and preferably greater than about 98 percent, by passing the natural gas feed stream sequentially through at least four adsorbent beds which are cycled through six phases comprising an adsorption phase to adsorb natural gas, a recycle phase to remove feed gas from the voids in the adsorbent bed and nitrogen from the adsorbent by the passage of a depressurization gas therethrough to produce a recycle gas, a depressurization phase to reduce the adsorbent bed pressure to about ambient and to produce the depressurization gas, an evacuation phase where the pressure in the adsorbent is further reduced and an enriched natural gas product stream recovered, a pressurization phase where the pressure in the adsorbent bed is increased using nitrogen gas from a bed in an adsorption phase, and further pressurizing the adsorbent bed in a recycle feed pressurization phase by the flow of the recycle gas therein.
摘要翻译： 通过使天然气进料流顺序地通过至少四个吸附床，可以将含有大量氮的天然气进料流增加到大于95体积％的天然气，优选大于约98％的含量， 通过包含吸附相的六相循环，循环阶段以通过减压气体从吸附剂床中的空隙中除去进料气体和来自吸附剂的氮气，以产生循环气体，减压阶段 将吸附剂床压力降低到大约环境温度并产生减压气体，其中进一步减少吸附剂中的压力并回收富集的天然气产物流的抽空阶段，其中吸附床中的压力增加的加压阶段，其中使用 在吸附相中来自床的氮气，并且在再循环fe中进一步加压吸附剂床 其中的再循环气体的流动被加压。
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公开(公告)号：US4733788A
公开(公告)日：1988-03-29
申请号：US18436
申请日：1987-02-25
申请人： Joseph S. D'Amico
发明人： Joseph S. D'Amico
CPC分类号： A45D40/265
摘要： A fingernail polish bottle has a neck which includes a liquid-holding well formed interiorly of the external threads which receive and retain the bottle's cap. The well captures and collects fingernail polish which runs down the neck so as to prevent the polish from fouling the threads.
摘要翻译： 指甲抛光瓶具有颈部，颈部包括容纳和保持瓶盖的外螺纹内部的液体保持孔。 井捕获并收集在颈部运行的指甲油，以防止抛光剂污染线。
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