METHOD OF PREPARING ORGANOSULFUR COMPOUND
    2.
    发明公开

    公开(公告)号:US20230391743A1

    公开(公告)日:2023-12-07

    申请号:US18034025

    申请日:2020-12-18

    CPC classification number: C07D327/10 B01J27/13

    Abstract: The present invention relates to a method of preparing an organosulfur compound, and more particularly, to a method of preparing an organosulfur compound including a step of synthesizing an organosulfur compound by reacting specific compounds with a metal hypohalite under a ruthenium catalyst in a mixed solvent containing water and an organic solvent, wherein the metal hypohalite is introduced in a solid state and a portion thereof reacts in an undissolved state. According to the present invention, the present invention has an effect of providing an organosulfur compound preparation method capable of preparing an organosulfur compound in high yield due to excellent reaction stability, short reaction time, and reduced side reactions.

    METHOD OF PREPARING ORGANOSULFUR COMPOUND
    4.
    发明公开

    公开(公告)号:US20230391793A1

    公开(公告)日:2023-12-07

    申请号:US18034022

    申请日:2020-12-18

    CPC classification number: C07D497/10 C07D327/10 B01J23/462

    Abstract: The present invention relates to a method of preparing an organosulfur compound, and more particularly, to a method of preparing an organosulfur compound including a step of synthesizing an organosulfur compound by reacting specific compounds with a metal hypohalite under a ruthenium catalyst in a mixed solvent containing water and an organic solvent, wherein reaction temperature during the synthesis is 0 to 25° C. According to the present invention, the present invention has an effect of providing an organosulfur compound preparation method capable of preparing an organosulfur compound in high yield due to excellent reaction stability, short reaction time, and reduced side reactions.

    METHOD OF PREPARING CYCLIC PHOSPHINE COMPOUND

    公开(公告)号:US20240409567A1

    公开(公告)日:2024-12-12

    申请号:US18704097

    申请日:2022-10-18

    Abstract: The present invention relates to a method of preparing a symmetric or asymmetric cyclic phosphine compound, the method including a step of reacting a cyclic phosphine compound with an organic halogen compound under a predetermined coupling agent. The present invention provides a method of preparing a symmetric or asymmetric cyclic phosphine compound that uses cheaper compounds compared to a conventional method, has excellent economics by stably storing reaction raw materials, improves productivity and yield due to easy reaction control and low generation of by-products, is easily applied on an industrial scale, and has excellent expandability or substitutivity of a synthetic route.

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