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    Mesoporous carbon, method of preparing the same, and fuel cell using the carbon
    1.
    发明授权
    Mesoporous carbon, method of preparing the same, and fuel cell using the carbon 有权
    介孔碳，其制备方法和使用碳的燃料电池

    公开(公告)号：US07854913B2

    公开(公告)日：2010-12-21

    申请号：US11443160

    申请日：2006-05-31

    申请人： Sang-hoon Joo ,  Chan-ho Pak ,  Hyuk Chang ,  Ji-man Kim ,  Hyung-ik Lee

    发明人： Sang-hoon Joo ,  Chan-ho Pak ,  Hyuk Chang ,  Ji-man Kim ,  Hyung-ik Lee

    IPC分类号： B01J19/08 ,  H01M8/00

    CPC分类号： H01M4/926 ,  B82Y30/00 ,  C01B32/00

    摘要： A mesoporous carbon is prepared by mixing a carbon precursor, an acid, and a solvent to obtain a carbon precursor mixture; impregnating an ordered mesoporous silica (OMS) with the carbon precursor mixture; carbonizing the impregnated OMS at 800 to 1300° C. by irradiating microwave energy with a power of 100 to 2000 W thereon to form an OMS-carbon composite; and removing the mesoporous silica from the OMS-carbon composite. The method of preparing a mesoporous carbon can significantly reduce a carbonization time by carbonizing a carbon precursor using microwave energy in a silica template compared to a conventional method using a heat treatment. A supported catalyst and a fuel cell include the mesoporous carbon.

    摘要翻译： 通过混合碳前体，酸和溶剂来制备介孔碳以获得碳前体混合物; 用碳前体混合物浸渍有序介孔二氧化硅（OMS）; 通过在其上照射100至2000W的功率的微波能量来在800至1300℃下将浸渍的OMS碳化，以形成OMS-碳复合材料; 并从OMS-碳复合材料中除去介孔二氧化硅。 制备介孔碳的方法与使用热处理的常规方法相比，通过使用微波能量在二氧化硅模板中碳化碳前体可显着降低碳化时间。 载体催化剂和燃料电池包括介孔碳。

    Sulfur-containing mesoporous carbon, method of manufacturing the same, and fuel cell using the mesoporous carbon
    3.
    发明授权
    Sulfur-containing mesoporous carbon, method of manufacturing the same, and fuel cell using the mesoporous carbon 有权
    含硫介孔碳，其制造方法以及使用介孔碳的燃料电池

    公开(公告)号：US07867941B2

    公开(公告)日：2011-01-11

    申请号：US11966266

    申请日：2007-12-28

    申请人： Sang Hoon Joo ,  Chan-ho Pak ,  Hyuk Chang ,  Ji-man Kim ,  Hyung-ik Lee

    发明人： Sang Hoon Joo ,  Chan-ho Pak ,  Hyuk Chang ,  Ji-man Kim ,  Hyung-ik Lee

    IPC分类号： B01J21/18 ,  C01B31/00 ,  H01M4/64

    CPC分类号： B01J37/0018 ,  B01J21/18 ,  B01J35/1061 ,  B01J37/084 ,  C01B32/00 ,  H01M4/92 ,  H01M4/926 ,  H01M8/1011 ,  Y02E60/523 ,  Y02P70/56

    摘要： A sulfur-containing mesoporous carbon that has mesopores with an average diameter of 2 to 10 nm, a method of preparing the same, a catalyst containing the mesoporous carbon as a catalyst support, and a fuel cell using the catalyst in which the sulfur-containing mesoporous carbon has a good affinity for and adhesion to catalyst particles so as to strongly support the catalyst particles due to the sulfur atoms substituting for carbons in an OMC carbon skeleton structure. The growth of metal catalyst particles is prevented when heat-treating the metal catalyst particles. The catalyst using the sulfur-containing mesoporous carbon can be applied to a fuel cell to prevent a reduction in catalytic activity due to increased particle size by an accumulation of catalyst particles. The catalyst containing the sulfur-containing mesoporous carbon as a catalyst support can be used to manufacture a fuel cell having an improved performance.

    摘要翻译： 具有平均直径为2〜10nm的介孔的含硫中孔碳，其制备方法，含有介孔碳作为催化剂载体的催化剂，以及使用该催化剂的燃料电池，其中，含硫 中孔碳对催化剂颗粒具有良好的亲和性和粘附性，从而由于在OMC碳骨架结构中用硫原子代替碳而强烈地支持催化剂颗粒。 当对金属催化剂颗粒进行热处理时，可防止金属催化剂颗粒的生长。 使用含硫介孔碳的催化剂可以应用于燃料电池，以防止由于催化剂颗粒的积聚引起的粒度增加导致的催化活性降低。 含有含硫介孔碳作为催化剂载体的催化剂可用于制造具有改进性能的燃料电池。

    Mesoporous carbon, method of preparing the same, and fuel cell using the carbon
    6.
    发明申请
    Mesoporous carbon, method of preparing the same, and fuel cell using the carbon 有权
    介孔碳，其制备方法和使用碳的燃料电池

    公开(公告)号：US20070116624A1

    公开(公告)日：2007-05-24

    申请号：US11443160

    申请日：2006-05-31

    申请人： Sang-hoon Joo ,  Chan-ho Pak ,  Hyuk Chang ,  Ji-man Kim ,  Hyung-ik Lee

    发明人： Sang-hoon Joo ,  Chan-ho Pak ,  Hyuk Chang ,  Ji-man Kim ,  Hyung-ik Lee

    IPC分类号： C01B31/02 ,  H01M4/96

    CPC分类号： H01M4/926 ,  B82Y30/00 ,  C01B32/00

    摘要： A mesoporous carbon is prepared by mixing a carbon precursor, an acid, and a solvent to obtain a carbon precursor mixture; impregnating an ordered mesoporous silica (OMS) with the carbon precursor mixture; carbonizing the impregnated OMS at 800 to 1300° C. by irradiating microwave energy with a power of 100 to 2000 W thereon to form an OMS-carbon composite; and removing the mesoporous silica from the OMS-carbon composite. The method of preparing a mesoporous carbon can significantly reduce a carbonization time by carbonizing a carbon precursor using microwave energy in a silica template compared to a conventional method using a heat treatment. A supported catalyst and a fuel cell include the mesoporous carbon.

    摘要翻译： 通过混合碳前体，酸和溶剂来制备介孔碳以获得碳前体混合物; 用碳前体混合物浸渍有序介孔二氧化硅（OMS）; 通过在其上照射100至2000W的功率的微波能量来在800至1300℃下将浸渍的OMS碳化，以形成OMS-碳复合材料; 并从OMS-碳复合材料中除去介孔二氧化硅。 制备介孔碳的方法与使用热处理的常规方法相比，通过使用微波能量在二氧化硅模板中碳化碳前体可显着降低碳化时间。 载体催化剂和燃料电池包括介孔碳。

    HETEROATOM-CONTAINING MESOPOROUS CARBON, METHOD OF PREPARING THE SAME, AND FUEL CELL USING THE HETEROATOM-CONTAINING MESOPOROUS CARBON
    8.
    发明申请
    HETEROATOM-CONTAINING MESOPOROUS CARBON, METHOD OF PREPARING THE SAME, AND FUEL CELL USING THE HETEROATOM-CONTAINING MESOPOROUS CARBON 审中-公开
    含异构体的多孔碳，其制备方法和使用含有异质多孔碳的燃料电池

    公开(公告)号：US20090239115A1

    公开(公告)日：2009-09-24

    申请号：US12258828

    申请日：2008-10-27

    申请人： Chan-ho Pak ,  Hyuk Chang ,  Ji-man Kim ,  Hyung-Ik Lee

    发明人： Chan-ho Pak ,  Hyuk Chang ,  Ji-man Kim ,  Hyung-Ik Lee

    IPC分类号： H01M8/10 ,  B32B9/00

    CPC分类号： H01M4/926 ,  C01B32/00 ,  H01M4/9083

    摘要： A heteroatom-containing mesoporous carbon has a pore diameter of 11 to 35 nm, has a specific surface area of 500 m2/g or more, and comprises a heteroatom. The heteroatom-containing mesoporous carbon is formed by a method including mixing a carbon precursor, a heteroatom-containing precursor, and silica particles to prepare a carbon precursor mixture; drying and carbonizing the carbon precursor mixture to prepare a silica-carbon composite; and removing silica from the silica-carbon composite. An anode and/or a cathode of fuel cell includes catalyst particles supported on the heteroatom-containing mesoporous carbon.

    摘要翻译： 含杂原子的介孔碳的孔径为11〜35nm，比表面积为500m 2 / g以上，且含有杂原子。 通过包括混合碳前体，含杂原子的前体和二氧化硅颗粒以制备碳前体混合物的方法形成含杂原子的介孔碳; 干燥和碳化碳前体混合物以制备二氧化硅 - 碳复合材料; 并从二氧化硅 - 碳复合材料中除去二氧化硅。 燃料电池的阳极和/或阴极包括负载在含杂原子的介孔碳上的催化剂颗粒。

    Supported catalyst, method of preparing the same, and fuel cell using the same
    9.
    发明申请
    Supported catalyst, method of preparing the same, and fuel cell using the same 有权
    负载催化剂，其制备方法和使用其的燃料电池

    公开(公告)号：US20070270305A1

    公开(公告)日：2007-11-22

    申请号：US11708600

    申请日：2007-02-21

    申请人： Chan-ho Pak ,  Dae-jong Yoo ,  Sang-hoon Joo ,  Hyuk Chang ,  Seol-ah Lee

    发明人： Chan-ho Pak ,  Dae-jong Yoo ,  Sang-hoon Joo ,  Hyuk Chang ,  Seol-ah Lee

    IPC分类号： B01J31/00

    CPC分类号： H01M4/926 ,  H01M4/8657 ,  H01M4/8814 ,  H01M4/885 ,  H01M4/92 ,  H01M4/921 ,  H01M8/1007 ,  H01M8/1011 ,  Y02E60/523 ,  Y02P70/56

    摘要： A method of preparing a supported catalyst, the method comprising mixing a first catalytic metal precursor and a first solvent to obtain a first catalytic metal precursor mixture; mixing a carbon support for catalyst and the first catalytic metal precursor mixture, and drying the mixture to obtain a primary supported catalyst precursor; subjecting the primary supported catalyst precursor to a hydrogen reduction heat treatment, to obtain a primary supported catalyst; mixing the primary supported catalyst and a polyhydric alcohol to obtain a primary supported catalyst mixture; mixing a second catalytic metal precursor and a second solvent to obtain a second catalytic metal precursor mixture; mixing the primary supported catalyst mixture and the second catalytic metal precursor mixture to obtain a secondary supported catalyst precursor mixture; and adjusting the pH of the secondary supported catalyst precursor mixture, and then heating the secondary supported catalyst precursor mixture to obtain a supported catalyst, a supported catalyst prepared by the method, an electrode comprising the supported catalyst, and a fuel cell including the electrode are provided. A supported catalyst having a desired amount of loaded catalytic metal particles can be obtained by preparing a primary supported catalyst containing catalytic metal particles that are obtained by a primary gas phase reduction reaction of a portion of the final loading amount of catalytic metal, and reducing the remaining portion of the catalytic metal by a secondary liquid phase reduction reaction. The supported catalyst contains catalytic metal particles having a very small average particle size, which are uniformly distributed on a carbon support at a high concentration, and thus exhibits maximal catalyst activity. A fuel cell produced using the supported catalyst has improved efficiency.

    摘要翻译： 一种制备负载型催化剂的方法，所述方法包括混合第一催化金属前体和第一溶剂以获得第一催化金属前体混合物; 混合催化剂用碳载体和第一催化金属前体混合物，干燥混合物得到主要负载型催化剂前体; 对初级负载催化剂前体进行氢还原热处理，得到主要负载型催化剂; 将主要负载型催化剂和多元醇混合，得到主要负载型催化剂混合物; 混合第二催化金属前体和第二溶剂以获得第二催化金属前体混合物; 将主要负载的催化剂混合物和第二催化金属前体混合物混合，得到二次负载催化剂前体混合物; 调节二次负载型催化剂前体混合物的pH，然后加热二次负载型催化剂前体混合物，得到负载型催化剂，通过该方法制备的负载催化剂，包含负载型催化剂的电极和包含该电极的燃料电池 提供。 具有所需量的负载的催化金属颗粒的负载型催化剂可以通过制备含有催化金属颗粒的主负载催化剂获得，所述催化金属颗粒是通过催化金属的最终负载量的一部分一次气相还原反应获得的， 催化金属的剩余部分通过二次液相还原反应。 载体催化剂含有平均粒径非常小的催化金属颗粒，其以高浓度均匀分布在碳载体上，因此表现出最大的催化剂活性。 使用负载型催化剂制造的燃料电池具有提高的效率。

    Supported catalyst, method of preparing the same, and fuel cell using the same
    10.
    发明授权
    Supported catalyst, method of preparing the same, and fuel cell using the same 有权
    负载催化剂，其制备方法和使用其的燃料电池

    公开(公告)号：US07994088B2

    公开(公告)日：2011-08-09

    申请号：US11708600

    申请日：2007-02-21

    申请人： Chan-ho Pak ,  Dae-jong Yoo ,  Sang-hoon Joo ,  Hyuk Chang ,  Seol-ah Lee

    发明人： Chan-ho Pak ,  Dae-jong Yoo ,  Sang-hoon Joo ,  Hyuk Chang ,  Seol-ah Lee

    IPC分类号： H01M4/88 ,  B01J21/18 ,  B01J23/00 ,  B01J23/40 ,  B01J23/74 ,  H01M4/02 ,  H01M4/36 ,  H01M4/92 ,  H01M4/94 ,  H01M4/90

    CPC分类号： H01M4/926 ,  H01M4/8657 ,  H01M4/8814 ,  H01M4/885 ,  H01M4/92 ,  H01M4/921 ,  H01M8/1007 ,  H01M8/1011 ,  Y02E60/523 ,  Y02P70/56

    摘要： A method of preparing a supported catalyst, a supported catalyst prepared by the method, and a fuel cell using the supported catalyst. In particular, a method of preparing a supported catalyst by preparing a primary supported catalyst containing catalytic metal particles that are obtained by a primary gas phase reduction reaction of a portion of the final loading amount of a catalytic metal, and reducing the remaining portion of the catalytic metal by a secondary liquid phase reduction reaction using the primary supported catalyst. The supported catalyst contains catalytic metal particles having a very small average particle size, which are uniformly distributed on a carbon support at a high concentration, and thus exhibits maximal catalyst activity. A fuel cell produced using the supported catalyst has improved efficiency.

    摘要翻译： 制备载体催化剂的方法，通过该方法制备的负载催化剂和使用负载型催化剂的燃料电池。 特别是制备负载型催化剂的方法，该方法是通过制备含有催化金属颗粒的主载体催化剂，所述催化剂金属颗粒是通过催化金属的最终负载量的一部分的一次气相还原反应获得的，并且还原剩余部分 催化金属通过使用主要负载催化剂的二次液相还原反应。 载体催化剂含有平均粒径非常小的催化金属颗粒，其以高浓度均匀分布在碳载体上，因此表现出最大的催化剂活性。 使用负载型催化剂制造的燃料电池具有提高的效率。