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公开(公告)号：US09456621B2
公开(公告)日：2016-10-04
申请号：US12975805
申请日：2010-12-22
申请人： Brent E. Green , Sarah Medina , Martin Schweizer , Kevin I. Segall , Johann Tergesen , Russ Sampson , Roland Rosset , Curtis D. Hayden , Edwin Catipon
发明人： Brent E. Green , Sarah Medina , Martin Schweizer , Kevin I. Segall , Johann Tergesen , Russ Sampson , Roland Rosset , Curtis D. Hayden , Edwin Catipon
CPC分类号： A23J3/16 , A23J1/14 , A23V2002/00 , A23V2250/5488 , A23V2200/21 , A23V2300/14 , A23V2300/24 , A23V2300/34 , A23V2300/40
摘要： pH-adjusted soy protein products, particularly isolates, that have a natural pH of about 6 and have a non-beany flavor are provided by the processing of soy protein product which is completely soluble in aqueous media at a pH of less than about 4.4 and heat stable in this pH range or a concentrated soy protein solution produced in the preparation of such soy protein product.
摘要翻译： pH调节大豆蛋白产品，特别是分离物，具有约6的天然pH并且具有非蜜饯味，通过加工大豆蛋白产物来提供，该蛋白质产物在小于约4.4的pH下完全溶于含水介质中， 在该pH范围内热稳定或在制备这种大豆蛋白产品中产生的浓缩大豆蛋白溶液。
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公开(公告)号：US08936824B2
公开(公告)日：2015-01-20
申请号：US13381132
申请日：2010-06-30
CPC分类号： A23L2/66 , A23J1/14 , A23L2/39 , A23L33/185 , A23V2002/00 , A23V2250/1578 , A23V2300/34 , A23V2300/38 , A23V2300/40
摘要： A soy protein product having a protein content of at least about 60 wt % (N×6.25) d.b., preferably an isolate having a protein content of at least about 90 wt % (N×6.25) d.b., is formed by extracting a soy protein source with a salt solution, preferably aqueous sodium chloride solution, to form an aqueous protein solution having a pH of about 1.5 to 11, preferably about 5 to about 7 and separating the resulting aqueous protein solution from residual soy protein source. The protein concentration of the aqueous protein solution is increased to about 50 to about 400 g/L while the ionic strength is maintained substantially constant by using a selective membrane technique. The resulting concentrated protein solution is optionally diafiltered and a calcium salt, preferably calcium chloride, is added to the concentrated and optionally diafiltered protein solution to a conductivity of 15 to about 85 mS. Precipitate formed as a result of the calcium salt addition is removed and the resulting clarified retentate is diluted into about 2 to about 20 volumes of water prior to acidification to a pH of about 1.5 to about 4.4 to produce an acidified clear protein solution. The acidified clear protein solution is then concentrated and optionally diafiltered and optionally dried. Variations of this procedure can be used to produce a soy protein product which is soluble, transparent and heat stable in acidic aqueous environments.
摘要翻译： 蛋白质含量至少约为60重量％（N×6.25）db，优选具有至少约90重量％（N×6.25）db蛋白质含量的分离物的大豆蛋白产物是通过提取大豆蛋白 来源于盐溶液，优选氯化钠水溶液，以形成pH为约1.5至11，优选约5至约7的蛋白质水溶液，并将所得蛋白质水溶液与残留的大豆蛋白源分离。 通过使用选择性膜技术，蛋白质水溶液的蛋白质浓度增加至约50至约400g / L，同时离子强度基本上保持恒定。 任选地将所得浓缩的蛋白质溶液进行渗滤，并将钙盐（优选氯化钙）加入到浓缩和任选的渗滤的蛋白质溶液中至15至约85mS的电导率。 去除由钙盐加入而形成的沉淀物，并将所得澄清的滞留物在酸化至约1.5至约4.4的pH之前稀释成约2至约20体积的水，以产生酸化的澄清蛋白质溶液。 然后浓缩酸化的透明蛋白质溶液，任选地进行渗滤并任选地干燥。 该方法的变化可用于生产在酸性水性环境中可溶，透明和热稳定的大豆蛋白产品。
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3.发明申请PREPARATION OF SOY PROTEIN ISOLATE USING CALCIUM CHLORIDE EXTRACTION ("S703") 审中-公开使用氯化钙提取制备分离的大豆蛋白（“S703”）公开(公告)号：US20140010944A1
公开(公告)日：2014-01-09
申请号：US14022316
申请日：2013-09-10
CPC分类号： A23J1/14 , A23J3/16 , A23L2/66 , A23V2002/00 , A23V2250/5488
摘要： A soy protein product having a protein content of at least about 60 wt % (N×6.25) d.b., preferably an isolate, is formed by a procedure in which soy protein is extracted from a soy source material using an aqueous calcium chloride solution at low pH, generally about 1.5 to about 5, and separating the resulting aqueous soy protein solution from residual soy protein source. The resulting clarified aqueous soy protein solution may be diluted and the pH adjusted within the range of 1.5-5.0. The solution may be concentrated by ultrafiltration, diafiltered and then dried to provide the soy protein product. The soy protein product is soluble in acidic medium and produces transparent, heat stable solutions and hence may be used for protein fortification of soft drinks and sports drinks.
摘要翻译： 蛋白质含量为至少约60重量％（N×6.25）db，优选分离物的大豆蛋白产品是通过使用氯化钙水溶液在大豆来源材料中提取大豆蛋白的方法形成的 通常约1.5至约5，并将所得的大豆蛋白水溶液与残留的大豆蛋白源分离。 所得澄清的大豆蛋白水溶液可以稀释，pH调节在1.5-5.0的范围内。 可以通过超滤浓缩溶液，进行渗滤，然后干燥以提供大豆蛋白产物。 大豆蛋白产品可溶于酸性介质，产生透明，热稳定的溶液，因此可用于软饮料和运动饮料的蛋白质强化。
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公开(公告)号：US08609177B2
公开(公告)日：2013-12-17
申请号：US12662594
申请日：2010-04-26
IPC分类号： A23J1/00
CPC分类号： A23J1/14 , A23V2002/00 , A23V2250/1578 , A23V2300/34 , A23V2300/40
摘要： The supernatant from the deposition of canola protein micellar mass is processed to provide a canola protein product having a protein content of about 60 to less than about 90 wt % (N×6.25) protein on a dry weight basis and which is soluble in an aqueous acidic environment.
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5.发明申请PRODUCTION OF SOY PROTEIN PRODUCT USING CALCIUM CHLORIDE EXTRACTION ("S702") 审中-公开使用氯化钙萃取生产大豆蛋白产品（“S702”）公开(公告)号：US20130101713A1
公开(公告)日：2013-04-25
申请号：US13712040
申请日：2012-12-12
IPC分类号： A23J1/14
CPC分类号： A23J1/14 , A23J3/16 , A23L2/39 , A23L2/66 , A23L33/185 , A23V2002/00 , A23V2300/34 , A23V2300/40
摘要： A soy protein product having a protein content of at least about 60 wt % (N×6.25) d.b., preferably a soy protein isolate having a protein content of at least about 90 wt % (N×6.25) d.b., is prepared from a soy protein source material by extraction of the soy protein source material with an aqueous calcium salt solution, preferably calcium chloride solution, to cause solubilization of soy protein from the protein source and to form an aqueous soy protein solution, separating the aqueous soy protein solution from residual soy protein source, concentrating the aqueous soy protein solution while maintaining the ionic strength substantially constant by using a selective membrane technique, optionally diafiltering the concentrated soy protein solution, and drying the concentrated and optionally diafiltered soy protein solution.
摘要翻译： 蛋白质含量为至少约60重量％（N×6.25）db，优选蛋白质含量为至少约90重量％（N×6.25）db的大豆蛋白分离物的大豆蛋白产品由大豆制备 通过用钙盐水溶液（优选氯化钙溶液）提取大豆蛋白源材料来引起大豆蛋白质从蛋白质来源溶解并形成大豆蛋白水溶液，从而将大豆蛋白水溶液与残留物分离 大豆蛋白源，浓缩大豆蛋白水溶液，同时通过使用选择性膜技术保持离子强度基本上恒定，任选地过滤浓缩的大豆蛋白溶液，并干燥浓缩和任选的渗滤的大豆蛋白溶液。
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公开(公告)号：US20110038993A1
公开(公告)日：2011-02-17
申请号：US12923897
申请日：2010-10-13
申请人： Martin Schweizer , Kevin I. Segall , Brent E. Green , Sarah Medina , James Logie , Brandy Gosnell
发明人： Martin Schweizer , Kevin I. Segall , Brent E. Green , Sarah Medina , James Logie , Brandy Gosnell
CPC分类号： A23L33/185 , A23J1/14 , A23J3/16 , A23L2/66 , A23L11/32 , A23V2002/00 , A23V2200/238 , A23V2250/5488 , A23V2300/14 , A23V2300/34 , C11B1/10
摘要： A soy protein product, which may be an isolate, produces transparent heat-stable solutions at low pH values and is useful for the fortification of soft drinks and sports drinks without precipitation of protein. The soy protein product is obtained by extracting a soy protein source material with an aqueous calcium salt solution to form an aqueous soy protein solution, separating the aqueous soy protein solution from residual soy protein source, adjusting the pH of the aqueous soy protein solution to a pH of about 1.5 to about 4.4 to produce an acidified clear soy protein solution, which may be dried, following optional concentration and diafiltration, to provide the soy protein product.
摘要翻译： 大豆蛋白产品，其可以是分离物，在低pH值下产生透明的热稳定溶液，并且可用于强化没有蛋白质沉淀的软饮料和运动饮料。 通过用钙盐水溶液提取大豆蛋白源材料以形成大豆蛋白水溶液溶液，将大豆蛋白水溶液与残留的大豆蛋白质源分离，将大豆蛋白水溶液的pH调节至 pH为约1.5至约4.4以产生酸化的透明大豆蛋白溶液，其可以在任选的浓缩和渗滤之后干燥，以提供大豆蛋白产物。
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公开(公告)号：US20100330248A1
公开(公告)日：2010-12-30
申请号：US12828199
申请日：2010-06-30
IPC分类号： A23L2/00 , C07K14/415
CPC分类号： A23L2/39 , A23J3/16 , A23L2/66 , A23V2002/00 , A23V2250/5488 , A23V2200/33
摘要： A soy protein product having a protein content of at least about 60 wt % (N×6.25) d.b., preferably an isolate having a protein content of at least about 90 wt % (N×6.25) d.b., is formed by extracting a soy protein source with a salt solution, preferably aqueous sodium chloride solution, to form an aqueous protein solution having a pH of about 1.5 to 11, preferably about 5 to about 7 and separating the resulting aqueous protein solution from residual soy protein source. The protein concentration of the aqueous protein solution is increased to about 50 to about 400 g/L while the ionic strength is maintained substantially constant by using a selective membrane technique. The resulting concentrated protein solution is optionally diafiltered and a calcium salt, preferably calcium chloride, is added to the concentrated and optionally diafiltered protein solution to a conductivity of 15 to about 85 mS. Precipitate formed as a result of the calcium salt addition is removed and the resulting clarified retentate is diluted into about 2 to about 20 volumes of water prior to acidification to a pH of about 1.5 to about 4.4 to produce an acidified clear protein solution. The acidified clear protein solution is then concentrated and optionally diafiltered and optionally dried. Variations of this procedure can be used to produce a soy protein product which is soluble, transparent and heat stable in acidic aqueous environments.
摘要翻译： 蛋白质含量至少约为60重量％（N×6.25）db，优选具有至少约90重量％（N×6.25）db蛋白质含量的分离物的大豆蛋白产物是通过提取大豆蛋白 来源于盐溶液，优选氯化钠水溶液，以形成pH为约1.5至11，优选约5至约7的蛋白质水溶液，并将所得蛋白质水溶液与残留的大豆蛋白源分离。 通过使用选择性膜技术，蛋白质水溶液的蛋白质浓度增加至约50至约400g / L，同时离子强度基本上保持恒定。 任选地将所得浓缩的蛋白质溶液进行渗滤，并将钙盐（优选氯化钙）加入到浓缩和任选的渗滤的蛋白质溶液中至15至约85mS的电导率。 去除由钙盐加入而形成的沉淀物，并将所得澄清的滞留物在酸化至约1.5至约4.4的pH之前稀释成约2至约20体积的水，以产生酸化的澄清蛋白质溶液。 然后浓缩酸化的透明蛋白质溶液，任选地进行渗滤并任选地干燥。 该方法的变化可用于生产在酸性水性环境中可溶，透明和热稳定的大豆蛋白产品。
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8.发明申请Production of Soy Protein Product Using Calcium Chloride Extraction ("S702") 审中-公开使用氯化钙提取生产大豆蛋白产品（“S702”）公开(公告)号：US20100203205A1
公开(公告)日：2010-08-12
申请号：US12704078
申请日：2010-02-11
CPC分类号： A23J1/14 , A23J3/16 , A23L2/39 , A23L2/66 , A23L33/185 , A23V2002/00 , A23V2300/34 , A23V2300/40
摘要： A soy protein product having a protein content of at least about 60 wt % (N×6.25) d.b., preferably a soy protein isolate having a protein content of at least about 90 wt % (N×6.25) d.b., is prepared from a soy protein source material by extraction of the soy protein source material with an aqueous calcium salt solution, preferably calcium chloride solution, to cause solubilization of soy protein from the protein source and to form an aqueous soy protein solution, separating the aqueous soy protein solution from residual soy protein source, concentrating the aqueous soy protein solution while maintaining the ionic strength substantially constant by using a selective membrane technique, optionally diafiltering the concentrated soy protein solution, and drying the concentrated and optionally diafiltered soy protein solution.
摘要翻译： 蛋白质含量为至少约60重量％（N×6.25）db，优选蛋白质含量为至少约90重量％（N×6.25）db的大豆蛋白分离物的大豆蛋白产品由大豆制备 通过用钙盐水溶液（优选氯化钙溶液）提取大豆蛋白源材料来引起大豆蛋白质从蛋白质来源溶解并形成大豆蛋白水溶液，从而将大豆蛋白水溶液与残留物分离 大豆蛋白源，浓缩大豆蛋白水溶液，同时通过使用选择性膜技术保持离子强度基本上恒定，任选地过滤浓缩的大豆蛋白溶液，并干燥浓缩和任选的渗滤的大豆蛋白溶液。
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9.发明申请公开(公告)号：US20130316069A1
公开(公告)日：2013-11-28
申请号：US13879418
申请日：2011-09-26
申请人： Martin Schweizer , Kevin I. Segall , Brent E. Green , Sarah Medina , James Logie , Brandy Gosnell
发明人： Martin Schweizer , Kevin I. Segall , Brent E. Green , Sarah Medina , James Logie , Brandy Gosnell
CPC分类号： A23L33/185 , A23J1/14 , A23J3/16 , A23L2/66 , A23L11/32 , A23V2002/00 , A23V2200/238 , A23V2250/5488 , A23V2300/14 , A23V2300/34 , C11B1/10
摘要： A soy protein product, which may be an isolate, produces transparent heat-stable solutions at low pH values and is useful for the fortification of soft drinks and sports drinks without precipitation of protein. The soy protein product is obtained by extracting a soy protein source material with an aqueous calcium salt solution to form an aqueous soy protein solution, separating the aqueous soy protein solution from residual soy protein source, adjusting the pH of the aqueous soy protein solution to a pH of about 1.5 to about 4.4 to produce an acidified clear soy protein solution, which may be dried, following optional concentration and diafiltration, to provide the soy protein product.
摘要翻译： 大豆蛋白产品，其可以是分离物，在低pH值下产生透明的热稳定溶液，并且可用于强化没有蛋白质沉淀的软饮料和运动饮料。 通过用钙盐水溶液提取大豆蛋白源材料以形成大豆蛋白水溶液溶液，将大豆蛋白水溶液与残留的大豆蛋白质源分离，将大豆蛋白水溶液的pH调节至 pH为约1.5至约4.4以产生酸化的透明大豆蛋白溶液，其可以在任选的浓缩和渗滤之后干燥，以提供大豆蛋白产物。
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10.发明授权Preparation of soy protein isolate using calcium chloride extraction (“S703”) 有权使用氯化钙提取制备大豆蛋白分离物（“S703”）公开(公告)号：US08557321B2
公开(公告)日：2013-10-15
申请号：US13378680
申请日：2010-06-30
IPC分类号： A23L2/38
CPC分类号： A23J1/14 , A23J3/16 , A23L2/66 , A23V2002/00 , A23V2250/5488
摘要： A soy protein product having a protein content of at least about 60 wt % (N×6.25) d.b., preferably an isolate, is formed by a procedure in which soy protein is extracted from a soy source material using an aqueous calcium chloride solution at low pH, generally about 1.5 to about 5, and separating the resulting aqueous soy protein solution from residual soy protein source. The resulting clarified aqueous soy protein solution may be diluted and the pH adjusted within the range of 1.5-5.0. The solution may be concentrated by ultrafiltration, diafiltered and then dried to provide the soy protein product. The soy protein product is soluble in acidic medium and produces transparent, heat stable solutions and hence may be used for protein fortification of soft drinks and sports drinks.
摘要翻译： 蛋白质含量为至少约60重量％（N×6.25）db，优选分离物的大豆蛋白产品是通过使用氯化钙水溶液在大豆来源材料中提取大豆蛋白的方法形成的 通常约1.5至约5，并将所得的大豆蛋白水溶液与残留的大豆蛋白源分离。 所得澄清的大豆蛋白水溶液可以稀释，pH调节在1.5-5.0的范围内。 可以通过超滤浓缩溶液，进行渗滤，然后干燥以提供大豆蛋白产物。 大豆蛋白产品可溶于酸性介质，产生透明，热稳定的溶液，因此可用于软饮料和运动饮料的蛋白质强化。
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