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公开(公告)号：US5166360A
公开(公告)日：1992-11-24
申请号：US697027
申请日：1991-05-07
IPC分类号： C07D209/48
CPC分类号： C07D209/48
摘要： The yellowness index of a flame retardant N,N'-alkylene-bis-(tetrahalophthalimide), such as N,N'-ethylene-bis-(tetrabromophthalimide), is reduced by treating the bis-imide with strong mineral acid.
摘要翻译： 通过用强无机酸处理双酰亚胺，可以减少阻燃剂N，N'-亚烷基 - 双 - （四卤代邻苯二甲酰亚胺）如N，N'-亚乙基 - 双（邻溴苯二酰亚胺）的黄度指数。
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公开(公告)号：US5141652A
公开(公告)日：1992-08-25
申请号：US714211
申请日：1991-06-12
摘要： This invention relates to a process for reducing the biological activity in water by feeding a solution of BrCl stabilized by a hydrohalic acid or an aqueous halide salt into the water to be treated in an amount sufficient to effect the reduction of biological activity in the water thus treated.
摘要翻译： 本发明涉及一种降低水中生物活性的方法，该方法通过将由氢卤酸或卤化水盐稳定的BrCl溶液以足以使水中生物活性降低的量加入待处理水中 治疗。
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3.发明授权公开(公告)号：US08293795B1
公开(公告)日：2012-10-23
申请号：US09451319
申请日：1999-11-30
CPC分类号： A01N59/00 , C02F1/766 , C02F2103/023 , C02F2103/28 , C02F2303/04 , G09F3/10 , A01N59/02 , A01N25/22 , A01N2300/00
摘要： A process of producing a concentrated liquid biocide formulation is described. Mixed together are (a) bromine and (b) an aqueous solution of alkali metal salt of sulfamic acid having a pH of at least about 12, in amounts such that (i) the active bromine content of the solution is at least about 100,000 ppm (wt/wt), and (ii) the atom ratio of nitrogen to active bromine from (a) and (b) is greater than 1. A continuous process for producing the concentrated liquid biocide composition is provided. This process comprises continuously feeding into mixing apparatus (i) bromine and (ii) an aqueous solution of alkali metal salt of sulfamic acid; the desired product is withdrawn from the mixing apparatus at a rate sufficient to enable the continuous feeding to be maintained. Also described are methods for disinfecting surfaces and for sanitizing bodies of water using a single-feed, bromine-based biocide. These methods use concentrated liquid biocide compositions comprising biocidally active bromine as the biocide.
摘要翻译： 描述了生产浓缩液体杀生物剂制剂的方法。 混合在一起是（a）溴和（b）具有至少约12的pH的氨基磺酸的碱金属盐的水溶液，其量使得（i）溶液的活性溴含量为至少约100,000ppm （重量/重量），和（ii）（a）和（b）的氮与活性溴的原子比大于1.提供了制备浓缩液体杀生物剂组合物的连续方法。 该方法包括连续输入混合装置（ⅰ）溴和（ⅱ）氨基磺酸的碱金属盐水溶液; 以足以使得能够维持连续进料的速率从混合装置中取出所需的产品。 还描述了使用单进料溴基杀生物剂消毒表面和消毒水体的方法。 这些方法使用包含杀生物活性溴的浓缩液体杀生物剂组合物作为杀生物剂。
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4.发明授权公开(公告)号：US06348219B1
公开(公告)日：2002-02-19
申请号：US09663788
申请日：2000-09-18
IPC分类号： A01N5902
CPC分类号： C02F1/766 , A01N59/00 , C02F2303/04 , A01N2300/00
摘要： The process involves (a) continuously forming bromine chloride from separate feed streams of bromine and chlorine by maintaining said streams under automatic feed rate control whereby the streams are continuously proportioned to come together to form bromine chloride; (b) continuously forming an aqueous product having an active bromine content of at least 100,000 ppm (wt/wt), a pH of at least 7, and an atom ratio of nitrogen to active bromine greater than 0.93:1 by continuously or intermittently feeding into mixing apparatus separate feed streams of (1) bromine chloride formed in (a), and (2) an aqueous solution of alkali metal salt of sulfamic acid, under automatic feed rate control.
摘要翻译： 该方法包括（a）通过在自动进料速率控制下将所述物流保持在连续成比例以一起形成氯化溴，从溴和氯的不同进料流中连续形成溴氯化物; （b）通过连续或间歇进料连续形成具有至少100,000ppm（wt / wt）的活性溴含量，至少7的pH以及氮与活性溴的原子比大于0.93:1的含水产物 在（a）中形成的（1）溴氯化物的进料流和（2）氨基磺酸的碱金属盐的水溶液中分离进料流，在自动进料速率控制下。
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公开(公告)号：US5175305A
公开(公告)日：1992-12-29
申请号：US743705
申请日：1991-08-12
IPC分类号： C07D209/48 , C08K5/3417
CPC分类号： C07D209/48 , C08K5/3417
摘要： This invention relates to a process for preparing and treating a product predominant in N,N'-bis(tetrabromophthalimide) so as to produce a bisimide product which has enhanced suitability for use in thermoplastic formulations as a result of reduction in volatile impurities and particle size.
摘要翻译： 本发明涉及一种制备和处理在N，N'-双（四溴邻苯二甲酰亚胺）中主要产物的方法，以便产生双酚化物产品，其由于挥发性杂质和粒度的降低而具有增强的适用于热塑性制剂的适用性 。
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6.发明授权公开(公告)号：US08048435B2
公开(公告)日：2011-11-01
申请号：US12480021
申请日：2009-06-08
CPC分类号： C02F1/766 , A01N59/00 , C02F2303/04 , G09F3/10 , A01N59/02 , A01N25/22 , A01N2300/00
摘要： A process of producing a concentrated liquid biocide formulation is described. Mixed together are (a) bromine and (b) an aqueous solution of alkali metal salt of sulfamic acid having a pH of at least about 12, in amounts such that (i) the active bromine content of the solution is at least about 100,000 ppm (wt/wt), and (ii) the atom ratio of nitrogen to active bromine from (a) and (b) is greater than 1. A continuous process for producing the concentrated liquid biocide composition is provided. This process comprises continuously feeding into mixing apparatus (i) bromine and (ii) an aqueous solution of alkali metal salt of sulfamic acid; the desired product is withdrawn from the mixing apparatus at a rate sufficient to enable the continuous feeding to be maintained. Also described are methods for disinfecting surfaces and for sanitizing bodies of water using a single-feed, bromine-based biocide. These methods use concentrated liquid biocide compositions comprising biocidally active bromine as the biocide.
摘要翻译： 描述了生产浓缩液体杀生物剂制剂的方法。 混合在一起是（a）溴和（b）具有至少约12的pH的氨基磺酸的碱金属盐的水溶液，其量使得（i）溶液的活性溴含量为至少约100,000ppm （重量/重量），和（ii）（a）和（b）的氮与活性溴的原子比大于1.提供了制备浓缩液体杀生物剂组合物的连续方法。 该方法包括连续输入混合装置（ⅰ）溴和（ⅱ）氨基磺酸的碱金属盐水溶液; 以足以使得能够维持连续进料的速率从混合装置中取出所需的产品。 还描述了使用单进料溴基杀生物剂消毒表面和消毒水体的方法。 这些方法使用包含杀生物活性溴的浓缩液体杀生物剂组合物作为杀生物剂。
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公开(公告)号：US06869620B2
公开(公告)日：2005-03-22
申请号：US10370333
申请日：2003-02-18
申请人： Robert M. Moore, Jr.
发明人： Robert M. Moore, Jr.
摘要： The production process comprises A) forming an acidic aqueous solution comprising alkali metal cations, bromide anions, and sulfamate anions; B) feeding into said aqueous solution a source of alkali metal cations and chlorine-containing bromide oxidant proportioned to keep the resultant aqueous medium acidic and to form an acidic product solution containing at least about 5 wt % of active bromine, and C) raising the pH of the aqueous product solution with water-soluble base to at least about 10.
摘要翻译： 制备方法包括：A）形成包含碱金属阳离子，溴离子和氨基磺酸根阴离子的酸性水溶液; B）向所述水溶液中加入成比例的碱金属阳离子和含氯溴化物氧化物源，以使所得水性介质保持酸性并形成含有至少约5重量％活性溴的酸性产物溶液，和C）将 具有水溶性碱的水溶液的pH至少为约10。
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公开(公告)号：US06511682B1
公开(公告)日：2003-01-28
申请号：US09506911
申请日：2000-02-18
IPC分类号： A01N3900
CPC分类号： C02F1/766 , A01N59/00 , C02F2303/04 , A01N2300/00
摘要： Described is a process of producing a concentrated liquid biocide formulation. Mixed together are (a) bromine chloride or bromine and (b) an aqueous solution of alkali metal salt of sulfamic acid having a pH of at least about 7, in amounts such that (i) the active bromine content of the solution is at least about 100,000 ppm (wt/wt), and (ii) the atom ratio of nitrogen to active bromine from (a) and (b) is greater than 1 when bromine is used and is greater than 0.93 when bromine chloride is used. Use of bromine chloride as the source of the active bromine in the process is preferred because in the resulting aqueous compositions, all of the bromine of the bromine chloride is made available as active bromine in solution. In other words, the chlorine of the bromine chloride is converted in the process to dissolved alkali metal chloride salt, thereby liberating all of the bromine in the biocidal composition as active bromine capable of providing biocidal activity.
摘要翻译： 描述了生产浓缩液体杀生物剂制剂的方法。 混合在一起是（a）溴化氯或溴，和（b）具有至少约7的pH的氨基磺酸的碱金属盐的水溶液，其量使得（i）溶液的活性溴含量至少为 大约100,000ppm（wt / wt），和（ii）当使用溴时，（a）和（b）的氮与活性溴的原子比大于1，并且当使用溴氯化物时大于0.93。 在该方法中使用溴氯化物作为活性溴的来源是优选的，因为在所得含水组合物中溴溴化物的溴全部作为活性溴在溶液中得到。 换句话说，溴化氯的氯在该过程中转化为溶解的碱金属氯化物盐，从而释放杀生物组合物中的全部溴作为能够提供杀生物活性的活性溴。
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9.发明授权
公开(公告)号：US5000879A
公开(公告)日：1991-03-19
申请号：US387776
申请日：1989-08-01
CPC分类号： C07C41/36
摘要： This invention relates to a process for increasing the melting point of partially brominated diphenyl oxide mixtures having an average bromine content of 7.2 to 7.7. The process comprises: forming a slurry comprised of C.sub.1 -C.sub.4 alkanol and the mixture; maintaining the slurry until the melting point increase which is sought is obtained; and separating the so-treated mixture from the slurry.
摘要翻译： 本发明涉及一种提高平均溴含量为7.2至7.7的部分溴化二苯醚混合物的熔点的方法。 该方法包括：形成由C1-C4链烷醇和混合物组成的浆料; 保持浆料直到获得所需的熔点增加; 并将如此处理的混合物与浆料分离。
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公开(公告)号：US08414932B2
公开(公告)日：2013-04-09
申请号：US10282290
申请日：2002-10-28
CPC分类号： A01N59/00 , C02F1/766 , C02F2303/04 , A01N59/02 , A01N25/22 , A01N2300/00
摘要： Described are highly concentrated liquid biocidal solutions formed in water from (a) specified bromine sources (e.g., BrCl or mixtures of BrCl and Br2) and (b) alkali metal salt of sulfamic acid and/or sulfamic acid and alkali metal base, wherein the solution contains >160,000 ppm of active bromine. Solutions of this type have been found to have greater stability than a commercially-available solution made from the same components containing 148,600 ppm of active bromine. Also described are new, water-soluble, solid state biocidal products formed by removing the water from solutions made in water from (a) and (b) irrespective of the initial concentration of active bromine. Removal of water can be accomplished by flashing or distillation at reduced pressure or preferably by spray drying. Such solid state products are typically in the form of powders or small particles, but can be compacted into larger forms preferably with the aid of one or more suitable binding agents.
摘要翻译： 描述了在（a）特定溴源（例如BrCl或BrCl和Br2的混合物）和（b）氨基磺酸和/或氨基磺酸和碱金属碱的碱金属盐中形成的高浓度液体杀生物溶液，其中 溶液含有> 160,000 ppm的活性溴。 已经发现这种溶液具有比由含有148,600ppm活性溴的相同成分制成的市售溶液更好的稳定性。 还描述了通过从（a）和（b）的水中制备的溶液中除去水而形成的新的水溶性固体杀生物产物，而不考虑活性溴的初始浓度。 水的除去可以通过在减压下进行闪蒸或蒸馏来完成，或优选通过喷雾干燥来完成。 这种固态产品通常是粉末或小颗粒的形式，但是可以优选地通过一种或多种合适的粘合剂的助剂压实成更大的形式。
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