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    PREPARING POLYMER COMPOSITE PARTICLE BY MINIEMULSION POLYMERIZATION USING REACTIVE CO-STABILIZER
    3.
    发明申请
    PREPARING POLYMER COMPOSITE PARTICLE BY MINIEMULSION POLYMERIZATION USING REACTIVE CO-STABILIZER 审中-公开
    通过使用反应性稳定剂的微型聚合制备聚合物复合颗粒

    公开(公告)号：US20170045836A1

    公开(公告)日：2017-02-16

    申请号：US14827274

    申请日：2015-08-15

    Applicant: King Abdulaziz City for Science and Technology

    Inventor： AHMED ALI BASFAR ,  Klaus Jähnichen ,  Brigitte Voit

    IPC: G03G9/09 ,  G03G9/097

    CPC classification number: G03G9/0904 ,  C08F2/24 ,  C08F2/26 ,  C08F2/44 ,  C08K3/14 ,  G03G9/09783 ,  C08L25/14

    Abstract: The present disclosure relates to a composition, comprising a monomer; a reactive co-stabilizer; a carbon black; a surfactant; and a filler, wherein the composition is used to prepare a polymer/carbon black composite particle by MEP technology along with a method for same. The reactive co-stabilizer as disclosed is methacrylate derivative containing a long alkyl chain R, with R consisting of 6-22 C atoms and being branched or linear, saturated and/or unsaturated such as stearyl methacrylate (SteaMA). The polymer/carbon black composite particle as prepared has an enhanced stability and low VOC as compared to a pure polymer prepared by MEP. Further, the prepared polymer can be used as basic resins in materials for toner applications.

    Abstract translation: 本公开涉及包含单体的组合物; 活性共稳定剂; 炭黑; 表面活性剂; 和填料，其中所述组合物用于通过MEP技术制备聚合物/炭黑复合颗粒及其方法。 所公开的反应性共稳定剂是含有长烷基链R的甲基丙烯酸酯衍生物，其中R由6-22个C原子组成，是支链或直链，饱和和/或不饱和的，如甲基丙烯酸硬脂酯（SteaMA）。 与由MEP制备的纯聚合物相比，制备的聚合物/炭黑复合颗粒具有增强的稳定性和低VOC。 此外，所制备的聚合物可用作用于调色剂应用的材料中的基础树脂。

    POLYMER NANOPARTICLE PREPARATION BY MINIEMULSION POLYMERIZATION
    4.
    发明申请
    POLYMER NANOPARTICLE PREPARATION BY MINIEMULSION POLYMERIZATION 有权
    通过微型聚合制备聚合物纳米颗粒

    公开(公告)号：US20170044273A1

    公开(公告)日：2017-02-16

    申请号：US14827270

    申请日：2015-08-14

    Applicant: King Abdulaziz City for Science and Technology (KACST)

    Inventor： AHMED ALI BASFAR ,  Klaus Jähnichen ,  Brigitte Voit

    IPC: C08F2/24 ,  C08K3/04 ,  C08F12/08 ,  C08F2/44 ,  G03G9/087

    CPC classification number: C08F2/24 ,  C08F2/44 ,  C08F12/08 ,  C08F112/08 ,  C08F212/08 ,  C08K3/04 ,  G03G9/0806 ,  G03G9/08706 ,  G03G9/08708 ,  C08F2220/1825 ,  C08F220/22 ,  C08L25/06

    Abstract: The present disclosure relates to a composition and a method to prepare a polymer nanoparticle using miniemulsion polymerization (MEP) comprising a monomer, a reactive co-stabilizer and a reactive surfactant. The reactive co-stabilizer as disclosed is a methacrylate containing perfluorinated or semifluorinated side chains like 1H,1H,2H,2H-perfluorodecyl methacrylate (H2F8MA). Further, the reactive stabilizer as used in the preparation is cetyl trimethyl ammonium chloride (CTAB). The polymer nanoparticle as formed has an enhanced stability and low VOC as compared to a pure polymer prepared by MEP.

    Abstract translation: 本公开涉及使用包含单体，反应性共稳定剂和反应性表面活性剂的细乳液聚合（MEP）制备聚合物纳米颗粒的组合物和方法。 所公开的反应性共稳定剂是含有全氟化或半氟化侧链，如1H，1H，2H，2H-全氟癸基甲基丙烯酸酯（H 2 F 8 MA）的甲基丙烯酸酯。 此外，制备中使用的反应性稳定剂是十六烷基三甲基氯化铵（CTAB）。 与由MEP制备的纯聚合物相比，形成的聚合物纳米颗粒具有增强的稳定性和低VOC。

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