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公开(公告)号：US20150291744A1
公开(公告)日：2015-10-15
申请号：US14443485
申请日：2013-07-16
发明人： Jin Ryul Son , Kil Seuk Byun
摘要： Provided is a hard capsule. The provided hard capsule includes water-soluble cellulose ether, about 0.5 parts by weight to about 1.5 parts by weight of a gelation agent based on 100 parts by weight of the water-soluble cellulose ether, and about 0 parts by weight to about 0.3 parts by weight of a gelation aid based on 100 parts by weight of the water-soluble cellulose ether, wherein the hard capsule comprises a body and a cap that seals the body, and a ratio of a maximum thickness to a minimum thickness of the body and the cap is each 2.5 or less.
摘要翻译： 提供了一个硬胶囊。 所提供的硬胶囊包括水溶性纤维素醚，基于100重量份水溶性纤维素醚约0.5重量份至约1.5重量份的凝胶剂，以及约0重量份至约0.3重量份 的基于100重量份的水溶性纤维素醚的凝胶助剂，其中所述硬胶囊包括主体和密封所述身体的帽，以及所述身体的最大厚度与最小厚度的比率，以及 盖每个2.5或更小。
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公开(公告)号：US20150252142A1
公开(公告)日：2015-09-10
申请号：US14423293
申请日：2013-05-20
发明人： Gyung Don Kang , Ki Chull Yun , Sang Yob Kim , Jung Ryum , Boo Seong Kim , Kil Seuk Byun , Sei Hoon Kim , Sung Bae Park
IPC分类号： C08G63/16
摘要： Provided is a method of continuous production of a biodegradable aliphatic polyester including continuously performing an esterification reaction of a mixture including an aliphatic dihydroxy compound and aliphatic dicarboxylic acid at a temperature of 185° C. or less to obtain an ester; continuously performing a first polycondensation reaction of the ester to obtain a preliminary polymer; and continuously performing a polycondensation reaction of the preliminary polymer. According to the method of production, an amount of the aliphatic dihydroxy compound used decreases, which is a starting material, thereby decreasing the manufacturing cost of the biodegradable aliphatic polyester.
摘要翻译： 提供连续制造生物降解性脂肪族聚酯的方法，包括在185℃以下的温度下连续进行包含脂肪族二羟基化合物和脂肪族二羧酸的混合物的酯化反应，得到酯; 连续进行酯的第一缩聚反应得到预聚合物; 并连续进行预聚合物的缩聚反应。 根据生产方法，使用的脂肪族二羟基化合物的量是起始原料，从而降低可生物降解的脂肪族聚酯的制造成本。
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3.发明申请METHOD FOR CONTINUOUSLY PREPARING BIODEGRADABLE ALIPHATIC/AROMATIC POLYESTER COPOYMER 有权连续制备生物可降解脂肪/芳族聚酯复合体的方法公开(公告)号：US20150183927A1
公开(公告)日：2015-07-02
申请号：US14423641
申请日：2013-05-20
发明人： Gyung Don Kang , Ki Chull Yun , Sang Yob Kim , Kil Seuk Byun , Jung Ryum , Boo Seong Kim , Sei Hoon Kim , Sung Bae Park
IPC分类号： C08G63/78
CPC分类号： C08G63/78 , C08G63/181 , C08G2230/00
摘要： Provided is a method of continuous preparation of a biodegradable aliphatic/aromatic polyester copolymer, the method including: performing a first esterification reaction of an aliphatic dihydroxy compound and an aliphatic dicarboxylic acid at a temperature of 185° C. or less; continuously performing a second esterification reaction of a reaction product obtained by the first esterification reaction; obtaining a pre-polymer by continuously performing a first polycondensation reaction of a reaction product obtained by the second esterification reaction; and continuously performing polycondensation reaction of the pre-polymer, wherein an aromatic carboxylic acid is added to a reactor in which the first esterification reaction or the second esterification reaction is performed, to prepare the biodegradable aliphatic/aromatic polyester copolymer. According to the method of continuous preparation of the biodegradable aliphatic/aromatic polyester copolymer as described above, the amount of the aliphatic dihydroxy compound used, which is a starting material, is reduced and accordingly, manufacturing costs are reduced.
摘要翻译： 提供一种生物降解性脂肪族/芳香族聚酯共聚物的连续制备方法，其特征在于，在185℃以下的温度下进行脂肪族二羟基化合物和脂肪族二羧酸的酯化反应， 连续进行通过第一酯化反应得到的反应产物的第二次酯化反应; 通过连续进行通过第二酯化反应获得的反应产物的第一缩聚反应获得预聚物; 并连续地进行预聚物的缩聚反应，其中在进行第一酯化反应或第二酯化反应的反应器中加入芳族羧酸，以制备可生物降解的脂族/芳族聚酯共聚物。 根据上述生物降解性脂肪族/芳香族聚酯共聚物的连续制备方法，作为起始原料的脂肪族二羟基化合物的使用量减少，因此制造成本降低。
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公开(公告)号：US10793687B2
公开(公告)日：2020-10-06
申请号：US14443485
申请日：2013-07-16
发明人： Jin Ryul Son , Kil Seuk Byun
摘要： Provided is a hard capsule. The provided hard capsule includes water-soluble cellulose ether, about 0.5 parts by weight to about 1.5 parts by weight of a gelation agent based on 100 parts by weight of the water-soluble cellulose ether, and about 0 parts by weight to about 0.3 parts by weight of a gelation aid based on 100 parts by weight of the water-soluble cellulose ether, wherein the hard capsule comprises a body and a cap that seals the body, and a ratio of a maximum thickness to a minimum thickness of the body and the cap is each 2.5 or less.
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5.发明授权Method for continuously preparing biodegradable aliphatic/aromatic polyester copolymer 有权连续制备生物降解脂肪/芳族聚酯共聚物的方法公开(公告)号：US09334359B2
公开(公告)日：2016-05-10
申请号：US14423293
申请日：2013-05-20
发明人： Gyung Don Kang , Ki Chull Yun , Sang Yob Kim , Jung Ryum , Boo Seong Kim , Kil Seuk Byun , Sei Hoon Kim , Sung Bae Park
摘要： Provided is a method of continuous production of a biodegradable aliphatic polyester including continuously performing an esterification reaction of a mixture including an aliphatic dihydroxy compound and aliphatic dicarboxylic acid at a temperature of 185° C. or less to obtain an ester; continuously performing a first polycondensation reaction of the ester to obtain a preliminary polymer; and continuously performing a polycondensation reaction of the preliminary polymer. According to the method of production, an amount of the aliphatic dihydroxy compound used decreases, which is a starting material, thereby decreasing the manufacturing cost of the biodegradable aliphatic polyester.
摘要翻译： 提供连续制造生物降解性脂肪族聚酯的方法，包括在185℃以下的温度下连续进行包含脂肪族二羟基化合物和脂肪族二羧酸的混合物的酯化反应，得到酯; 连续进行酯的第一缩聚反应得到预聚合物; 并连续进行预聚合物的缩聚反应。 根据生产方法，使用的脂肪族二羟基化合物的量是起始原料，从而降低可生物降解的脂肪族聚酯的制造成本。
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