Abstract:
A method of manufacturing a solid electrolytic capacitor including a porous anode body made of a valve metal having a dielectric film on a surface thereof, and a solid electrolyte layer disposed on a surface of the dielectric film. The method including: a step of; in a liquid including a polyanion and an aqueous medium, polymerizing a monomer compound to obtain a dispersion (1) containing a conjugated electrically conductive polymer and subjecting dispersion treatment to the dispersion (1) to obtain a dispersion (2) containing the conjugated electrically conductive polymer; depositing the dispersion (2) to a porous anode body made of a valve metal having a dielectric coating on a surface thereof; and removing the aqueous medium from the dispersion (2) deposited on the porous anode body to form a solid electrolyte layer, wherein an operation which pauses the dispersion treatment is performed.
Abstract:
A method for manufacturing a solid electrolytic capacitor, which includes the steps of: in a dispersion medium containing a monomer for obtaining a conjugated conductive polymer and a seed particle with protective colloid formed of a polyanion, polymerizing the monomer to obtain a conjugated conductive polymer-containing dispersion liquid; attaching the conjugated conductive polymer-containing dispersion liquid to the surface of a porous anode body at least having an anode body made of a valve metal and a dielectric film formed on the surface of the anode body; and removing a part or all of the dispersion medium from the conjugated conductive polymer-containing dispersion liquid attached to the porous anode body to form a solid electrolyte layer. Also disclosed is a solid electrolytic capacitor obtained by the method.
Abstract:
A method for producing a conductive polymer-containing dispersion, the method including a polymerization step of subjecting a monomer that is to be a constitutional unit of a conjugated conductive polymer to a polymerization reaction in a mixed solution containing the monomer, a polyanion, and a dispersion medium to produce a polymerized product; and a dispersion treatment step of performing a dispersion treatment on a reaction solution obtained in the polymerization step to prepare a dispersion of the polymerized product, wherein a dispersion medium is added one or more times at any point in time from after the polymerization step to during the dispersion treatment step to make a mass concentration (B) of the polymerized product in the dispersion after the dispersion treatment step lower than a mass concentration (A) of the polymerized product in the reaction solution.
Abstract:
The present invention provides a method for producing a conductive polymer-containing dispersion, including: a polymerization step of polymerizing a monomer for obtaining a conjugated conductive polymer in a dispersion medium including the monomer and seed particles converted into a protective colloid by a polyanion.