公开(公告)号：US08992700B2

公开(公告)日：2015-03-31

申请号：US12474651

申请日：2009-05-29

申请人： Kenneth Rees Bain ,  David Paul Mourer ,  Richard DiDomizio ,  Timothy Hanlon ,  Laurent Cretegny ,  Andrew Ezekiel Wessman

发明人： Kenneth Rees Bain ,  David Paul Mourer ,  Richard DiDomizio ,  Timothy Hanlon ,  Laurent Cretegny ,  Andrew Ezekiel Wessman

IPC分类号： C22C19/05 ,  C22C30/00 ,  C22C1/04

CPC分类号： C22C19/056 ,  B22F2998/00 ,  C22C1/0433 ,  B22F5/009

摘要： A gamma prime nickel-base superalloy and components formed therefrom that exhibit improved high-temperature dwell capabilities, including creep and hold time fatigue crack growth behavior. A particular example of a component is a powder metallurgy turbine disk of a gas turbine engine. The gamma-prime nickel-base superalloy contains, by weight, 18.0 to 30.0% cobalt, 11.4 to 16.0% chromium, up to 6.0% tantalum, 2.5 to 3.5% aluminum, 2.5 to 4.0% titanium, 5.5 to 7.5% molybdenum, up to 2.0% niobium, up to 2.0% hafnium, 0.04 to 0.20% carbon, 0.01 to 0.05% boron, 0.03 to 0.09% zirconium, the balance essentially nickel and impurities, wherein the titanium:aluminum weight ratio is 0.71 to 1.60.

摘要翻译： 一种伽马级镍基超级合金以及由此形成的部件具有改善的高温驻留能力，包括蠕变和保持时间疲劳裂纹扩展行为。 组件的一个具体实例是燃气涡轮发动机的粉末冶金涡轮盘。 γ-贱金属镍基超合金含有18.0至30.0％的钴，11.4至16.0％的铬，至多6.0％的钽，2.5至3.5％的铝，2.5至4.0％的钛，5.5至7.5％的钼， 至2.0％的铌，0.04％至0.20％的碳，0.01至0.05％的硼，0.03至0.09％的锆，余量基本为镍和杂质，其中钛：铝的重量比为0.71至1.60。

公开(公告)号：US20100303665A1

公开(公告)日：2010-12-02

申请号：US12474580

申请日：2009-05-29

申请人： Kenneth Rees Bain ,  David Paul Mourer ,  Richard DiDomizio ,  Timothy Hanlon ,  Laurent Cretegny ,  Andrew Ezekiel Wessman

发明人： Kenneth Rees Bain ,  David Paul Mourer ,  Richard DiDomizio ,  Timothy Hanlon ,  Laurent Cretegny ,  Andrew Ezekiel Wessman

IPC分类号： C22C19/05 ,  C22C30/00

CPC分类号： C22C19/056 ,  B22F3/15 ,  B22F3/20 ,  B22F5/08 ,  B22F2998/00 ,  C22C1/0433 ,  C22C19/057 ,  C22C30/00 ,  C22F1/10 ,  F01D9/02 ,  B22F5/009

摘要： A gamma prime nickel-base superalloy and components formed therefrom that exhibit improved high-temperature dwell capabilities, including creep and hold time fatigue crack growth behavior. A particular example of a component is a powder metallurgy turbine disk of a gas turbine engine. The gamma-prime nickel-base superalloy contains, by weight, 16.0 to 30.0% cobalt, 11.5 to 15.0% chromium, 4.0 to 6.0% tantalum, 2.0 to 4.0% aluminum, 1.5 to 6.0% titanium, up to 5.0% tungsten, 1.0 to 7.0% molybdenum, up to 3.5% niobium, up to 1.0% hafnium, 0.02 to 0.20% carbon, 0.01 to 0.05% boron, 0.02 to 0.10% zirconium, the balance essentially nickel and impurities, wherein the titanium:aluminum weight ratio is 0.5 to 2.0.

摘要翻译： 一种伽马级镍基超级合金以及由此形成的部件具有改善的高温驻留能力，包括蠕变和保持时间疲劳裂纹扩展行为。 组件的一个具体实例是燃气涡轮发动机的粉末冶金涡轮盘。 所述γ型镍基超合金含有16.0〜30.0％的钴，11.5〜15.0％的铬，4.0〜6.0％的钽，2.0〜4.0％的铝，1.5〜6.0％的钛，至多5.0％的钨，1.0 至7.0％的钼，至多3.5％的铌，至多1.0％的铪，0.02至0.20％的碳，0.01至0.05％的硼，0.02至0.10％的锆，余量基本上为镍和杂质，其中钛：铝的重量比为 0.5〜2.0。

公开(公告)号：US08992699B2

公开(公告)日：2015-03-31

申请号：US12474580

申请日：2009-05-29

申请人： Kenneth Rees Bain ,  David Paul Mourer ,  Richard DiDomizio ,  Timothy Hanlon ,  Laurent Cretegny ,  Andrew Ezekiel Wessman

发明人： Kenneth Rees Bain ,  David Paul Mourer ,  Richard DiDomizio ,  Timothy Hanlon ,  Laurent Cretegny ,  Andrew Ezekiel Wessman

IPC分类号： C22C19/05 ,  C22C30/00 ,  C22C1/04 ,  C22F1/10

CPC分类号： C22C19/056 ,  B22F3/15 ,  B22F3/20 ,  B22F5/08 ,  B22F2998/00 ,  C22C1/0433 ,  C22C19/057 ,  C22C30/00 ,  C22F1/10 ,  F01D9/02 ,  B22F5/009

摘要： A gamma prime nickel-base superalloy and components formed therefrom that exhibit improved high-temperature dwell capabilities, including creep and hold time fatigue crack growth behavior. A particular example of a component is a powder metallurgy turbine disk of a gas turbine engine. The gamma-prime nickel-base superalloy contains, by weight, 16.0 to 30.0% cobalt, 11.5 to 15.0% chromium, 4.0 to 6.0% tantalum, 2.0 to 4.0% aluminum, 1.5 to 6.0% titanium, up to 5.0% tungsten, 1.0 to 7.0% molybdenum, up to 3.5% niobium, up to 1.0% hafnium, 0.02 to 0.20% carbon, 0.01 to 0.05% boron, 0.02 to 0.10% zirconium, the balance essentially nickel and impurities, wherein the titanium:aluminum weight ratio is 0.5 to 2.0.

摘要翻译： 一种伽马级镍基超级合金以及由此形成的部件具有改善的高温驻留能力，包括蠕变和保持时间疲劳裂纹扩展行为。 组件的一个具体实例是燃气涡轮发动机的粉末冶金涡轮盘。 所述γ型镍基超合金含有16.0〜30.0％的钴，11.5〜15.0％的铬，4.0〜6.0％的钽，2.0〜4.0％的铝，1.5〜6.0％的钛，至多5.0％的钨，1.0 至7.0％的钼，至多3.5％的铌，至多1.0％的铪，0.02至0.20％的碳，0.01至0.05％的硼，0.02至0.10％的锆，余量基本上为镍和杂质，其中钛：铝的重量比为 0.5〜2.0。

公开(公告)号：US20100303666A1

公开(公告)日：2010-12-02

申请号：US12474651

申请日：2009-05-29

申请人： Kenneth Rees Bain ,  David Paul Mourer ,  Richard DiDomizio ,  Timothy Hanlon ,  Laurent Cretegny ,  Andrew Ezekiel Wessman

发明人： Kenneth Rees Bain ,  David Paul Mourer ,  Richard DiDomizio ,  Timothy Hanlon ,  Laurent Cretegny ,  Andrew Ezekiel Wessman

IPC分类号： C22C19/05 ,  C22C30/00

CPC分类号： C22C19/056 ,  B22F2998/00 ,  C22C1/0433 ,  B22F5/009

摘要： A gamma prime nickel-base superalloy and components formed therefrom that exhibit improved high-temperature dwell capabilities, including creep and hold time fatigue crack growth behavior. A particular example of a component is a powder metallurgy turbine disk of a gas turbine engine. The gamma-prime nickel-base superalloy contains, by weight, 18.0 to 30.0% cobalt, 11.4 to 16.0% chromium, up to 6.0% tantalum, 2.5 to 3.5% aluminum, 2.5 to 4.0% titanium, 5.5 to 7.5% molybdenum, up to 2.0% niobium, up to 2.0% hafnium, 0.04 to 0.20% carbon, 0.01 to 0.05% boron, 0.03 to 0.09% zirconium, the balance essentially nickel and impurities, wherein the titanium:aluminum weight ratio is 0.71 to 1.60.

摘要翻译： 一种伽马级镍基超级合金以及由此形成的部件具有改善的高温驻留能力，包括蠕变和保持时间疲劳裂纹扩展行为。 组件的一个具体实例是燃气涡轮发动机的粉末冶金涡轮盘。 γ-贱金属镍基超合金含有18.0至30.0％的钴，11.4至16.0％的铬，至多6.0％的钽，2.5至3.5％的铝，2.5至4.0％的钛，5.5至7.5％的钼， 至2.0％的铌，0.04％至0.20％的碳，0.01至0.05％的硼，0.03至0.09％的锆，余量基本为镍和杂质，其中钛：铝的重量比为0.71至1.60。

公开(公告)号：US20110203707A1

公开(公告)日：2011-08-25

申请号：US13099641

申请日：2011-05-03

申请人： David Paul Mourer ,  Kenneth Rees Bain

发明人： David Paul Mourer ,  Kenneth Rees Bain

IPC分类号： C22F1/10 ,  C22F1/16 ,  C22C19/05 ,  C22C30/00

CPC分类号： C22C19/056 ,  C22F1/10 ,  C22F1/16

摘要： A gamma prime nickel-base superalloy and components formed therefrom that exhibit improved high-temperature dwell capabilities, including creep and dwell fatigue crack growth behavior. The superalloy contains, by weight, 10.00 to 22.0% cobalt, 10.0 to 14.0% chromium, 4.0 to 6.0% tantalum, 2.0 to 4.0% aluminum, 2.0 to 6.0% titanium, 1.5 to 5.0% tungsten, 1.5 to 5.0% molybdenum, 1.0 to 3.5% niobium, 0.05 to 0.6% hafnium, 0.02 to 0.10% carbon, 0.01 to 0.40% boron, 0.02 to 0.10% zirconium, the balance essentially nickel and impurities, wherein the titanium:aluminum weight ratio is 0.7 to 1.5. The superalloy is hot worked and heat treated to contain cellular gamma prime precipitates that distort grain boundaries, creating tortuous grain boundary fracture paths that are believed to promote the fatigue crack growth resistance of the superalloy.

摘要翻译： 一种伽马级镍基超级合金及其形成的部件，其具有改善的高温停留能力，包括蠕变和驻留疲劳裂纹扩展行为。 超合金含有10.00〜22.0％的钴，10.0〜14.0％的铬，4.0〜6.0％的钽，2.0〜4.0％的铝，2.0〜6.0％的钛，1.5〜5.0的钨，1.5〜5.0的钼，1.0 至3.5％的铌，0.05-0.6％的铪，0.02至0.10％的碳，0.01至0.40％的硼，0.02至0.10％的锆，余量基本为镍和杂质，其中钛：铝的重量比为0.7至1.5。 超合金被热加工和热处理以包含使晶界变形的细胞γ原子沉淀物，产生曲折的晶界断裂路径，据信这可以促进超合金的疲劳裂纹扩展性。

公开(公告)号：US07833472B2

公开(公告)日：2010-11-16

申请号：US11142786

申请日：2005-06-01

申请人： Eric Allen Ott ,  Andrew Philip Woodfield ,  David Paul Mourer ,  John Frederick Ackerman ,  Jon Raymond Groh ,  Robert Edward Schafrik ,  Kenneth Rees Bain ,  Michael Francis Xavier Gigliotti ,  Matthew Bernard Buczek

发明人： Eric Allen Ott ,  Andrew Philip Woodfield ,  David Paul Mourer ,  John Frederick Ackerman ,  Jon Raymond Groh ,  Robert Edward Schafrik ,  Kenneth Rees Bain ,  Michael Francis Xavier Gigliotti ,  Matthew Bernard Buczek

IPC分类号： B22F1/00 ,  B22F1/02

CPC分类号： B22F1/025 ,  B22F2999/00 ,  C23C16/4417 ,  C23C16/442 ,  B22F9/18 ,  B22F9/28

摘要： An article is prepared by furnishing a plurality of powder particle substrates made of a substrate metal, providing a nonmetallic precursor of a metallic coating material, wherein the metallic coating material comprises an alloying element that is thermophysically melt incompatible with the substrate metal, contacting the powder particle substrates with the nonmetallic precursor, chemically reducing the nonmetallic precursor to form coated powder particles comprising the powder particle substrates having a surface-enriched layer of the metallic coating material thereon without melting the powder particle substrates, and processing the coated powder particles to form the article, without melting the powder particle substrates.

摘要翻译： 通过提供由基底金属制成的多个粉末颗粒基底来制备制品，提供金属涂层材料的非金属前体，其中所述金属涂层材料包括与所述基底金属不相容的热物理熔融的合金元素，使所述粉末接触所述粉末 具有非金属前体的化学还原剂，化学还原非金属前体以形成包含粉末颗粒基质的包覆粉末颗粒，所述粉末颗粒基材具有金属涂层材料的表面富集层，而不熔化粉末颗粒基质，并且处理涂覆的粉末颗粒以形成 制品，不熔化粉末颗粒基质。

公开(公告)号：US08613810B2

公开(公告)日：2013-12-24

申请号：US13099641

申请日：2011-05-03

申请人： David Paul Mourer ,  Kenneth Rees Bain

发明人： David Paul Mourer ,  Kenneth Rees Bain

IPC分类号： C22C19/05 ,  C22F1/10

CPC分类号： C22C19/056 ,  C22F1/10 ,  C22F1/16

摘要： A gamma prime nickel-base superalloy and components formed therefrom that exhibit improved high-temperature dwell capabilities, including creep and dwell fatigue crack growth behavior. The superalloy contains, by weight, 10.00 to 22.0% cobalt, 10.0 to 14.0% chromium, 4.0 to 6.0% tantalum, 2.0 to 4.0% aluminum, 2.0 to 6.0% titanium, 1.5 to 5.0% tungsten, 1.5 to 5.0% molybdenum, 1.0 to 3.5% niobium, 0.05 to 0.6% hafnium, 0.02 to 0.10% carbon, 0.01 to 0.40% boron, 0.02 to 0.10% zirconium, the balance essentially nickel and impurities, wherein the titanium:aluminum weight ratio is 0.7 to 1.5. The superalloy is hot worked and heat treated to contain cellular gamma prime precipitates that distort grain boundaries, creating tortuous grain boundary fracture paths that are believed to promote the fatigue crack growth resistance of the superalloy.

摘要翻译： 一种伽马级镍基超级合金及其形成的部件，其具有改善的高温停留能力，包括蠕变和驻留疲劳裂纹扩展行为。 超合金含有10.00〜22.0％的钴，10.0〜14.0％的铬，4.0〜6.0％的钽，2.0〜4.0％的铝，2.0〜6.0％的钛，1.5〜5.0的钨，1.5〜5.0的钼，1.0 至3.5％的铌，0.05-0.6％的铪，0.02至0.10％的碳，0.01至0.40％的硼，0.02至0.10％的锆，余量基本为镍和杂质，其中钛：铝的重量比为0.7至1.5。 超合金被热加工和热处理以包含使晶界变形的细胞γ原子沉淀物，产生曲折的晶界断裂路径，据信这可以促进超合金的疲劳裂纹扩展性。

公开(公告)号：US20090000706A1

公开(公告)日：2009-01-01

申请号：US11770257

申请日：2007-06-28

申请人： Eric Scott Huron ,  Joseph Aloysius Heaney ,  David Paul Mourer ,  Jon Raymond Groh ,  Edward Lee Raymond ,  David Alan Utah ,  Michael James Weimer ,  Kenneth Rees Bain

发明人： Eric Scott Huron ,  Joseph Aloysius Heaney ,  David Paul Mourer ,  Jon Raymond Groh ,  Edward Lee Raymond ,  David Alan Utah ,  Michael James Weimer ,  Kenneth Rees Bain

IPC分类号： C22F1/10 ,  C22C19/05

CPC分类号： C22F1/10 ,  C22C19/056 ,  C22C19/057

摘要： A method of forming a component from a gamma prime precipitation-strengthened nickel-base superalloy. The method entails formulating the superalloy to have a sufficiently high carbon content and forging the superalloy at sufficiently high local strain rates so that, following a supersolvus heat treatment, the component is characterized by a fine and substantially uniform grain size distribution, preferably finer than ASTM 7 and more preferably in a range of about ASTM 8 to 10.

摘要翻译： 一种由伽玛原淀粉强化的镍基超级合金形成组分的方法。 该方法需要配制超级合金以具有足够高的碳含量并以足够高的局部应变速率锻造超合金，使得在超溶氧热处理之后，该组分的特征在于精细且基本均匀的晶粒尺寸分布，优选比ASTM 7，更优选在约8〜10℃的范围内。

公开(公告)号：US20100329883A1

公开(公告)日：2010-12-30

申请号：US12494896

申请日：2009-06-30

申请人： David Paul Mourer ,  Kenneth Rees Bain

发明人： David Paul Mourer ,  Kenneth Rees Bain

IPC分类号： F01D5/28 ,  C22F1/10 ,  C22F1/16 ,  B22D25/06 ,  B22F3/24

CPC分类号： C22C19/056 ,  C22C19/03 ,  C22C19/057 ,  C22F1/10 ,  F05B2230/21

摘要： A gamma prime precipitation-strengthened nickel-base superalloy and method of forging an article from the superalloy to promote a low cycle fatigue resistance and high temperature dwell behavior of the article. The superalloy has a composition of, by weight, 16.0-22.4% cobalt, 6.6-14.3% chromium, 2.6-4.8% aluminum, 2.4-4.6% titanium, 1.4-3.5% tantalum, 0.9-3.0% niobium, 1.9-4.0% tungsten, 1.9-3.9% molybdenum, 0.0-2.5% rhenium, greater than 0.05% carbon, at least 0.1% hafnium, 0.02-0.10% boron, 0.03-0.10% zirconium, the balance nickel and incidental impurities. A billet is formed of the superalloy and worked at a temperature below the gamma prime solvus temperature of the superalloy so as to form a worked article, which is then heat treated above the gamma prime solvus temperature of the superalloy to uniformly coarsen the grains of the article, after which the article is cooled to reprecipitate gamma prime. The article has an average grain size of not coarser than ASTM 7 and is substantially free of critical grain growth.

摘要翻译： 伽马级沉淀强化镍基超级合金和从超合金锻造制品的方法，以促进制品的低循环耐疲劳性和高温停留行为。 超合金具有重量百分比为16.0-22.4％的钴，6.6-14.3％的铬，2.6-4.8％的铝，2.4-4.6％的钛，1.4-3.5％的钽，0.9-3.0％的铌，1.9-4.0％ 钨，1.9-3.9％钼，0.0-2.5％铼，大于0.05％的碳，至少0.1％的铪，0.02-0.10％的硼，0.03-0.10％的锆，余量的镍和附带的杂质。 一个坯料由超级合金制成，并在低于该合金的γ'固溶温度的温度下加工，以便形成一个加工制品，然后在该高温合金的γ'固溶温度之上进行热处理，以均匀地粗化该 制品，之后将制品冷却以再沉淀γ'。 该制品的平均粒度不比ASTM 7粗，并且基本上没有关键的晶粒生长。

公开(公告)号：US20100329876A1

公开(公告)日：2010-12-30

申请号：US12494806

申请日：2009-06-30

申请人： Kenneth Rees Bain ,  David Paul Mourer

发明人： Kenneth Rees Bain ,  David Paul Mourer

IPC分类号： B64C27/46 ,  C22C19/05

CPC分类号： C22C19/056 ,  B22F2998/00 ,  C22C1/0433 ,  C22F1/10 ,  B22F5/009

摘要： Gamma prime nickel-base superalloy and components formed therefrom. The alloy contains, by weight, 11.3 to 13.3% cobalt, 12.4 to 15.2% chromium, 2.1 to 2.7% aluminum, 3.6 to 5.8% titanium, 3.5 to 4.5% tungsten, 3.1 to 3.8% molybdenum, 0.0 to 1.2% niobium, 0.0 to 2.3% tantalum, 0.0 to 0.5% hafnium, 0.040 to 0.100% carbon, 0.010 to 0.046% boron, 0.030 to 0.080% zirconium, the balance nickel and impurities, wherein the Nb+Ta content is 0.0-3.5%.

摘要翻译： 伽玛级镍基超级合金及其成分。 该合金含有11.3至13.3％的钴，12.4至15.2％的铬，2.1至2.7％的铝，3.6至5.8％的钛，3.5至4.5％的钨，3.1至3.8％的钼，0.0至1.2％的铌，0.0 至2.3％的钽，0.0至0.5％的铪，0.040至0.100％的碳，0.010至0.046％的硼，0.030至0.080％的锆，余量的镍和杂质，其中Nb + Ta含量为0.0-3.5％。