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    Viscous carrier compositions, including gels, formed with an organic liquid carrier, a layered material: polymer complex, and a di-, and/or tri-valent cation
    1.
    发明授权
    Viscous carrier compositions, including gels, formed with an organic liquid carrier, a layered material: polymer complex, and a di-, and/or tri-valent cation 失效
    粘性载体组合物，包括由有机液体载体形成的凝胶，层状材料：聚合物复合物，和二价和/或三价阳离子

    公开(公告)号：US5998528A

    公开(公告)日：1999-12-07

    申请号：US17421

    申请日：1998-02-02

    申请人： Semeon Tsipursky ,  Vladimir Dolinko ,  Vasiliki Psihogios ,  Gary W. Beall

    发明人： Semeon Tsipursky ,  Vladimir Dolinko ,  Vasiliki Psihogios ,  Gary W. Beall

    IPC分类号： C01B33/44 ,  C08K3/00 ,  C08K3/34 ,  C08K7/00 ,  C08K9/04 ,  C08K9/08 ,  C08L101/00 ,  C11C5/00 ,  C08J5/10 ,  C08L39/06

    CPC分类号： B82Y30/00 ,  A61K8/26 ,  A61K8/27 ,  A61K8/8176 ,  A61Q5/04 ,  C01B33/44 ,  C08K3/34 ,  C08K7/00 ,  C08K9/04 ,  C08K9/08 ,  C11C5/002 ,  A61K2800/56 ,  C01P2002/74 ,  C01P2004/20 ,  C01P2004/54 ,  C01P2004/64

    摘要： Intercalates formed by contacting the layer material, e.g., a phyllosilicate, with an intercalant to sorb or intercalate the between adjacent platelets of the layered material. Sufficient intercalant polymer is sorbed between adjacent platelets to expand the adjacent platelets at least about 5 .ANG. (as measured after water removal to 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. A monovalent, divalent and/or trivalent cation is added to the intercalating composition, or after intercalation for surprising increases in viscosity. The intercalated complex is combined with an organic liquid into an unexpectedly viscous carrier material, for delivery of the carrier material, or for delivery of an active compound, e.g., a pharmaceutical, or cosmetic, or lubricant, e.g., food grade lubricants dissolved or dispersed in the carrier material. Alternatively, the intercalated complex can be exfoliated prior to combination with the organic liquid.

    摘要翻译： 通过使层状材料例如页硅酸盐与插入剂接触而形成的插层，以吸附或插入层状材料的相邻片晶之间。 在相邻的血小板之间吸附足够的嵌入聚合物以将相邻的血小板膨胀至少约5 ANGSTROM（在去除水至5重量％水之后测量），高达约100安培，优选在约10-45安培姆范围内 插入物容易被剥离成单独的血小板。 将一价，二价和/或三价阳离子加入到插层组合物中，或插入后，使粘度增加令人惊讶。 插入的络合物与有机液体组合成意外粘稠的载体材料，用于递送载体材料，或用于递送活性化合物，例如药物或化妆品或润滑剂，例如溶解或分散的食品级润滑剂 在载体材料中。 或者，插入的复合物可以在与有机液体组合之前被剥离。

    Intercalates and exfoliates formed with N-alkenyl amides and/or acrylate-functional pyrrolidone and allylic monomers, oligomers and copolymers and composite materials containing same
    2.
    发明授权
    Intercalates and exfoliates formed with N-alkenyl amides and/or acrylate-functional pyrrolidone and allylic monomers, oligomers and copolymers and composite materials containing same 失效
    由N-烯基酰胺和/或丙烯酸酯官能的吡咯烷酮和烯丙基单体，低聚物和共聚物以及含有它们的复合材料形成的嵌入物和去角质

    公开(公告)号：US5849830A

    公开(公告)日：1998-12-15

    申请号：US951094

    申请日：1997-10-15

    申请人： Semeon Tsipursky ,  Gary W. Beall ,  Elena I. Vinokour

    发明人： Semeon Tsipursky ,  Gary W. Beall ,  Elena I. Vinokour

    IPC分类号： C01B33/44 ,  C08K3/34 ,  C08K7/00 ,  C08K9/04 ,  C08K9/08 ,  C08L33/26 ,  C08L67/02 ,  C08L77/00 ,  C08L101/00 ,  C11C5/00 ,  C08J5/10 ,  C08L33/00

    CPC分类号： C01B33/44 ,  B82Y30/00 ,  C08K3/34 ,  C08K7/00 ,  C08K9/04 ,  C08K9/08 ,  C11C5/002 ,  C01P2002/74 ,  C01P2004/20 ,  C01P2004/54 ,  C01P2004/64

    摘要： Nanocomposites are manufactured by combining a host material, such as an organic solvent or a matrix polymer and exfoliated intercalates formed by contacting a phyllosilicate with an intercalant selected from the group consisting of (1) an N-alkenyl amide monomer and an allylic monomer; (2) an oligomer formed by copolymerizing an N-alkenyl amide monomer and an allylic monomer; (3) a polymer formed by copolymerizing an N-alkenyl amide monomer and an allylic monomer; and (4) mixtures thereof to adsorb or the intercalant between adjacent phyllosilicate platelets. Sufficient polymer is adsorbed between adjacent phyllosilicate platelets to expand the adjacent platelets to increase the spacing at least about 10 .ANG., preferably at least about 20 .ANG. (as measured after water removal), up to about 100 .ANG. and preferably in the range of about 30-40 .ANG., so that the intercalate easily can be exfoliated, e.g., when mixed with an organic solvent or a polymer melt, to provide a carrier material for drugs and the like, or to provide a matrix polymer/platelet composite (nanocomposite) material--the platelets being exfoliated from the intercalate.

    摘要翻译： 纳米复合材料通过将主体材料如有机溶剂或基质聚合物和通过使页硅酸盐与选自（1）N-烯基酰胺单体和烯丙基单体的插入剂接触而形成的剥离的嵌入物组合而制造; （2）通过共聚N-烯基酰胺单体和烯丙基单体形成的低聚物; （3）通过共聚N-烯基酰胺单体和烯丙基单体形成的聚合物; 和（4）它们的混合物以吸附相邻的页硅酸盐血小板之间的嵌入剂。 在相邻的页硅酸盐片晶之间吸附足够的聚合物以扩展相邻的血小板，以将间隔增加至少约10安培，优选至少约20安培（在除水后测量），高达约100安培，优选在约30 -40 ANGSTROM，使得嵌入物容易被剥离，例如当与有机溶剂或聚合物熔体混合时，提供用于药物等的载体材料，或提供基质聚合物/血小板复合材料（纳米复合材料） - 血小板从插层中剥离。

    Intercalates and exfoliates formed with long chain (C.sub.10 +) monomeric organic intercalant compounds; and composite materials containing same
    4.
    发明授权
    Intercalates and exfoliates formed with long chain (C.sub.10 +) monomeric organic intercalant compounds; and composite materials containing same 失效
    由长链（C10 +）单体有机插层剂形成的插层和去角质; 和含有它们的复合材料

    公开(公告)号：US5952095A

    公开(公告)日：1999-09-14

    申请号：US758740

    申请日：1996-12-06

    申请人： Gary W. Beall ,  Fernando Serrano ,  Semeon Tsipursky ,  Steven J. Engman

    发明人： Gary W. Beall ,  Fernando Serrano ,  Semeon Tsipursky ,  Steven J. Engman

    IPC分类号： C01B33/44 ,  C08K7/00 ,  C08K9/04 ,  C08L101/00 ,  C09C1/42 ,  C09C3/10 ,  B32B7/00

    CPC分类号： C09C1/42 ,  C01B33/44 ,  C08K9/04 ,  C09C3/10 ,  C01P2002/08 ,  C01P2002/72 ,  C01P2002/77 ,  C01P2004/54 ,  Y10T428/26

    摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer including an alkyl radical having at least 10 carbon atoms and having a dipole moment greater than the dipole moment of water, to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG. (as measured after water removal to a maximum of 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix.

    摘要翻译： 通过使层状材料例如页硅酸盐与包含具有至少10个碳原子的烷基并且具有大于偶极矩的偶极矩的插层单体接触形成的插层，以吸附或插入相邻片晶之间的插入剂单体 的分层材料。 在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5 ANGSTROM（水除去后测量到最多5％（重量）水）的间隔，最高达约100安培，最好在 约10-45安士，使得插入物容易被剥离成单独的血小板。 插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。

    Intercalates and exfoliates formed with hydroxyl-functional; polyhydroxyl-functional; and aromatic compounds; composite materials containing same and methods of modifying rheology therewith
    6.
    发明授权
    Intercalates and exfoliates formed with hydroxyl-functional; polyhydroxyl-functional; and aromatic compounds; composite materials containing same and methods of modifying rheology therewith 有权
    插层和去角质形成羟基官能团; 多羟基官能团 和芳香族化合物; 含有其的复合材料以及用其改性流变性的方法

    公开(公告)号：US06461423B1

    公开(公告)日：2002-10-08

    申请号：US09578129

    申请日：2000-05-24

    申请人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    发明人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    IPC分类号： B05D700

    CPC分类号： C01B33/44 ,  C08K9/04 ,  F16C2240/64

    摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer having a hydroxyl and/or an aromatic ring functionality to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 Å (as measured after water removal to a maximum of 5% by weight water), up to about 100 Å and preferably in the range of about 10-45 Å, so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix. Alternatively, the intercalated complex can be exfoliated prior to or after combination with the organic liquid or the matrix polymer.

    摘要翻译： 通过使分层材料例如页硅酸盐与具有羟基和/或芳环官能团的嵌入剂单体接触形成的嵌入体，以在分层材料的相邻片晶之间吸附或插入插入剂单体。 在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5埃的水平（在除水后测量为最多5重量％的水），至多约100埃，优选在 约10-45埃，使得插入物容易被剥离成单独的血小板。 插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。 或者，插入的复合物可以在与有机液体或基质聚合物组合之前或之后剥离。

    Intercalates and exfoliates formed with organic pesticides compounds and compositions containing the same
    7.
    发明授权
    Intercalates and exfoliates formed with organic pesticides compounds and compositions containing the same 失效
    用有机农药化合物和含有它们的组合物形成的插层和去角质

    公开(公告)号：US5955094A

    公开(公告)日：1999-09-21

    申请号：US963818

    申请日：1997-11-04

    申请人： Gary W. Beall ,  Semeon Tsipursky ,  Katherine R. Turk

    发明人： Gary W. Beall ,  Semeon Tsipursky ,  Katherine R. Turk

    IPC分类号： A01N25/08 ,  A01N25/10

    CPC分类号： A01N25/08

    摘要： Intercalates formed by contacting an activated layered material, e.g., an activated phyllosilicate, with an intercalant pesticide to intercalate an intercalant pesticide between adjacent platelets of the layered material is disclosed. Sufficient intercalant pesticide is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG. (as measured after water removal to a maximum of 5% by weight water) up to about 100 .ANG., and preferably in the range of about 10 to about 45 .ANG., so that, if desired, the intercalate can be exfoliated into individual platelets. The intercalate can be combined with an organic liquid to form a viscous composition for delivery of a pesticide compound. Alternatively, the intercalate can be exfoliated prior to combination with the organic liquid. The intercalated complex also can be admixed with solid particles to provide a granular, dust, or wettable powder pesticide composition.

    摘要翻译： 公开了通过使活化的层状材料（例如活化的页硅酸盐）与插入剂农药接触而形成的插层，以在层状材料的相邻片晶之间插入插入剂农药。 在相邻血小板之间吸附足够的嵌入剂杀虫剂以将相邻的血小板膨胀至至多约5安培的水平（在除水至最多5重量％水之后测量）至多约100安培的范围内，优选在 约10至约45个角度，使得如果需要，插层物可以被剥离成单独的血小板。 插层物可以与有机液体组合以形成用于递送农药化合物的粘性组合物。 或者，插入物可以在与有机液体组合之前被剥离。 插层的复合物也可以与固体颗粒混合，以提供颗粒状，粉尘或可湿性粉剂农药组合物。

    Intercalates; exfoliates; process for manufacturing intercalates and exfoliates and composite materials containing same
    9.
    发明授权
    Intercalates; exfoliates; process for manufacturing intercalates and exfoliates and composite materials containing same 失效
    插层; 去角质 用于制造插层和去角质的方法以及含有它们的复合材料

    公开(公告)号：US5578672A

    公开(公告)日：1996-11-26

    申请号：US480080

    申请日：1995-06-07

    申请人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    发明人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    IPC分类号： B29C47/00 ,  C01B33/44 ,  C08K3/34 ,  C08K9/04 ,  C08L101/00 ,  C11C5/00 ,  C08K9/06

    CPC分类号： C11C5/002 ,  C01B33/44 ,  C08K9/04 ,  Y10T428/259

    摘要： Intercalates formed by mixing the phyllosilicate with a polymer and a liquid carrier, and extruding the mixture through a die-opening to adsorb or intercalate the polymer between adjacent phyllosilicate platelets. Sufficient polymer is adsorbed between adjacent phyllosilicate platelets to expand the adjacent platelets to a spacing of at least about 10 .ANG. (as measured after water removal), up to about 55 .ANG. and preferably in the range of about 30-40 .ANG., so that the intercalate easily can be exfoliated into individual platelets by heating the polymer to its melting point, to provide a matrix polymer/platelet composite material.

    摘要翻译： 通过将页硅酸盐与聚合物和液体载体混合而形成的嵌入物，并且通过模具开口挤出混合物以在相邻的页硅酸盐片剂之间吸附或嵌入聚合物。 在相邻的页硅酸盐片之间吸附足够的聚合物以使相邻的血小板膨胀至至少约10安培（除水后测量）的间隔，最高约为55安培，优选在约30-40安培范围内， 通过将聚合物加热至其熔点，易于插入到各个血小板中，以提供基质聚合物/血小板复合材料。

    Intercalates and exfoliates formed with hydroxyl-functional; polyhydroxyl-functional; and aromatic compounds; composite materials containing same and methods of modifying rheology therewith
    10.
    发明授权
    Intercalates and exfoliates formed with hydroxyl-functional; polyhydroxyl-functional; and aromatic compounds; composite materials containing same and methods of modifying rheology therewith 有权
    插层和去角质形成羟基官能团; 多羟基官能团 和芳香族化合物; 含有其的复合材料以及用其改性流变性的方法

    公开(公告)号：US6126734A

    公开(公告)日：2000-10-03

    申请号：US158490

    申请日：1998-09-22

    申请人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    发明人： Gary W. Beall ,  Semeon Tsipursky ,  Anatoliy Sorokin ,  Anatoliy Goldman

    IPC分类号： C01B33/44 ,  C08K9/04 ,  B05D7/00

    CPC分类号： C01B33/44 ,  C08K9/04

    摘要： Intercalates formed by contacting a layered material, e.g., a phyllosilicate, with an intercalant monomer having a hydroxyl and/or an aromatic ring functionality to sorb or intercalate the intercalant monomer between adjacent platelets of the layered material. Sufficient intercalant monomer is sorbed between adjacent platelets to expand the adjacent platelets to a spacing of at least about 5 .ANG. (as measured after water removal to a maximum of 5% by weight water), up to about 100 .ANG. and preferably in the range of about 10-45 .ANG., so that the intercalate easily can be exfoliated into individual platelets. The intercalated complex can be combined with an organic liquid into a viscous carrier material, for delivery of the carrier material, or for delivery of an active compound; or the intercalated complex can be combined with a matrix polymer to form a strong, filled polymer matrix. Alternatively, the intercalated complex can be exfoliated prior to or after combination with the organic liquid or the matrix polymer.

    摘要翻译： 通过使分层材料例如页硅酸盐与具有羟基和/或芳环官能团的嵌入剂单体接触形成的嵌入体，以在分层材料的相邻片晶之间吸附或插入插入剂单体。 在相邻的血小板之间吸附足够的嵌入剂单体以将相邻的血小板膨胀至至少约5 ANGSTROM（水除去后测量到最多5％（重量）水）的间隔，最高达约100安培，最好在 约10-45安士，使得插入物容易被剥离成单独的血小板。 插入的复合物可以与有机液体结合成粘性载体材料，用于递送载体材料或递送活性化合物; 或者插层的复合物可以与基质聚合物组合以形成强的，填充的聚合物基质。 或者，插入的复合物可以在与有机液体或基质聚合物组合之前或之后剥离。