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公开(公告)号：US5478919A
公开(公告)日：1995-12-26
申请号：US283268
申请日：1994-07-29
CPC分类号： C08G69/10 , C08G73/1092
摘要： Aspartic acid precursors such as mono and diammonium maleate, maleamic acid, ammonium maleamate, ammonium malate and mixtures of these and other precursors are copolycondensed thermally with a variety of mono, di and multifunctional monomers containing amino, hydroxyl and carboxyl functional groups. The resulting condensation copolymers and terpolymers contain succinimide units derived from aspartic acid precursors, condensed with other functional group monomers usually though amide and ester linkages. Hydrolysis of the polysuccinimide copolymers and terpolymers with alkali, alkaline earth and ammonium hydroxide produces aspartic acid copolymer and terpolymer salts.
摘要翻译： 天冬氨酸前体如马来酸单和二铵，马来酰胺酸，马来酸铵，马来酸铵，这些和其它前体的混合物与含有氨基，羟基和羧基官能团的各种单，二和多官能单体共缩聚。 所得的缩合共聚物和三元共聚物含有衍生自天冬氨酸前体的琥珀酰亚胺单元，其通常通过酰胺和酯键与其它官能团单体缩合。 聚琥珀酰亚胺共聚物和三元共聚物与碱金属，碱土金属和氢氧化铵的水解产生天冬氨酸共聚物和三元共聚物盐。
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公开(公告)号：USRE36234E
公开(公告)日：1999-06-22
申请号：US995444
申请日：1997-12-22
CPC分类号： C08G69/10 , C08G73/1092
摘要： Aspartic acid precursors such as mono and diammonium maleate, maleamic acid, ammonium maleamate, ammonium malate and mixtures of these and other precursors are copolycondensed thermally with a variety of mono, di and multifunctional monomers containing amino, hydroxyl and carboxyl functional groups. The resulting condensation copolymers and terpolymers contain succinimide units derived from aspartic acid precursors, condensed with other functional group monomers usually .�.though.!. .Iadd.through .Iaddend.amide and ester linkages. Hydrolysis of the polysuccinimide copolymers and terpolymers with alkali, alkaline earth and ammonium hydroxide produces aspartic acid copolymer and terpolymer salts.
摘要翻译： 天冬氨酸前体如马来酸单和二铵，马来酰胺酸，马来酸铵，马来酸铵，这些和其它前体的混合物与含有氨基，羟基和羧基官能团的各种单，二和多官能单体共缩聚。 所得的缩合共聚物和三元共聚物含有衍生自天冬氨酸前体的琥珀酰亚胺单元，其与通常通过酰胺和酯键的其它官能团单体缩合。 聚琥珀酰亚胺共聚物和三元共聚物与碱金属，碱土金属和氢氧化铵的水解产生天冬氨酸共聚物和三元共聚物盐。
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3.发明授权Methods to recover and reclaim hydrocarbons or hydrophobic substances in an aqueous environment 有权在含水环境中回收和回收碳氢化合物或疏水物质的方法公开(公告)号：US08628669B2
公开(公告)日：2014-01-14
申请号：US13164642
申请日：2011-06-20
申请人： Larry P. Koskan , Abdul R. Meah , Jon Vander Woude
发明人： Larry P. Koskan , Abdul R. Meah , Jon Vander Woude
CPC分类号： C02F1/5272 , C02F1/285 , C02F1/56 , C02F1/681 , C02F2101/32
摘要： The present invention provides useful biodegradable and environmentally friendly cost effective methods for oil recovery and reclamation from oil spills and chemical spills. More particularly, methods to recover and reclaim hydrocarbons or hydrophobic substances in an aqueous environment.
摘要翻译： 本发明提供了用于石油泄漏和化学品泄漏的油回收和回收的有用的可生物降解和环境友好的成本有效的方法。 更具体地，在水性环境中回收和回收碳氢化合物或疏水性物质的方法。
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公开(公告)号：US20130248186A1
公开(公告)日：2013-09-26
申请号：US13781367
申请日：2013-03-28
申请人： Larry P. Koskan , Abdul R. Meah
发明人： Larry P. Koskan , Abdul R. Meah
摘要： An illustrative method of reducing an amount of treatment water injected into a subterranean well may include providing an environmentally friendly polymer, such as a biodegradable polymer (e.g., an aspartic acid based polymer), to the subterranean well. In some cases, the aspartic acid based polymer may include one or more of a copolymer of the aspartic acid based polymer, a terpolymer of the aspartic acid based polymer, an aspartic acid based polymer derivative, an aspartic acid based polymer having an end cap, and a soluble salt of the aspartic acid based polymer. In some cases, the treatment water use may be reduced within the range of about five percent to about ninety five percent.
摘要翻译： 减少注入地下井的处理水量的说明性方法可以包括向地下井提供环境友好的聚合物，例如可生物降解的聚合物（例如天冬氨酸基聚合物）。 在一些情况下，天冬氨酸类聚合物可以包括天冬氨酸类聚合物的共聚物，天冬氨酸类聚合物的三元共聚物，天冬氨酸类聚合物衍生物，具有端帽的天冬氨酸类聚合物， 和天冬氨酸类聚合物的可溶性盐。 在一些情况下，处理用水可以在约百分之五至百分之九十五的范围内降低。
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公开(公告)号：US5373088A
公开(公告)日：1994-12-13
申请号：US188539
申请日：1994-01-28
申请人： Larry P. Koskan , Abdul R. Y. Meah
发明人： Larry P. Koskan , Abdul R. Y. Meah
CPC分类号： C08G69/08 , C08G69/10 , C08G73/1092
摘要： Polyaspartic acid is produced by thermal condensation of ammonium maleate derived from maleic acid and ammonia. Solid ammonium maleate in particulate form is heated to a temperature of at least about 170.degree. C. to effect thermal condensation to a polysuccinimide which is then base hydrolyzed to a polyaspartic acid salt.
摘要翻译： 聚天冬氨酸通过马来酸铵和氨的马来酸铵的热缩合而产生。 颗粒形式的马来酸固体马来酸盐被加热到至少约170℃的温度，以进行聚琥珀酰亚胺的热冷凝，然后将其碱基水解成聚天冬氨酸盐。
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6.发明授权
公开(公告)号：US5057597A
公开(公告)日：1991-10-15
申请号：US547875
申请日：1990-07-03
申请人： Larry P. Koskan
发明人： Larry P. Koskan
CPC分类号： C08G73/1092
摘要： A process for the manufacture of polyamino acids, particularly polyaspartic acid. A solid, particulate, amino acid is fluidized by agitation in a nitrogen atmosphere and heated to a temperature of at least 180.degree. C. and maintained at that temperature for a sufficient amount of time to polymerize the amino acid and to drive off water from the heated bed. A degree of agitation sufficient to substantially fluidize the particles is provided and a particle size of no more than 150 microns is maintained throughout the process. The resultant anhydropolyamino acid is then hydrolyzed to a polyamino acid.
摘要翻译： 一种制备聚氨基酸，特别是聚天冬氨酸的方法。 固体颗粒状氨基酸通过在氮气气氛中搅拌而流化并加热到至少180℃的温度，并在该温度下保持足够的时间以聚合氨基酸并从水中除去水 加热床。 提供足以使颗粒基本上流化的搅拌程度，并且在整个过程中保持不超过150微米的粒度。 然后将所得的脱氢氨基酸水解成聚氨基酸。
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公开(公告)号：US5552516A
公开(公告)日：1996-09-03
申请号：US263459
申请日：1994-06-22
申请人： Robert J. Ross , Kim C. Low , Larry P. Koskan
发明人： Robert J. Ross , Kim C. Low , Larry P. Koskan
CPC分类号： C02F5/12 , C08G73/1092 , C11D3/3719
摘要： Disclosed are methods of producing high molecular weight, soluble, crosslinked polyaspartates from crosslinked polysuccinimide. In one preferred method aspect, polysuccinimide is first reacted with an organic crosslinking agent, preferably an organic base containing at least two primary amine groups to form a crosslinked polysuccinimide. The crosslinked polysuccinimide is then hydrolyzed to crosslinked polyaspartate which is soluble in polar solvents, preferably water, alcohol and mixtures thereof. Alternative method aspects are disclosed in which soluble crosslinked polyaspartates are produced in a single reaction vessel by sequentially crosslinking polysuccinimide with the organic crosslinking agent in an aqueous reaction mixture and hydrolyzing the product to crosslinked polyaspartate.
摘要翻译： 公开了从交联聚琥珀酰亚胺生产高分子量可溶性交联聚天冬氨酸酯的方法。 在一个优选的方法中，聚琥珀酰亚胺首先与有机交联剂，优选含有至少两个伯胺基团的有机碱反应以形成交联的聚琥珀酰亚胺。 然后将交联的聚琥珀酰亚胺水解成可溶于极性溶剂，优选水，醇及其混合物的交联聚天冬氨酸酯。 公开了可替代的方法方面，其中可溶性交联聚天冬氨酸酯通过在含水反应混合物中顺序交联聚琥珀酰亚胺与有机交联剂并将产物水解成交联的聚天冬氨酸酯而在单个反应容器中制备。
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8.发明授权Polyaspartic acid having more than 50% .beta. form and less that 50% .alpha. form 失效具有超过50％β形式和少于50％α形式的聚天冬氨酸
公开(公告)号：US5373086A
公开(公告)日：1994-12-13
申请号：US186974
申请日：1994-01-26
申请人： Larry P. Koskan , Kim C. Low , Abdul R. Y. Meah , Anne M. Atencio
发明人： Larry P. Koskan , Kim C. Low , Abdul R. Y. Meah , Anne M. Atencio
IPC分类号： C08G69/10 , C02F5/12 , C07C237/22 , C08G63/685 , C08G73/10 , C09K8/528 , C11D3/37
CPC分类号： C02F5/12 , C07C237/22 , C08G63/6852 , C08G69/10 , C08G73/1092 , C09K8/528 , C11D3/3719
摘要： .beta.-Polyaspartic acid having a weight average molecular weight of 1000 to 5000 produced by hydrolysis of anhydropolyaspartic acid exhibits a high degree of calcium carbonate and calcium phosphate inhibition.
摘要翻译： 通过水解脱水天冬氨酸产生的重均分子量为1000〜5000的β-聚天冬氨酸显示出高度的碳酸钙和磷酸钙抑制。
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公开(公告)号：US5350735A
公开(公告)日：1994-09-27
申请号：US972375
申请日：1992-11-05
IPC分类号： A01N37/44 , A01N33/04 , A01N37/18 , A01N37/46 , A01N59/00 , A01N61/00 , A01P21/00 , C05F11/00 , C05G3/00 , C05G3/02
CPC分类号： C05G3/0064 , A01N37/46 , C05F11/00 , C05G3/00
摘要： Water-soluble poly(organic acids) having a molecular size of more than 1,500 Daltons enhance fertilizer uptake and promote plant growth. Particularly suitable for this purpose are the poly(amino acids) such as poly(aspartic acid) and copolymers thereof.
摘要翻译： 分子量大于1500道尔顿的水溶性聚（有机酸）增强了肥料吸收并促进植物生长。 特别适合于此目的的是聚（氨基酸）如聚（天冬氨酸）及其共聚物。
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公开(公告)号：US4100258A
公开(公告)日：1978-07-11
申请号：US677924
申请日：1976-04-19
申请人： Peter H. Vossos , Morris Mindick , Larry P. Koskan
发明人： Peter H. Vossos , Morris Mindick , Larry P. Koskan
CPC分类号： B01D53/501
摘要： SO.sub.3 is removed from flue gas by injecting liquid sodium aluminate, achieving essentially complete SO.sub.3 removal.
摘要翻译： 通过注入液体铝酸钠从烟道气中除去SO3，实现基本上完全的SO 3去除。
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