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1.发明申请公开(公告)号：US20070135637A1
公开(公告)日：2007-06-14
申请号：US10581311
申请日：2004-12-02
申请人： Marco Bosch , Ulrich Muller , Matthias Frauenkron
发明人： Marco Bosch , Ulrich Muller , Matthias Frauenkron
IPC分类号： C01B39/00 , B01J29/00 , B01J29/06 , C07D487/04
CPC分类号： B01J29/40 , B01J35/023 , B01J37/0009 , B01J37/0018 , B01J2229/42 , C01B39/36 , C01B39/40 , C07D487/08
摘要： Zeolite material of the pentasil type has an alkali metal and alkaline earth metal content of not more than 100 ppm and a molar ratio of Si to Al of from 250 to 1500, at least 90% of the primary particles of the zeolite material being spherical and 95% by weight of the spherical primary particles having a diameter of less than or equal to 1 μm.
摘要翻译： pentasil型沸石材料的碱金属和碱土金属含量不超过100ppm，Si与Al的摩尔比为250至1500，沸石材料的初级颗粒的至少90％为球形， 95重量％的直径小于或等于1μm的球形初级颗粒。
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公开(公告)号：US20060116517A1
公开(公告)日：2006-06-01
申请号：US10559493
申请日：2004-06-04
申请人： Marco Bosch , Bernd Stein , Matthias Frauenkron , Ulrich Muller
发明人： Marco Bosch , Bernd Stein , Matthias Frauenkron , Ulrich Muller
IPC分类号： C07D487/04 , C04B33/34
CPC分类号： C07D487/08 , B01J29/06 , B01J29/40 , B01J2229/36
摘要： An increase in the cutting hardness of a shaped body comprising a crystalline aluminosilicate is achieved by treating the shaped body with a gas comprising water vapor at from 100 to 600° C. and an absolute pressure of from 0.1 to 10 bar for a period of at least 20 hours, and this shaped body having an increased cutting hardness can be used in processes for chemical synthesis, in particular in a process for preparing triethylenediamine (TEDA) by reaction of ethylenediamine (EDA) and/or piperazine (PIP).
摘要翻译： 包含结晶硅铝酸盐的成形体的切削硬度的增加通过用包含100-600℃的水蒸气和0.1至10巴的绝对压力的气体处理成型体达到一段时间 至少20小时，具有增加的切削硬度的成形体可用于化学合成的方法中，特别是在通过乙二胺（EDA）和/或哌嗪（PIP）的反应制备三亚乙基二胺（TEDA）的方法中。
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3.发明授权Shaped body containing a microporous material and at least one silicon-containing binder, method for the production thereof and its use as a catalyst, particularly in a method for producing triethylenediamine (TEDA). 有权包含微孔材料和至少一种含硅粘合剂的成形体，其制备方法及其作为催化剂的用途，特别是在三亚乙基二胺（TEDA）的制造方法中。公开(公告)号：US07582583B2
公开(公告)日：2009-09-01
申请号：US11629889
申请日：2005-06-10
申请人： Marco Bosch , Matthias Frauenkron , Milan Kostur , Otto Hofstadt
发明人： Marco Bosch , Matthias Frauenkron , Milan Kostur , Otto Hofstadt
IPC分类号： B01J29/06 , C07C209/60
CPC分类号： B01J37/086 , B01J29/06 , B01J29/40 , B01J35/002 , B01J35/023 , B01J37/0009 , B01J2229/42 , C07D487/08 , Y10T428/256
摘要： Process for producing a shaped body comprising a microporous material and at least one silicon-containing binder, which comprises the steps (I) preparing a mixture comprising the microporous material, the binder, a make-up aid and a solvent, (II) mixing and densifying the mixture, (III) shaping the densified mixture to give a shaped body, (IV) drying the shaped body and (V) calcining the dried shaped body, wherein the binder used is an organosilicon compound, shaped bodies which can be produced by this process, their use as catalyst, in particular in organic synthesis and very particularly preferably in a process for preparing triethylenediamine (TEDA).
摘要翻译： 包括微孔材料和至少一种含硅粘合剂的成形体的制造方法，其包括步骤（I）制备包含微孔材料，粘合剂，补充助剂和溶剂的混合物，（II）混合 （III）使致密混合物成形，得到成型体，（IV）干燥成形体，（V）煅烧干燥的成形体，其中使用的粘合剂是有机硅化合物，可以生产的成形体 通过该方法，它们用作催化剂，特别是在有机合成中，非常特别优选用于制备三亚乙基二胺（TEDA）的方法。
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4.发明申请PENTASIL-STRUCTURE ZEOLITHIC MATERIAL THE PRODUCTION AND USE THEREOF 有权PENTASIL-STRUCTURE ZEOLITHIC材料的生产和使用公开(公告)号：US20110144335A1
公开(公告)日：2011-06-16
申请号：US13030689
申请日：2011-02-18
申请人： Marco Bosch , Ulrich Müller , Matthias Frauenkron
发明人： Marco Bosch , Ulrich Müller , Matthias Frauenkron
IPC分类号： B01J29/40 , C07D487/08
CPC分类号： B01J29/40 , B01J35/023 , B01J37/0009 , B01J37/0018 , B01J2229/42 , C01B39/36 , C01B39/40 , C07D487/08
摘要： Zeolite material of the pentasil type has an alkali metal and alkaline earth metal content of not more than 100 ppm and a molar ratio of Si to Al of from 250 to 1500, at least 90% of the primary particles of the zeolite material being spherical and 95% by weight of the spherical primary particles having a diameter of less than or equal to 1 μm.
摘要翻译： pentasil型沸石材料的碱金属和碱土金属含量不超过100ppm，Si与Al的摩尔比为250至1500，沸石材料的初级颗粒的至少90％为球形， 95重量％的直径小于或等于1μm的球形初级颗粒。
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公开(公告)号：US07132538B2
公开(公告)日：2006-11-07
申请号：US10829176
申请日：2004-04-22
申请人： Ortmund Lang , Bernd Rumpf , Matthias Frauenkron , Marco Bosch , Helmut Berrsche , Anton Meier
发明人： Ortmund Lang , Bernd Rumpf , Matthias Frauenkron , Marco Bosch , Helmut Berrsche , Anton Meier
IPC分类号： C07D487/00
CPC分类号： C07D487/08 , B01D3/14 , B01D3/141 , B01D3/322 , B01J2219/32 , C07C209/84 , C07C211/10
摘要： Process for purifying triethylenediamine (TEDA) by disillation, in which the fractionation is carried out in a dividing wall column.
摘要翻译： 通过蒸馏纯化三亚乙基二胺（TEDA）的方法，其中分馏在分隔壁塔中进行。
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6.发明授权公开(公告)号：US08344141B2
公开(公告)日：2013-01-01
申请号：US13030689
申请日：2011-02-18
申请人： Marco Bosch , Ulrich Müller , Matthias Frauenkron
发明人： Marco Bosch , Ulrich Müller , Matthias Frauenkron
IPC分类号： C07D487/08
CPC分类号： B01J29/40 , B01J35/023 , B01J37/0009 , B01J37/0018 , B01J2229/42 , C01B39/36 , C01B39/40 , C07D487/08
摘要： Zeolite material of the pentasil type has an alkali metal and alkaline earth metal content of not more than 100 ppm and a molar ratio of Si to Al of from 250 to 1500, at least 90% of the primary particles of the zeolite material being spherical and 95% by weight of the spherical primary particles having a diameter of less than or equal to 1 μm.
摘要翻译： pentasil型沸石材料的碱金属和碱土金属含量不超过100ppm，Si与Al的摩尔比为250至1500，沸石材料的初级颗粒的至少90％为球形， 95重量％的直径小于或等于1μm的球形初级颗粒。
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7.发明授权公开(公告)号：US07902102B2
公开(公告)日：2011-03-08
申请号：US10581311
申请日：2004-12-02
申请人： Marco Bosch , Ulrich Müller , Matthias Frauenkron
发明人： Marco Bosch , Ulrich Müller , Matthias Frauenkron
CPC分类号： B01J29/40 , B01J35/023 , B01J37/0009 , B01J37/0018 , B01J2229/42 , C01B39/36 , C01B39/40 , C07D487/08
摘要： Zeolite material of the pentasil type has an alkali metal and alkaline earth metal content of not more than 100 ppm and a molar ratio of Si to Al of from 250 to 1500, at least 90% of the primary particles of the zeolite material being spherical and 95% by weight of the spherical primary particles having a diameter of less than or equal to 1 μm.
摘要翻译： pentasil型沸石材料的碱金属和碱土金属含量不超过100ppm，Si与Al的摩尔比为250至1500，沸石材料的初级颗粒的至少90％为球形， 95重量％的直径小于或等于1μm的球形初级颗粒。
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公开(公告)号：US07754139B2
公开(公告)日：2010-07-13
申请号：US10559493
申请日：2004-06-04
申请人： Marco Bosch , Bernd Stein , Matthias Frauenkron , Ulrich Müller
发明人： Marco Bosch , Bernd Stein , Matthias Frauenkron , Ulrich Müller
IPC分类号： B28B3/20
CPC分类号： C07D487/08 , B01J29/06 , B01J29/40 , B01J2229/36
摘要： An increase in the cutting hardness of a shaped body comprising a crystalline aluminosilicate is achieved by treating the shaped body with a gas comprising water vapor at from 100 to 600° C. and an absolute pressure of from 0.1 to 10 bar for a period of at least 20 hours, and this shaped body having an increased cutting hardness can be used in processes for chemical synthesis, in particular in a process for preparing triethylenediamine (TEDA) by reaction of ethylenediamine (EDA) and/or piperazine (PIP).
摘要翻译： 包含结晶硅铝酸盐的成形体的切削硬度的增加通过用包含100-600℃的水蒸气和0.1至10巴的绝对压力的气体处理成形体来实现一段时间 至少20小时，具有增加的切削硬度的成形体可用于化学合成的方法中，特别是在通过乙二胺（EDA）和/或哌嗪（PIP）的反应制备三亚乙基二胺（TEDA）的方法中。
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9.发明申请Shaped Body Containing a Microporous Material and at Least One Silicon-Containing Binder, Method For the Production Thereof and Its Use as a Catalyst, Particularly in a Method For Producing Triethylenediamine (Teda) 有权包含微孔材料和至少一种含硅粘合剂的成形体，其制备方法及其作为催化剂的用途，特别是在制备三乙二胺（Teda）的方法中，公开(公告)号：US20080221326A1
公开(公告)日：2008-09-11
申请号：US11629889
申请日：2005-06-10
申请人： Marco Bosch , Matthias Frauenkron , Milan Kostur , Otto Hofstadt
发明人： Marco Bosch , Matthias Frauenkron , Milan Kostur , Otto Hofstadt
CPC分类号： B01J37/086 , B01J29/06 , B01J29/40 , B01J35/002 , B01J35/023 , B01J37/0009 , B01J2229/42 , C07D487/08 , Y10T428/256
摘要： Process for producing a shaped body comprising a microporous material and at least one silicon-containing binder, which comprises the steps (I) preparing a mixture comprising the microporous material, the binder, a make-up aid and a solvent, (II) mixing and densifying the mixture, (III) shaping the densified mixture to give a shaped body, (IV) drying the shaped body and (V) calcining the dried shaped body, wherein the binder used is an organosilicon compound, shaped bodies which can be produced by this process, their use as catalyst, in particular in organic synthesis and very particularly preferably in a process for preparing triethylenediamine (TEDA).
摘要翻译： 包括微孔材料和至少一种含硅粘合剂的成形体的制造方法，其包括步骤（I）制备包含微孔材料，粘合剂，补充助剂和溶剂的混合物，（II）混合 （III）使致密混合物成形，得到成型体，（IV）干燥成形体，（V）煅烧干燥的成形体，其中使用的粘合剂是有机硅化合物，可以生产的成形体 通过该方法，它们用作催化剂，特别是在有机合成中，非常特别优选用于制备三亚乙基二胺（TEDA）的方法。
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公开(公告)号：US20060276649A1
公开(公告)日：2006-12-07
申请号：US10566419
申请日：2004-07-15
申请人： Matthias Frauenkron , Thomas Krug , Holger Evers , Johann-Peter Melder , Roderich Rottger , Markus Siegert , Till Gerlach , Jan Nouwen , Ellen Dahlhoff , Christian Miller
发明人： Matthias Frauenkron , Thomas Krug , Holger Evers , Johann-Peter Melder , Roderich Rottger , Markus Siegert , Till Gerlach , Jan Nouwen , Ellen Dahlhoff , Christian Miller
IPC分类号： C07D241/04 , C07C211/13 , C07C211/09
CPC分类号： C07C209/64 , C07C211/14
摘要： Process for the preparation of ethylenamines, in particular diethylenetriamine (DETA), by continuous reaction of ethylenediamine (EDA) in the presence of a heterogeneous catalyst, where the reaction is carried out in a reaction column.
摘要翻译： 通过乙二胺（EDA）在多相催化剂存在下连续反应制备乙烯胺，特别是二亚乙基三胺（DETA）的方法，其中反应在反应塔中进行。
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