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公开(公告)号：US20110239901A1
公开(公告)日：2011-10-06
申请号：US13075084
申请日：2011-03-29
申请人： Shinnosuke Koji , Kazumichi Nakahama , Shoji Koike
发明人： Shinnosuke Koji , Kazumichi Nakahama , Shoji Koike
IPC分类号： C09D11/02
CPC分类号： C09B67/0086 , B82Y30/00 , C09B67/0005 , C09B67/0096 , C09D11/023 , C09D11/328
摘要： The present invention provides coloring particles containing a dye and a water-insoluble low-molecular-weight dispersant, wherein the average particle size of the coloring particles is 10 nm or more and 80 nm or less; the solubility parameter of the dye in water with a pH of 6.0 to 10.0 is 9.20 or more, the solubility parameter being represented by formula (1); and the content of the dye and the content of the water-insoluble low-molecular-weight dispersant satisfy a relationship of formula (2).
摘要翻译： 本发明提供了含有染料和水不溶性低分子量分散剂的着色颗粒，其中着色颗粒的平均粒径为10nm以上且80nm以下， 该染料在pH为6.0〜10.0的水中的溶解度参数为9.20以上，溶解度参数由式（1）表示; 并且染料的含量和水不溶性低分子量分散剂的含量满足式（2）的关系。
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公开(公告)号：US08262791B2
公开(公告)日：2012-09-11
申请号：US13075084
申请日：2011-03-29
申请人： Shinnosuke Koji , Kazumichi Nakahama , Shoji Koike
发明人： Shinnosuke Koji , Kazumichi Nakahama , Shoji Koike
CPC分类号： C09B67/0086 , B82Y30/00 , C09B67/0005 , C09B67/0096 , C09D11/023 , C09D11/328
摘要： The present invention provides coloring particles containing a dye and a water-insoluble low-molecular-weight dispersant, wherein the average particle size of the coloring particles is 10 nm or more and 80 nm or less; the solubility parameter of the dye in water with a pH of 6.0 to 10.0 is 9.20 or more, the solubility parameter being represented by formula (1); and the content of the dye and the content of the water-insoluble low-molecular-weight dispersant satisfy a relationship of formula (2).
摘要翻译： 本发明提供了含有染料和水不溶性低分子量分散剂的着色颗粒，其中着色颗粒的平均粒径为10nm以上且80nm以下， 该染料在pH为6.0〜10.0的水中的溶解度参数为9.20以上，溶解度参数由式（1）表示; 并且染料的含量和水不溶性低分子量分散剂的含量满足式（2）的关系。
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公开(公告)号：US20120252974A1
公开(公告)日：2012-10-04
申请号：US13432155
申请日：2012-03-28
IPC分类号： C08G63/91
CPC分类号： C08F2/18
摘要： A method for producing polymer particles includes a preparation step for preparing a first oily liquid containing an oily olefin monomer, a radical polymerization initiator, and an iodine molecule, a synthesis step for obtaining a second oily liquid containing at least an iodine compound produced by a reaction between a radical generated by cleavage of the radical polymerization initiator and the iodine molecule in the first oily liquid, a suspension step for obtaining an oil droplet of the second oily liquid by suspending the second oily liquid in water, and a polymerization step for polymerizing the oily olefin monomer in the oil droplet.
摘要翻译： 制备聚合物颗粒的方法包括制备含有油性烯烃单体，自由基聚合引发剂和碘分子的第一油性液体的制备步骤，用于获得至少含有碘化合物的第二油性液体的合成步骤 通过自由基聚合引发剂的裂解和第一油性液体中的碘分子产生的自由基之间的反应，通过将第二油性液体悬浮在水中获得第二油性液体的油滴的悬浮液步骤和聚合步骤 油滴中的油状烯烃单体。
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4.发明申请MICROWAVE REACTOR AND METHOD OF PRODUCING POLYMER COMPOUND USING THE SAME 有权微波反应器及使用该聚合物的聚合物化合物的制造方法公开(公告)号：US20120048721A1
公开(公告)日：2012-03-01
申请号：US13214539
申请日：2011-08-22
IPC分类号： B01J19/12
CPC分类号： B01J19/126 , B01J19/18 , B01J2219/00063 , B01J2219/00078 , B01J2219/1215 , B01J2219/123 , B01J2219/1242 , B01J2219/1245 , B01J2219/126 , B01J2219/1293 , C08F2/46 , C08F12/08 , C08F120/06
摘要： Provided is a microwave reactor including a reaction container for receiving a reaction solution, a microwave radiator for irradiating the reaction solution received in the reaction container with microwaves, and a cooler for cooling the reaction solution received in the reaction container, wherein a heat-generating medium generating heat by absorbing the microwaves is arranged on a surface of the cooler or in the vicinity of the surface at a position receiving the microwaves from the microwave radiator through the reaction solution.
摘要翻译： 本发明提供一种微波反应器，其包括用于接收反应溶液的反应容器，用微波照射容纳在反应容器中的反应溶液的微波辐射器，以及用于冷却接收在反应容器中的反应溶液的冷却器，其中发热 通过吸收微波产生热量的介质通过反应溶液布置在冷却器的表面或表面附近，通过微波辐射器接收微波的位置。
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公开(公告)号：US20120277390A1
公开(公告)日：2012-11-01
申请号：US13453196
申请日：2012-04-23
IPC分类号： C08F4/04
CPC分类号： C08F2/18 , C08F2/38 , C08F112/08 , C08F120/14 , C08F212/08 , C08F220/14
摘要： A method for producing polymer particles includes a suspension step of suspending a first liquid mixture containing an oily olefin monomer, a radical polymerization initiator, and an iodine molecule in a second liquid mixture containing water and an iodide ion to prepare a suspension containing an oil droplet having the first liquid mixture; a synthesis step of synthesizing an iodine compound by allowing a radical generated by cleavage of the radical polymerization initiator to react with the iodine molecule in the oil droplet; and a polymerization step of polymerizing the oily olefin monomer in the oil droplet.
摘要翻译： 制备聚合物颗粒的方法包括将含有油性烯烃单体，自由基聚合引发剂和碘分子的第一液体混合物悬浮在含有水和碘离子的第二液体混合物中以制备含有油滴的悬浮液的悬浮步骤 具有第一液体混合物; 通过使自由基聚合引发剂的裂解产生的自由基与油滴中的碘分子反应来合成碘化合物的合成步骤; 以及在油滴中聚合油性烯烃单体的聚合步骤。
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公开(公告)号：US08993696B2
公开(公告)日：2015-03-31
申请号：US13453196
申请日：2012-04-23
IPC分类号： C08F4/04 , C08F2/18 , C08F2/38 , C08F112/08 , C08F120/14 , C08F212/08 , C08F220/14
CPC分类号： C08F2/18 , C08F2/38 , C08F112/08 , C08F120/14 , C08F212/08 , C08F220/14
摘要： A method for producing polymer particles includes a suspension step of suspending a first liquid mixture containing an oily olefin monomer, a radical polymerization initiator, and an iodine molecule in a second liquid mixture containing water and an iodide ion to prepare a suspension containing an oil droplet having the first liquid mixture; a synthesis step of synthesizing an iodine compound by allowing a radical generated by cleavage of the radical polymerization initiator to react with the iodine molecule in the oil droplet; and a polymerization step of polymerizing the oily olefin monomer in the oil droplet.
摘要翻译： 制备聚合物颗粒的方法包括将含有油性烯烃单体，自由基聚合引发剂和碘分子的第一液体混合物悬浮在含有水和碘离子的第二液体混合物中以制备含有油滴的悬浮液的悬浮步骤 具有第一液体混合物; 通过使自由基聚合引发剂的裂解产生的自由基与油滴中的碘分子反应来合成碘化合物的合成步骤; 以及在油滴中聚合油性烯烃单体的聚合步骤。
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公开(公告)号：US08969499B2
公开(公告)日：2015-03-03
申请号：US13494789
申请日：2012-06-12
IPC分类号： C08F2/18 , C08F2/32 , C08F2/38 , C08F2/40 , C08F212/08
CPC分类号： C08F2/32 , C08F2/18 , C08F2/38 , C08F2/40 , C08F212/08 , C08F220/14
摘要： A method for producing polymer particles includes a preparation step for preparing a first oily liquid containing an oily olefin monomer, a radical polymerization initiator, and an iodine molecule; a synthesis step for obtaining a second oily liquid containing at least an iodine compound produced by a reaction between a radical generated by cleavage of the radical polymerization initiator and the iodine molecule in the first oily liquid; a suspension step for obtaining an oil droplet of the second oily liquid by suspending the second oily liquid in an aqueous solution containing an oxidizing agent, an acid, and a dispersant; and a polymerization step for polymerizing the oily olefin monomer in the oil droplet.
摘要翻译： 制备聚合物颗粒的方法包括制备含有油性烯烃单体，自由基聚合引发剂和碘分子的第一油性液体的制备步骤; 一种合成步骤，用于获得含有至少一种通过自由基聚合引发剂裂解产生的自由基与第一油性液体中的碘分子之间的反应产生的至少一种碘化合物的油性液体; 用于通过将第二油性液体悬浮在含有氧化剂，酸和分散剂的水溶液中来获得第二油性液体的油滴的悬浮步骤; 以及用于在油滴中聚合油性烯烃单体的聚合步骤。
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公开(公告)号：US08946354B2
公开(公告)日：2015-02-03
申请号：US13432155
申请日：2012-03-28
CPC分类号： C08F2/18
摘要： A method for producing polymer particles includes a preparation step for preparing a first oily liquid containing an oily olefin monomer, a radical polymerization initiator, and an iodine molecule, a synthesis step for obtaining a second oily liquid containing at least an iodine compound produced by a reaction between a radical generated by cleavage of the radical polymerization initiator and the iodine molecule in the first oily liquid, a suspension step for obtaining an oil droplet of the second oily liquid by suspending the second oily liquid in water, and a polymerization step for polymerizing the oily olefin monomer in the oil droplet.
摘要翻译： 制备聚合物颗粒的方法包括制备含有油性烯烃单体，自由基聚合引发剂和碘分子的第一油性液体的制备步骤，用于获得至少含有碘化合物的第二油性液体的合成步骤 通过自由基聚合引发剂的裂解和第一油性液体中的碘分子产生的自由基之间的反应，通过将第二油性液体悬浮在水中获得第二油性液体的油滴的悬浮液步骤和聚合步骤 油滴中的油状烯烃单体。
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9.发明授权公开(公告)号：US08383053B2
公开(公告)日：2013-02-26
申请号：US13214539
申请日：2011-08-22
IPC分类号： B01J19/08
CPC分类号： B01J19/126 , B01J19/18 , B01J2219/00063 , B01J2219/00078 , B01J2219/1215 , B01J2219/123 , B01J2219/1242 , B01J2219/1245 , B01J2219/126 , B01J2219/1293 , C08F2/46 , C08F12/08 , C08F120/06
摘要： Provided is a microwave reactor including a reaction container for receiving a reaction solution, a microwave radiator for irradiating the reaction solution received in the reaction container with microwaves, and a cooler for cooling the reaction solution received in the reaction container, wherein a heat-generating medium generating heat by absorbing the microwaves is arranged on a surface of the cooler or in the vicinity of the surface at a position receiving the microwaves from the microwave radiator through the reaction solution.
摘要翻译： 本发明提供一种微波反应器，其包括用于接收反应溶液的反应容器，用微波照射容纳在反应容器中的反应溶液的微波辐射器，以及用于冷却接收在反应容器中的反应溶液的冷却器，其中发热 通过吸收微波产生热量的介质通过反应溶液布置在冷却器的表面或表面附近，通过微波辐射器接收微波的位置。
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公开(公告)号：US20120322965A1
公开(公告)日：2012-12-20
申请号：US13494789
申请日：2012-06-12
IPC分类号： C08F2/32 , C08F112/08 , C08F222/12
CPC分类号： C08F2/32 , C08F2/18 , C08F2/38 , C08F2/40 , C08F212/08 , C08F220/14
摘要： A method for producing polymer particles includes a preparation step for preparing a first oily liquid containing an oily olefin monomer, a radical polymerization initiator, and an iodine molecule; a synthesis step for obtaining a second oily liquid containing at least an iodine compound produced by a reaction between a radical generated by cleavage of the radical polymerization initiator and the iodine molecule in the first oily liquid; a suspension step for obtaining an oil droplet of the second oily liquid by suspending the second oily liquid in an aqueous solution containing an oxidizing agent, an acid, and a dispersant; and a polymerization step for polymerizing the oily olefin monomer in the oil droplet.
摘要翻译： 制备聚合物颗粒的方法包括制备含有油性烯烃单体，自由基聚合引发剂和碘分子的第一油性液体的制备步骤; 一种合成步骤，用于获得含有至少一种通过自由基聚合引发剂裂解产生的自由基与第一油性液体中的碘分子之间的反应产生的至少一种碘化合物的油性液体; 用于通过将第二油性液体悬浮在含有氧化剂，酸和分散剂的水溶液中来获得第二油性液体的油滴的悬浮步骤; 以及用于在油滴中聚合油性烯烃单体的聚合步骤。
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