公开(公告)号：US06774752B2

公开(公告)日：2004-08-10

申请号：US10345491

申请日：2003-01-17

申请人： Klaus Schlenga ,  Gerhard Roth ,  Arne Kasten

发明人： Klaus Schlenga ,  Gerhard Roth ,  Arne Kasten

IPC分类号： H01F722

CPC分类号： G01R33/3815 ,  Y10S336/01 ,  Y10S505/705 ,  Y10S505/879

摘要： The invention concerns an NMR (nuclear magnetic resonance) high field magnet coil system comprising superconducting conductor structures for generating a homogeneous magnetic field B0 in a measuring volume (23) with several radially nested solenoidal coil sections (12, 13, 31), which is characterized in that the radially innermost coil section (31) is wound with a band-shaped superconductor with an aspect ratio (width to thickness) >3 on a coil support which axially projects, at least at one axial end, past the winding packet of the radially neighboring coil section (12) and the band-shaped superconductor is guided on this side tangentially towards the outside to a region of reduced magnetic field strength and terminates in at least one electrical connecting point (16). This permits use of a brittle band-shaped superconductor for the innermost coil system (31) which cannot be strongly bent at the upper edge.

摘要翻译： 本发明涉及一种包括超导导体结构的NMR（核磁共振）高场磁体线圈系统，用于在具有多个径向嵌套的螺线管线圈段（12,13,31）的测量体积（23）中产生均匀磁场B0， 其特征在于，径向最内侧的线圈部分（31）在线圈支架上缠绕有长宽比（宽度 - 厚度）> 3的带状超导体，至少在一个轴向端部沿轴向突出超过绕组包 径向相邻的线圈部分（12）和带状超导体在该侧面上朝向外侧切向导致磁场强度降低的区域，并且终止于至少一个电连接点（16）。 这允许对最上面的线圈系统（31）使用脆性带状超导体，其不能在上边缘处强烈弯曲。

公开(公告)号：US06600398B2

公开(公告)日：2003-07-29

申请号：US10147474

申请日：2002-05-17

申请人： Gerhard Roth ,  Arne Kasten

发明人： Gerhard Roth ,  Arne Kasten

IPC分类号： H01F600

CPC分类号： G01R33/34053 ,  G01R33/34023 ,  G01R33/34092 ,  H01F6/06 ,  H01F41/048 ,  Y10S505/705 ,  Y10S505/879 ,  Y10S505/924 ,  Y10T29/49014

摘要： A superconducting very high field magnet coil with several solenoidal multi-layer coil sections which are wound in layers onto a hollow cylindrical support body (3) about a common central axis a, and which are electrically connected in series to carry a current in excess of 100 A is characterized in that the radially innermost coil section (1) comprises superconducting wire (2) which contains oxidic, high temperature superconductor (HTS) material, wherein the layers of the radially innermost coil section (1) are helically wound such that there is a free axial space between the walls, which is then sealed. The corresponding production method comprises the steps of helically winding a layer of superconducting HTS wire together with a filler wire onto the support body; removing the filler wire from the support body; repeating steps (a) and (b) until a desired number of layers of the coil section is obtained; thermally treating the winding packet for reacting the HTS material under a gaseous atmosphere containing O2 with optimized annealing parameters; and sealing the hollow spaces of the coil section. This permits production of an NMR-capable solenoid coil having only a few superconducting joints, of topologically simple construction that can carry a current of a few hundred amperes and which contains HTS material to produce magnetic fields in excess of 21 Tesla.

公开(公告)号：US5739689A

公开(公告)日：1998-04-14

申请号：US757702

申请日：1996-12-03

申请人： Gerhard Roth ,  Arne Kasten

发明人： Gerhard Roth ,  Arne Kasten

IPC分类号： F17C3/08 ,  G01R33/3815 ,  H01F6/04 ,  G01V3/00

CPC分类号： G01R33/3815 ,  F17C3/085 ,  H01F6/04 ,  F17C2201/0119 ,  F17C2203/0687 ,  F17C2221/017 ,  F17C2223/0161 ,  F17C2270/0536

摘要： The invention concerns a superconducting magnet configuration for a high resolution NMR spectrometer which is highly stable over time and having a cryostat (21) with a vertical room temperature bore (23). A transverse access (32) through the cryostat (21) to the room temperature bore (23) is provided for at an easily accessible height directly above the upper end of the superconducting magnet coil (25) to substantially simplify the introduction of a sample. In a system having two helium tanks (26, 27), it is advantageous to have the access (32) arranged between these helium tanks.

摘要翻译： 本发明涉及一种用于高分辨率NMR光谱仪的超导磁体配置，该光谱仪随着时间的推移具有高度稳定性，并且具有具有垂直室温孔（23）的低温恒温器（21）。 提供通过低温恒温器（21）到室温孔（23）的横向通路（32），以便在直接位于超导磁体线圈（25）的上端上方的容易接近的高度处，从而大大简化了样品的引入。 在具有两个氦气罐（26,27）的系统中，有利的是在这些氦气罐之间设置通路（32）。

公开(公告)号：US08255022B2

公开(公告)日：2012-08-28

申请号：US12225188

申请日：2007-03-07

申请人： Theo Schneider ,  Gerhard Roth ,  Arne Kasten

发明人： Theo Schneider ,  Gerhard Roth ,  Arne Kasten

IPC分类号： H01F6/04 ,  H01F6/06 ,  G01V3/00

CPC分类号： H01F6/04

摘要： A cryostat (1) with a magnet coil system including superconductors for the production of a magnet field B0 in a measuring volume (3) has a plurality of radially nested solenoid-shaped coil sections (4, 5, 6) which are electrically connected in series, at least one of which being an LTS section (5, 6) with a conventional low temperature superconductor (LTS) and at least one of which being an HTS section (4) including a high temperature superconductor (HTS), wherein the LTS section (5, 6) is located in a first helium tank (9) of the cryostat (1) along with liquid helium at a helium temperature TL

摘要翻译： 具有包括用于在测量体积（3）中产生磁场B0的超导体的磁体线圈系统的低温恒温器（1）具有多个径向嵌套的螺线管状线圈部分（4,5,6），其电连接在 系列，其中至少一个是具有常规低温超导体（LTS）的LTS部分（5,6），并且其中至少一个是包括高温超导体（HTS）的HTS部分（4），其中LTS 部分（5,6）位于低温恒温器（1）的第一氦罐（9）中以及氦温度TL <4K的液氦。该装置的特征在于HTS部分（4）径向地设置 在具有正常液氦的低温恒温器（1）的单独的氦罐（19）内的LTS部分（5,6）内，并且通过至少一个壁与LTS部分（5,6）分开， 氦罐。 根据本发明，HTS线圈段可以在长时间和可靠的方式保持在低温恒温器中。

公开(公告)号：US20090291850A1

公开(公告)日：2009-11-26

申请号：US12225188

申请日：2007-03-07

申请人： Theo Schneider ,  Gerhard Roth ,  Arne Kasten

发明人： Theo Schneider ,  Gerhard Roth ,  Arne Kasten

IPC分类号： G01R33/035 ,  H01F6/06 ,  H01L39/00 ,  F17C3/02

CPC分类号： H01F6/04

摘要： A cryostat (1) with a magnet coil system including superconductors for the production of a magnet field Bo in a measuring volume (3) has a plurality of radially nested solenoid-shaped coil sections (4, 5, 6) which are electrically connected in series, at least one of which being an LTS section (5, 6) with a conventional low temperature superconductor (LTS) and at least one of which being an HTS section (4) including a high temperature superconductor (HTS), wherein the LTS section (5, 6) is located in a first helium tank (9) of the cryostat (1) along with liquid helium at a helium temperature TL

摘要翻译： 具有包括用于在测量体积（3）中产生磁场Bo的超导体的磁体线圈系统的低温恒温器（1）具有多个径向嵌套的螺线管状线圈段（4,5,6），其电连接在 系列，其中至少一个是具有常规低温超导体（LTS）的LTS部分（5,6），并且其中至少一个是包括高温超导体（HTS）的HTS部分（4），其中LTS 部分（5,6）位于低温恒温器（1）的第一氦罐（9）中以及氦温度TL <4K的液氦。该装置的特征在于HTS部分（4）径向地设置 在具有正常液氦的低温恒温器（1）的单独的氦罐（19）内的LTS部分（5,6）内，并且通过至少一个壁与LTS部分（5,6）分开， 氦罐。 根据本发明，HTS线圈段可以在长时间和可靠的方式保持在低温恒温器中。

公开(公告)号：US5721522A

公开(公告)日：1998-02-24

申请号：US609802

申请日：1996-03-01

申请人： Gerhard Roth ,  Arne Kasten

发明人： Gerhard Roth ,  Arne Kasten

IPC分类号： F17C13/00 ,  G01R33/3815 ,  H01F6/04 ,  H01F1/00

CPC分类号： H01F6/04 ,  G01R33/3815

摘要： In a superconducting magnet coil configuration, in particular for a high resolution analytical nuclear resonance (NMR) spectrometer, with a cryostat having extremely low heat losses (low loss), comprising at least one essentially cylindrical container (1) with a vertical cylinder axis (k), with a vertical cylindrical room temperature bore (3) and with at least one inner tank (4) for a cryogenic liquid in thermal contact with a superconducting magnet coil (2) enclosing the room temperature bore (3), for generating a vertically directed, extremely homogeneous and stable magnetic field of high field strength inside a measuring volume of the room temperature bore (3), the vertical axes (r) of the room temperature bore (3) and of the superconducting magnet coil (2) run parallel to and at a distance from the vertical cylinder axis (k) of at least one of the cylindrical cryostat containers (1). In this way, access to the room temperature bore (3) is considerably simplified.

摘要翻译： 在超导磁体线圈配置中，特别是对于具有极低热损失（低损耗）的低温恒温器的高分辨率分析核共振（NMR）光谱仪，包括至少一个具有垂直圆柱体轴线的基本上圆柱形的容器（1） k），具有垂直圆柱形室温孔（3）和至少一个用于与包围室温孔（3）的超导磁体线圈（2）热接触的低温液体的内罐（4），用于产生 在室温孔（3）的测量体积，室温膛（3）和超导磁体线圈（2）的垂直轴（r）运行的高场强度的垂直方向，非常均匀和稳定的磁场 平行于至少一个圆柱形低温恒温器容器（1）的垂直圆柱体轴线（k）并与其一定距离。 以这种方式，可以大大简化对室温膛（3）的访问。

公开(公告)号：US07183769B2

公开(公告)日：2007-02-27

申请号：US11047637

申请日：2005-02-02

申请人： Arne Kasten ,  Michael Westphal

发明人： Arne Kasten ,  Michael Westphal

IPC分类号： G01V3/00

CPC分类号： G01R33/389 ,  G01R33/3815 ,  G01R33/421

摘要： The system describes a means and a method for stabilizing the magnetic field generated in the measuring volume of a high-resolution magnetic resonance spectrometer having an actively shielded magnet coil (4) which is located in a cryostat (2) and which is superconductingly short-circuited. The system comprises a compensation coil (12) which is decoupled from the magnet coil (4), and is disposed on the shielding coil (4b) of the magnet coil (4).

摘要翻译： 该系统描述了用于稳定在高分辨率磁共振光谱仪的测量体积中产生的磁场的方法和方法，所述高分辨率磁共振光谱仪具有位于低温恒温器（2）中的主动屏蔽的磁体线圈（4），并且是超导短路的， 电路 该系统包括与磁体线圈（4）去耦的补偿线圈（12），并设置在电磁线圈（4）的屏蔽线圈（4b）上。

公开(公告)号：US20060108534A1

公开(公告)日：2006-05-25

申请号：US11257765

申请日：2005-10-25

申请人： Gijsbertus Kerpershoek ,  Leendert Seijbel ,  Arjen Storm ,  Arne Kasten

发明人： Gijsbertus Kerpershoek ,  Leendert Seijbel ,  Arjen Storm ,  Arne Kasten

IPC分类号： G01T1/24

CPC分类号： G01N23/20008

摘要： An X-ray analysis device makes use of a variable aperture for controlling the position and cross section of the X-ray beam. The variable aperture is configured to allow changes in the cross section and/or position of the beam by movement of one aperture component in one direction. In one embodiment, the aperture medium is a perforated disk that is rotated to expose different aperture holes to the beam. In another embodiment, the aperture medium is a perforated tape that is moved in a linear direction to expose different aperture holes to the beam. The tape may be wound about two axes to control its movement, or may be a continuous loop. A cassette may also be used to house the tape.

摘要翻译： X射线分析装置利用可变孔径来控制X射线束的位置和横截面。 可变孔径被配置为允许通过一个孔径分量在一个方向上的移动来改变横梁的横截面和/或位置。 在一个实施例中，孔介质是被旋转以暴露到梁的不同孔径的多孔盘。 在另一个实施例中，孔径介质是穿过带状物，其沿直线方向移动以暴露到梁的不同孔径。 磁带可以围绕两个轴线缠绕以控制其运动，或者可以是连续的环路。 也可以使用盒式磁带来容纳磁带。

公开(公告)号：US06972566B2

公开(公告)日：2005-12-06

申请号：US10764981

申请日：2004-01-26

申请人： Gisela Guthausen ,  Arne Kasten

发明人： Gisela Guthausen ,  Arne Kasten

IPC分类号： G01N24/08 ,  G01R33/44 ,  G01V3/00

CPC分类号： G01R33/44 ,  G01N24/08

摘要： A description is given of a method for determining the content of a first component of a sample, which first component provides a first NMR signal and has a first self-diffusion coefficient D1, the sample additionally containing at least one further component which provides a further NMR signal and has a larger self-diffusion coefficient D2, in particular for determining the fat content of a hydrous sample, with the aid of a low-resolution nuclear magnetic resonance (NMR) pulse spectrometer, the sample being excited by a radio-frequency (RF) excitation pulse and being exposed to a magnetic gradient field and to a sequence of further refocusing RF pulses for generating spin echo signals, the spin echo signals being detected and their amplitude values being determined, from which a value for the content of the first component of the sample is determined. The magnetic gradient field is not switched off during the sequence of further refocusing RF pulses.

摘要翻译： 给出了用于确定样品的第一组分的含量的方法的描述，该第一组分提供第一NMR信号并具有第一自扩散系数D 1，样品另外含有 至少一个另外的组分，其提供另外的NMR信号并且具有较大的自扩散系数D 2，特别是用于通过低分辨率核磁铁来确定含水样品的脂肪含量 共振（NMR）脉冲光谱仪，样品被射频（RF）激发脉冲激发并暴露于磁梯度场和进一步重新聚焦RF脉冲序列以产生自旋回波信号，检测到自旋回波信号 并且确定它们的振幅值，由此确定样品的第一组分的含量的值。 在进一步重新聚焦RF脉冲的序列期间，磁梯度场不被关闭。

公开(公告)号：US06727699B2

公开(公告)日：2004-04-27

申请号：US10050996

申请日：2002-01-22

申请人： Arne Kasten

发明人： Arne Kasten

IPC分类号： G01V300

CPC分类号： G01R33/389 ,  G01R33/3815

摘要： The invention concerns a means and a method for stabilizing a magnetic field generated by a superconductingly short-circuited main coil located in a cryostat in the measuring volume of a high-resolution magnetic resonance spectrometer, which comprises compensation coils which are dimensioned and positioned such that they, in their entirety, are suited to largely compensate for field drifts of the superconductingly short-circuited main coil in the measuring volume. The drift compensation coils consist of HTS material and are disposed radially outside of the main coil at a higher temperature level.

摘要翻译： 本发明涉及一种用于稳定位于高分辨率磁共振光谱仪的测量体积中的低温恒温器中的超导短路主线圈所产生的磁场的方法和方法，该补偿线圈的尺寸和位置使得 它们整体上适合于大大地补偿测量体积中超导短路主线圈的场漂移。 漂移补偿线圈由HTS材料组成，并在较高的温度水平位于主线圈的径向外侧。