公开(公告)号：US09233849B2

公开(公告)日：2016-01-12

申请号：US13985915

申请日：2012-02-28

申请人： Shiro Tsubokura ,  Toru Suzuki ,  Michiaki Maruyama ,  Yasuyuki Aiura

发明人： Shiro Tsubokura ,  Toru Suzuki ,  Michiaki Maruyama ,  Yasuyuki Aiura

IPC分类号： C07C303/40 ,  C01B21/087 ,  C01B21/093 ,  C01B21/086

CPC分类号： C01B21/086 ,  C01B21/087 ,  C01B21/093 ,  C07C303/40 ,  C07C311/48

摘要： By reacting a fluorine-containing sulfonylimide ammonium salt such as ammonium N,N-di(fluorosulfonyl)imide with an alkali metal hydroxide such as lithium hydroxide, potassium hydroxide or sodium hydroxide under reduced pressure and at a low temperature of approximately 40° C., a fluorine-containing sulfonylimide alkali metal salt such as lithium N,N-di(fluorosulfonyl)imide, potassium N,N-di(fluorosulfonyl)imide or sodium N,N-di(fluorosulfonyl)imide is obtained.

摘要翻译： 使N，N-二（氟磺酰基）酰亚胺铵等含氟磺酰亚胺铵盐与碱金属氢氧化物如氢氧化锂，氢氧化钾或氢氧化钠在减压下和约40℃的低温下反应。 得到N，N-二（氟磺酰基）酰亚胺锂，N，N-二（氟磺酰基）酰亚胺钾，N，N-二（氟磺酰基）酰亚胺钠等含氟磺酰亚胺碱金属盐。

公开(公告)号：US09096502B2

公开(公告)日：2015-08-04

申请号：US14001547

申请日：2012-02-24

申请人： Shiro Tsubokura ,  Yasuyuki Aiura ,  Toru Suzuki ,  Michiaki Maruyama

发明人： Shiro Tsubokura ,  Yasuyuki Aiura ,  Toru Suzuki ,  Michiaki Maruyama

IPC分类号： C07C311/48 ,  C07C303/40 ,  C01B21/093 ,  H01M10/052 ,  H01M10/0568 ,  C01B21/092

CPC分类号： C07C311/48 ,  C01B21/0923 ,  C01B21/093 ,  C07C303/40 ,  H01M10/052 ,  H01M10/0568 ,  Y02E60/122 ,  Y02P70/54

摘要： A compound [II] such as ammonium N,N-di(fluorosulfonyl)imide is obtained by reacting a compound [I] such as N,N-di(chlorosulfonyl)imide and NH4F (HF)p. A compound [IV] such as an N,N-di(fluorosulfonyl)imide alkali metal salt is obtained by reacting the obtained compound [II] and an alkali metal compound or the like.

摘要翻译： 通过使诸如N，N-二（氯磺酰基）酰亚胺和NH 4 F（HF）p的化合物[I]与N，N-二（氟磺酰基）酰亚胺铵形成化合物[II]。 通过使所得化合物[II]与碱金属化合物等反应，得到N，N-二（氟磺酰基）酰亚胺碱金属盐等化合物[Ⅳ]。

公开(公告)号：US20130331609A1

公开(公告)日：2013-12-12

申请号：US14001547

申请日：2012-02-24

申请人： Shiro Tsubokura ,  Yasuyuki Aiura ,  Toru Suzuki ,  Michiaki Maruyama

发明人： Shiro Tsubokura ,  Yasuyuki Aiura ,  Toru Suzuki ,  Michiaki Maruyama

IPC分类号： C07C311/48

CPC分类号： C07C311/48 ,  C01B21/0923 ,  C01B21/093 ,  C07C303/40 ,  H01M10/052 ,  H01M10/0568 ,  Y02E60/122 ,  Y02P70/54

摘要： A compound [II] such as ammonium N,N-di(fluorosulfonyl)imide is obtained by reacting a compound [I] such as N,N-di(chlorosulfonyl)imide and NH4F (HF)p. A compound [IV] such as an N,N-di(fluorosulfonyl)imide alkali metal salt is obtained by reacting the obtained compound [II] and an alkali metal compound or the like.

摘要翻译： 通过使诸如N，N-二（氯磺酰基）酰亚胺和NH 4 F（HF）p的化合物[I]与N，N-二（氟磺酰基）酰亚胺铵形成化合物[II]。 通过使所得化合物[II]与碱金属化合物等反应，得到N，N-二（氟磺酰基）酰亚胺碱金属盐等化合物[Ⅳ]。

公开(公告)号：US20130323155A1

公开(公告)日：2013-12-05

申请号：US13985915

申请日：2012-02-28

申请人： Shiro Tsubokura ,  Toru Suzuki ,  Michiaki Maruyama ,  Yasuyuki Aiura

发明人： Shiro Tsubokura ,  Toru Suzuki ,  Michiaki Maruyama ,  Yasuyuki Aiura

IPC分类号： C01B21/086

CPC分类号： C01B21/086 ,  C01B21/087 ,  C01B21/093 ,  C07C303/40 ,  C07C311/48

摘要： By reacting a fluorine-containing sulfonylimide ammonium salt such as ammonium N,N-di(fluorosulfonyl)imide with an alkali metal hydroxide such as lithium hydroxide, potassium hydroxide or sodium hydroxide under reduced pressure and at a low temperature of approximately 40° C., a fluorine-containing sulfonylimide alkali metal salt such as lithium N,N-di(fluorosulfonyl)imide, potassium N,N-di(fluorosulfonyl)imide or sodium N,N-di(fluorosulfonyl)imide is obtained.

摘要翻译： 使N，N-二（氟磺酰基）酰亚胺铵等含氟磺酰亚胺铵盐与碱金属氢氧化物如氢氧化锂，氢氧化钾或氢氧化钠在减压下和约40℃的低温下反应。 得到N，N-二（氟磺酰基）酰亚胺锂，N，N-二（氟磺酰基）酰亚胺钾，N，N-二（氟磺酰基）酰亚胺钠等含氟磺酰亚胺碱金属盐。