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公开(公告)号：US10884155B2
公开(公告)日：2021-01-05
申请号：US16157480
申请日：2018-10-11
Applicant: PetroChina Company Limited
Inventor： Hua Tian , Shuichang Zhang , Shaobo Liu , Caineng Zou , Keyu Liu , Xuesong Lu , Mengjun Zhao , Lin Jiang , Xingzhi Ma , Bin Zhang , Junjia Fan , Peiqiang Yang
IPC: G01N24/08 , G01R33/483 , G01R33/44 , G01R33/54 , G01R33/561 , G01R33/31 , G01R33/48 , G01R33/563 , G01V3/32
Abstract: A method and an apparatus for measuring oil content of a tight reservoir based on nuclear magnetic resonance includes applying a pulse sequence to a tight reservoir rock, and after applying a first pulse and a last pulse in the pulse sequence, applying a gradient magnetic field to the tight reservoir rock, respectively, directions of the two applied gradient magnetic fields being opposite to each other, wherein the pulse sequence is composed of three 90° pulses; acquiring a nuclear magnetic resonance signal of the tight reservoir rock; and determining oil content of the tight reservoir rock according to an intensity of the nuclear magnetic resonance signal. The method can accurately distinguish an oil phase nuclear magnetic resonance signal and a water phase nuclear magnetic resonance signal in nanopores of tight reservoir rock, thereby effectively improving the accuracy of the detection result of the oil content of the tight reservoir rock.
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公开(公告)号：US10598595B2
公开(公告)日：2020-03-24
申请号：US15693380
申请日：2017-08-31
Applicant: PetroChina Company Limited
Inventor： Hua Tian , Keyu Liu , Caineng Zou , Shuichang Zhang , Shaobo Liu , Xuesong Lu , Junjia Fan , Xiuli Li , Mengjun Zhao , Qingong Zhuo , Yanjie Gong
Abstract: The invention provides a method for determining oil contents in rocks. The method comprises steps of: measuring a plurality of calibration oil samples having different oil contents, and acquiring a holographic fluorescence spectral intensity corresponding to the calibration oil samples; acquiring a fit relation between the holographic fluorescence spectral intensity and the oil contents of the calibration oil, according to the oil contents of the plurality of calibration oil samples and a plurality of three-dimensional fluorescence spectral intensities corresponding thereto; adding a certain amount of the calibration oil after dilution to rocks to be measured, acquiring a sample of the rocks to be measured and performing a holographic fluorescence measurement of the rock sample to be measured; and introducing the holographic fluorescence spectral intensity of the rock sample to be measured to the fit relation, thus an oil content of the rock sample to be measured is obtained. Accordingly, oil is detectable together with an organic solvent without volatilization of the organic solvent, which not only saves time, but also address a low-detection-limit problem for oil content resulting from volatilization of oil when the organic solvent is volatilized in the conventional method.
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公开(公告)号：US20180059022A1
公开(公告)日：2018-03-01
申请号：US15693380
申请日：2017-08-31
Applicant: PetroChina Company Limited
Inventor： Hua Tian , Keyu Liu , Xuesong Lu , Junjia Fan , Xiuli Li , Mengjun Zhao , Qingong Zhuo , Yanjie Gong
CPC classification number: G01N21/64 , G01N33/241 , G01N2021/6417 , G01N2021/6421 , G01N2201/13
Abstract: The invention provides a method for determining oil contents in rocks. The method comprises steps of: measuring a plurality of calibration oil samples having different oil contents, and acquiring a holographic fluorescence spectral intensity corresponding to the calibration oil samples; acquiring a fit relation between the holographic fluorescence spectral intensity and the oil contents of the calibration oil, according to the oil contents of the plurality of calibration oil samples and a plurality of three-dimensional fluorescence spectral intensities corresponding thereto; adding a certain amount of the calibration oil after dilution to rocks to be measured, acquiring a sample of the rocks to be measured and performing a holographic fluorescence measurement of the rock sample to be measured; and introducing the holographic fluorescence spectral intensity of the rock sample to be measured to the fit relation, thus an oil content of the rock sample to be measured is obtained. Accordingly, oil is detectable together with an organic solvent without volatilization of the organic solvent, which not only saves time, but also address a low-detection-limit problem for oil content resulting from volatilization of oil when the organic solvent is volatilized in the conventional method.
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公开(公告)号：US10533944B2
公开(公告)日：2020-01-14
申请号：US16170914
申请日：2018-10-25
Applicant: PetroChina Company Limited
Inventor： Keyu Liu , Hua Tian , Caineng Zou , Shuichang Zhang , Shaobo Liu , Mengjun Zhao , Xuesong Lu , Junjia Fan , Xiuli Li , Lili Gui , Qingong Zhuo , Xingzhi Ma , Yanjie Gong , Zhichao Yu , Qingyang Meng
Abstract: A device and method of determining thermal maturity of oil source rocks by total scanning fluorescence including testing the organic solution of the extract from a series of oil source rock samples collected at different depths by total scanning fluorescence; building a model for interpretation of the oil source rock maturity according to the variation with depth of the TSF Intensity parameter and the TSF R1 parameter obtained by total scanning fluorescence, and identifying the stage of initial oil generation, the stage of major oil generation and the stage of major gas generation; and establishing the relationship between the TSF Intensity parameter and/or the TSF R1 parameter with the existing characteristic parameters that quantitatively characterize the maturity of oil source rocks, thereby accomplishing the analysis and determination of the maturity of the oil source rocks.
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