METHOD FOR MANUFACTURING NICKEL POWDER, AND METHOD FOR OPERATING REACTION FACILITY

    公开(公告)号:US20180257143A1

    公开(公告)日:2018-09-13

    申请号:US15759356

    申请日:2016-07-11

    IPC分类号: B22F9/24 C22B3/00 C22B3/06

    摘要: A method for manufacturing nickel powder whereby a reduction in production efficiency due to abrasion of a flash vessel connected to a pressurized container can be suppressed when nickel powder is generated using the pressurized container and subsequently recovered. The method for manufacturing nickel powder comprises charging a pressurized container with a nickel sulfate ammine complex solution and seed crystals, adding hydrogen gas to the pressurized container, and reducing the nickel included in the nickel sulfate ammine complex solution, wherein, when a nickel powder slurry obtained in the pressurized container is extracted to a flash vessel connected to the pressurized container, the slurry is extracted to the flash vessel while the supply rate of the nickel ammine complex solution to the pressurized container and/or the extraction rate of the nickel slurry from the pressurized container is controlled so the liquid level in the pressurized container is in a fixed range.

    Method for recovering scandium
    4.
    发明授权

    公开(公告)号:US10156002B2

    公开(公告)日:2018-12-18

    申请号:US15546038

    申请日:2015-12-08

    摘要: Provided is a method for recovering scandium with which scandium can be efficiently recovered as high purity scandium oxide from a scandium-containing solution containing impurities such as iron without causing problems such as increased cost and safety problems. According to the method for recovering scandium according to the present invention, the pH of a solution containing scandium and iron (scandium-containing solution) is adjusted within the range of not less than −0.5 and less than 1, then scandium oxalate is obtained by adding the pH adjusted solution to an oxalic acid solution, and the scandium oxalate is roasted into scandium oxide.