PROCESS FOR PREPARING A CLOMAZONE, NOVEL FORM AND USE OF THE SAME

    公开(公告)号:US20190284145A1

    公开(公告)日:2019-09-19

    申请号:US16406768

    申请日:2019-05-08

    IPC分类号: C07D261/04 A01N43/80

    摘要: A process for preparing clomazone is provided, the process comprising reacting 4,4-dimethyl-3-isoxazolidinone with 2-chlorobenzyl chloride in an aqueous medium in the presence of a base, in particular an alkali metal hydroxide. A method for preparing clomazone is also disclosed, the method comprising (a) crystallizing clomazone from solution in an organic solvent; and (b) isolating the resulting crystals. N-benzene is a particularly suitable solvent. Further, there is provided Form I crystalline 2-[(2-chlorophenyl)methyl]-4,4-dimethyl-3-isoxazolidinone (clomazone), wherein the polymorph Form I is characterized by at least one of the following properties: (i) an X-ray powder diffraction pattern having characteristic peaks expressed in degrees 2θ(+/−0.20° θ) at one or more of the following positions: about 10.63, 16.07, 18.08, 19.11, 19.34, 21.20, 24.78 and 28.80; and (ii) an infrared (IR) spectrum having a characteristic peak: at about 2967 and 2870 cm−1.

    SYNERGISTIC HERBICIDAL COMPOSITION AND USE THEREOF

    公开(公告)号:US20170156332A1

    公开(公告)日:2017-06-08

    申请号:US14957853

    申请日:2015-12-03

    IPC分类号: A01N51/00 A01N47/36

    摘要: A herbicidal composition is provided, the composition comprising: (A) the crystalline modification I of 2-(4-mesyl-2-nitrobenzoyl)cyclohexane-1,3-dione (mesotrione); and (B) the crystalline modification I of methyl 2-[(4,6-dimethoxypyrimidin-2-ylcarbamoyl)sulfamoyl]-α-(methanesulfonamido)-p-toluate (mesosulfuron-methyl). A method of controlling undesirable plant growth at a locus comprises applying to the locus herbicidally effective amounts of both (A) the crystalline modification I of 2-(4-mesyl-2-nitrobenzoyl)cyclohexane-1,3-dione (mesotrione); and (B) the crystalline modification I of methyl 2-[(4,6-dimethoxypyrimidin-2-ylcarbamoyl)sulfamoyl]-α-(methanesulfonamido)-p-toluate (mesosulfuron-methyl).

    SYNERGISTIC HERBICIDAL COMPOSITION AND USE THEREOF

    公开(公告)号:US20170150721A1

    公开(公告)日:2017-06-01

    申请号:US14955220

    申请日:2015-12-01

    IPC分类号: A01N47/36 A01N41/10

    摘要: A herbicidal composition is provided, the composition comprising: (A) the crystalline modification I of 2-(4-mesyl-2-nitrobenzoyl)cyclohexane-1,3-dione (mesotrione); and (B) the crystalline modification I of methyl 2-[[[[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)methylamino]carbonyl]amino]sulfonyl]benzoate (tribenuron-methyl). A method of controlling plant growth at a locus comprises applying to the locus herbicidally effective amounts of both (A) the crystalline modification I of 2-(4-mesyl-2-nitrobenzoyl)cyclohexane-1,3-dione (mesotrione); and (B) the crystalline modification I of 2-[[[[(4-methoxy-6-methyl-1,3,5 -triazin-2-yl)methylamino]carbonyl]amino]sulfonyl]benzoate (tribenuron-methyl).

    CLOSURE ASSEMBLY FOR A CONTAINER AND A CONTAINER COMPRISING THE SAME
    7.
    发明申请
    CLOSURE ASSEMBLY FOR A CONTAINER AND A CONTAINER COMPRISING THE SAME 审中-公开
    用于集装箱和包含该容器的集装箱的封闭装置

    公开(公告)号:US20160264314A1

    公开(公告)日:2016-09-15

    申请号:US15030822

    申请日:2014-10-13

    摘要: A closure assembly for a container is provided, the closure assembly comprising: a closure body for securing to the container to extend across and seal an opening in the container; the closure body comprising a bore therein, the bore communicating with the opening in the container and providing a conduit between the interior of the container and the exterior of the container through which product within the container may be dispensed; a closure member having a port therein, the closure member slideably mounted to the closure body and slideable between a closed position in which the port is out of alignment with the bore in the closure body and the closure member acts to close the bore in the closure member and an open position in which the port is aligned with the bore in the closure body. A measuring vessel for use with the closure assembly is also provided.

    摘要翻译: 提供了一种用于容器的封闭组件,封闭组件包括:封闭体,用于固定到容器以延伸并密封容器中的开口; 所述封闭主体包括其中的孔,所述孔与所述容器中的开口连通并且在所述容器的内部和所述容器的外部之间提供导管,所述容器内的产品可以通过所述导管分配; 封闭构件,其中具有端口,所述封闭构件可滑动地安装到所述封闭件主体并可在关闭位置之间滑动,在所述闭合位置中,所述端口与所述封闭件主体中的所述孔不对齐,并且所述封闭构件用于封闭所述封闭件 构件和打开位置,其中端口与封闭体中的孔对齐。 还提供了用于封闭组件的测量容器。

    PROCESS FOR PREPARING A NOVEL FORMULATION OF RIMSULFURON AND USE OF THE SAME
    8.
    发明申请
    PROCESS FOR PREPARING A NOVEL FORMULATION OF RIMSULFURON AND USE OF THE SAME 有权
    制备RIMSULFURON的新方法及其使用的方法

    公开(公告)号:US20160235066A1

    公开(公告)日:2016-08-18

    申请号:US14620477

    申请日:2015-02-12

    IPC分类号: A01N43/80 A01N47/36

    CPC分类号: A01N47/36 A01N25/22 A01N43/80

    摘要: A herbicidal composition including rimsulfuron with anti-hydrolysis agent, wherein the anti-hydrolysis agent is 2-isoxazoline-3-carboxylic acid derivatives having formula (I): in which R1 is phenyl which is unsubstituted or substituted, R2 is (C1-C6)alkyl, (C3-C6)cycloalkyl or phenyl, each of the 3 last-mentioned radicals is unsubstituted or substituted, R3 is hydrogen or a hydrocarbon radical having 1 to 18 C atoms which is unsubstituted or substituted. A method for controlling weeds, including applying to a plant, plant part, or locus thereof, an effective amount of the herbicidal composition. A method for imparting hydrolysis resistance to a herbicidal composition containing rimsulfuron by adding to the composition an effective amount of the compound of formula (I).

    摘要翻译: 一种除草组合物,其包含含有抗水解剂的嘧磺隆,其中所述抗水解剂是具有式(I)的2-异恶唑啉-3-羧酸衍生物:其中R1是未取代或取代的苯基,R2是(C1-C6 )烷基,(C 3 -C 6)环烷基或苯基,3个最后提及的基团中的每一个是未取代的或取代的,R 3是氢或具有未取代或取代的1至18个C原子的烃基。 一种控制杂草的方法,包括施用于植物,植物部分或其所在地,有效量的除草组合物。 通过向组合物中加入有效量的式(I)化合物,赋予含有噻嘧磺隆的除草组合物具有耐水解性的方法。

    A NOVEL AQUEOUS SUSPOEMULSION AND A PROCESS FOR PREPARING THE SAME
    10.
    发明申请
    A NOVEL AQUEOUS SUSPOEMULSION AND A PROCESS FOR PREPARING THE SAME 审中-公开
    一种新型水性硫化物及其制备方法

    公开(公告)号:US20160198703A1

    公开(公告)日:2016-07-14

    申请号:US14913244

    申请日:2014-06-19

    IPC分类号: A01N25/04 A01N53/00 A01N51/00

    CPC分类号: A01N25/04 A01N51/00 A01N53/00

    摘要: An aqueous suspoemulsion (SE) comprising:a dispersed oil phase of Component (a), comprising: (i) lambda-cyhalothrin as the first active ingredient; (ii) at least one solvent having lambda-cyhalothrin dissolved therein; a continuous water phase of Component (b), comprising: (i) imidacloprid as the second active ingredient; and (ii) water having imidacloprid suspended therein; and optionally at least one additive is provided. A process for preparing an aqueous suspoemulsion comprising: Step 1: Preparing lambda-cyhalothrin EC phase by mixing the active ingredient with a suitable solvent; Step 2: Preparing a dispersion of imidacloprid in a continuous water phase by mixing the active ingredient, a dispersant and a required amount of water; and Step 3: Combining the EC phase in Step 1 with the water phase in Step 2.

    摘要翻译: 一种水性悬乳剂(SE),其包含:组分(a)的分散油相,其包含:(i)λ-三氟氯氰菊酯作为第一活性成分; (ii)至少一种溶解有λ-氯氟氰菊酯的溶剂; 组分(b)的连续水相,其包含:(i)吡虫啉作为第二活性成分; 和(ii)其中悬浮有吡虫啉的水; 并且可选地提供至少一种添加剂。 一种制备含水悬液乳液的方法,包括:步骤1:通过将活性成分与合适的溶剂混合来制备λ-氯氟氰菊酯EC相; 步骤2:通过混合活性成分,分散剂和所需量的水,在连续水相中制备吡虫啉的分散体; 步骤3:将步骤1中的EC相与步骤2中的水相合并。