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    PROCESS FOR OLIGOMERIZATION OF ETHYLENE
    1.
    发明申请
    PROCESS FOR OLIGOMERIZATION OF ETHYLENE 审中-公开
    乙烯低聚方法

    公开(公告)号：US20150299069A1

    公开(公告)日：2015-10-22

    申请号：US14125805

    申请日：2013-09-05

    Applicant: Saudi Basic Industries Corporation ,  Linde AG

    Inventor： Shahid Majeed Azam ,  Abduljelil Iliyas ,  Abdullah Mohammad Alqahtani ,  Shehzada Khurram ,  Anina Wöhl ,  Wolfgang Müller ,  Marco Harff ,  Andreas Meiswinkel ,  Heinz Bölt

    IPC: C07C2/34

    CPC classification number: C07C2/34 ,  C07C2/36 ,  C07C2531/18 ,  C07C2531/20 ,  C07C2531/22 ,  C07C2531/34 ,  C07C11/107

    Abstract: The present invention relates to a process for the oligomerization of ethylene, comprising: a) oligomerizing of ethylene in a reactor in the presence of solvent and catalyst; b) transferring reactor overhead effluent to an externally located cooling device and recycling condensed effluent into the reactor; c) transferring the reactor bottom effluent to a series of fractionation columns and, in the following order, i) optionally separating C4 fraction, ii) separating C6 fraction, iii) simultaneously separating C8 and C10 fractions and recycling thereof into the reac-tor, and iv) separating residues comprising ≧C12 fractions, spent catalyst, polymer material and quench media, from the process, wherein the solvent is separated in any of the steps i)-iv) and/or in an additional step.

    Abstract translation: 本发明涉及乙烯低聚方法，包括：a）在溶剂和催化剂存在下，在反应器中使乙烯低聚; b）将反应器塔顶流出物转移到外部定位的冷却装置，并将冷凝的流出物再循环到反应器中; c）将反应器底部流出物转移到一系列分馏塔中，并且按照以下顺序，i）任选地分离C4级分，ii）分离C6级分，iii）同时分离C8和C10级分并将其再循环到反应器中， 以及iv）从所述方法分离包含≥12c部分的残留物，废催化剂，聚合物材料和骤冷介质，其中所述溶剂在步骤i）-iv）和/或另外的步骤中分离。

    METHOD FOR PURIFYING A CRUDE PNPNH COMPOUND
    2.
    发明申请
    METHOD FOR PURIFYING A CRUDE PNPNH COMPOUND 有权
    净化PNPNH化合物的方法

    公开(公告)号：US20140228594A1

    公开(公告)日：2014-08-14

    申请号：US14176609

    申请日：2014-02-10

    Applicant: LINDE AG ,  SAUDI BASIC INDUSTRIES CORPORATION

    Inventor： Uwe Rosenthal ,  Bernd H. Müller ,  Normen Peulecke ,  Marco Harff ,  Anina Wöhl ,  Andreas Meiswinkel ,  Heinz Bölt ,  Wolfgang Müller ,  Abdullah Mohammad Al-Qahtani ,  Mohammed H. Al-Hazmi ,  Shahid Majeed Azam

    IPC: C07F9/50

    CPC classification number: C07F9/5095 ,  B01J31/143 ,  B01J31/189 ,  B01J2231/20 ,  B01J2531/62

    Abstract: A method for purifying a crude PNPNH compound of the general structure R1R2P—N(R3)—P(R4)—N(R5)—H wherein R1, R2, R3, R4 and R5 are independently halogen, amino, trimethylsilyl, C1-C10-alkyl, substituted C1-C10-alkyl, C6-C20-aryl and substituted C6-C20-aryl, or any cyclic derivative wherein at least one of the P or N atoms of the PNPN—H structure is a member of a ring system, the ring system being formed from one or more constituent compounds of the PNPNH-structure by substitution, the method comprising the steps: A. a) dissolving the crude PNPNH-compound in a C1-C10 alcohol or mixture thereof under heating; b) cooling the solution obtained in step a), c) precipitating the PNPNH compound, separating and optionally drying, or B. (i) washing the crude PNPNH compound with C1-C10 alcohol or a mixture thereof, (ii) separating the PNPNH compound and optionally drying thereof.

    Abstract translation: 纯化通式为R 1 R 2 P -N（R 3）-P（R 4）-N（R 5）-H）的粗PNPNH化合物的方法，其中R1，R2，R3，R4和R5独立地为卤素，氨基，三甲基甲硅烷基，C1- C 10 - 烷基，取代的C 1 -C 10 - 烷基，C 6 -C 20 - 芳基和取代的C 6 -C 20 - 芳基，或任何环状衍生物，其中PNPN-H结构的P或N原子中的至少一个是环的成员 该系统由一种或多种通过取代的PNPNH结构的组成化合物形成，所述方法包括以下步骤：a）a）将粗PNPNH化合物在加热下溶解在C1-C10醇或其混合物中; b）冷却步骤a）中获得的溶液，c）沉淀PNPNH化合物，分离并任选地干燥或B.（i）用C1-C10醇或其混合物洗涤粗PNPNH化合物，（ii）将PNPNH 化合物和任选地干燥。

    Method for purifying a crude PNPNH compound
    6.
    发明授权
    Method for purifying a crude PNPNH compound 有权
    纯化粗PNPNH化合物的方法

    公开(公告)号：US09206207B2

    公开(公告)日：2015-12-08

    申请号：US14176609

    申请日：2014-02-10

    Applicant: SAUDI BASIC INDUSTRIES CORPORATION ,  LINDE AG

    Inventor： Uwe Rosenthal ,  Bernd H. Müller ,  Normen Peulecke ,  Marco Harff ,  Anina Wöhl ,  Andreas Meiswinkel ,  Heinz Bölt ,  Wolfgang Müller ,  Abdullah Mohammad Al-Qahtani ,  Mohammed H. Al-Hazmi ,  Shahid Majeed Azam

    IPC: C07F9/50 ,  B01J31/14 ,  B01J31/18

    CPC classification number: C07F9/5095 ,  B01J31/143 ,  B01J31/189 ,  B01J2231/20 ,  B01J2531/62

    Abstract: A method for purifying a crude PNPNH compound of the general structure R1R2P—N(R3)—P(R4)—N(R5)—H wherein R1, R2, R3, R4 and R5 are independently halogen, amino, trimethylsilyl, C1-C10-alkyl, substituted C1-C10-alkyl, C6-C20-aryl and substituted C6-C20-aryl, or any cyclic derivative wherein at least one of the P or N atoms of the PNPN—H structure is a member of a ring system, the ring system being formed from one or more constituent compounds of the PNPNH-structure by substitution, the method comprising the steps: A. a) dissolving the crude PNPNH-compound in a C1-C10 alcohol or mixture thereof under heating; b) cooling the solution obtained in step a), c) precipitating the PNPNH compound, separating and optionally drying, or B. (i) washing the crude PNPNH compound with C1-C10 alcohol or a mixture thereof, (ii) separating the PNPNH compound and optionally drying thereof.

    Abstract translation: 纯化通式为R 1 R 2 P -N（R 3）-P（R 4）-N（R 5）-H）的粗PNPNH化合物的方法，其中R1，R2，R3，R4和R5独立地为卤素，氨基，三甲基甲硅烷基，C1- C 10 - 烷基，取代的C 1 -C 10 - 烷基，C 6 -C 20 - 芳基和取代的C 6 -C 20 - 芳基，或任何环状衍生物，其中PNPN-H结构的P或N原子中的至少一个是环的成员 该系统由一种或多种通过取代的PNPNH结构的组成化合物形成，所述方法包括以下步骤：a）a）将粗PNPNH化合物在加热下溶解在C1-C10醇或其混合物中; b）冷却步骤a）中获得的溶液，c）沉淀PNPNH化合物，分离并任选地干燥或B.（i）用C1-C10醇或其混合物洗涤粗PNPNH化合物，（ii）将PNPNH 化合物和任选地干燥。

    Method for removal and recovery of organic amines from a hydrocarbon stream
    7.
    发明授权
    Method for removal and recovery of organic amines from a hydrocarbon stream 有权
    从烃流中去除和回收有机胺的方法

    公开(公告)号：US08809611B2

    公开(公告)日：2014-08-19

    申请号：US14070039

    申请日：2013-11-01

    Applicant: Saudi Basic Industries Corporation

    Inventor： Fuad M. Mosa ,  Shahid Majeed Azam ,  Sultan Eid Al-Otaibi

    IPC: C07C7/00 ,  C07C209/86

    CPC classification number: C07C209/86 ,  C07C7/17 ,  C07C7/171 ,  C10G17/02 ,  C10G50/00 ,  C10G57/02 ,  C10G2300/202 ,  C07C11/02

    Abstract: A method for removal and recovery of an organic amine from a hydrocarbon stream containing the amine, including: i) mixing the hydrocarbon stream containing the amine with an aqueous inorganic acid in a volumetric ratio of hydrocarbon stream:aqueous inorganic acid of greater than 1:1-5:1, preferably 1.5:1-4:1, more preferably 3:1, ii) phase separating of hydrocarbon and aqueous phase; iii) removing the hydrocarbon phase and optionally further purifying thereof, iv) optionally recycling at least a part of the hydrocarbon phase obtained in step (iii) into mixing step (i), v) mixing the aqueous phase obtained in step (iii) with an aqueous alkaline solution, vi) phase separating of an aqueous phase and an organic phase formed, vii) removing the organic phase obtained in step (vi) and optionally further purifying thereof.

    Abstract translation: 一种从含有胺的烃流中除去和回收有机胺的方法，包括：i）将含有胺的烃流与含水无机酸的烃流：含水无机酸的体积比大于1： 1-5：1，优选1.5：1-4：1，更优选3：1，ii）烃和水相的相分离; iii）除去烃相并任选地进一步纯化，iv）任选地将步骤（iii）中获得的烃相的至少一部分再循环到混合步骤（ⅰ）中，v）将步骤（iii）中获得的水相与 水性碱性溶液，vi）水相和形成的有机相的相分离，vii）除去步骤（vi）中获得的有机相，并任选进一步纯化。

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