Method for suspension-polymerizing vinyl chloride
    1.
    发明授权
    Method for suspension-polymerizing vinyl chloride 失效
    悬浮聚合氯乙烯的方法

    公开(公告)号:US4136242A

    公开(公告)日:1979-01-23

    申请号:US788256

    申请日:1977-04-18

    IPC分类号: C08F14/06 C08F2/20 C08F114/06

    CPC分类号: C08F14/06

    摘要: A polymerization vessel equipped with a condenser is charged with vinyl chloride, a suspending agent or dispersing agent, and water. The mixture is subjected to a preparatory stirring in the absence of a catalyst. The polymerization catalyst is added thereto when bubbling caused by the preparatory stirring subsides and stable suspended oil drops form. Blockage of the condenser by polymer scale deposition is substantially reduced. The addition of an alkaline substance, an oxidizing substance or an azine dye further reduces polymer scale deposition. Preferably the operation of the condenser is initiated only after the conversion rate is higher than 5% or the average value per unit hour.

    Method of preparing vinyl chloride resins
    2.
    发明授权
    Method of preparing vinyl chloride resins 失效
    制备氯乙烯树脂的方法

    公开(公告)号:US4029619A

    公开(公告)日:1977-06-14

    申请号:US312306

    申请日:1972-12-05

    IPC分类号: C08F14/00 C08F2/26 C08F14/06

    CPC分类号: C08F14/06 Y10S526/911

    摘要: Vinyl chloride monomer is polymerized in aqueous medium under the influence of oil soluble polymerization initiators in the presence of alkali metal salts of higher fatty acid, higher alcohols and/or higher fatty acids, and hydroxides of alkali metals in certain amounts respectively, to produce vinyl chloride resin, stable for making resin/plasticizer pastes, mostly composed of particles having diameters lying between 0.1 and 2 microns. The resins are suitable for making resin/plasticizer pastes that have a low initial viscosity, little change in viscosities during storage, good thermal stability and excellent degassing property. Reduced deposition of polymer scales on the walls of the polymerization vessels was successful.

    摘要翻译: 氯乙烯单体在水溶性介质中在油溶性聚合引发剂的影响下,在高级脂肪酸,高级醇和/或高级脂肪酸的碱金属盐和碱金属的氢氧化物存在下分别聚合,生成乙烯基 氯化物树脂,对于制备树脂/增塑剂浆料是稳定的,主要由直径在0.1和2微米之间的颗粒组成。 这些树脂适用于制造具有低初始粘度,储存期间粘度变化小,热稳定性好,脱气性好的树脂/增塑剂糊剂。 在聚合容器的壁上减少聚合物垢的沉积是成功的。

    Alloys suitable for hydrogen storage, method of producing the same and
electrode using the same
    3.
    发明授权
    Alloys suitable for hydrogen storage, method of producing the same and electrode using the same 失效
    适合于氢存储的合金,其制备方法和使用其的电极

    公开(公告)号:US5578266A

    公开(公告)日:1996-11-26

    申请号:US308327

    申请日:1994-09-19

    摘要: Disclosed are a hydrogen storage alloy which contains carbon in a proportion of from 30 to 500 ppm and is represented by the stoichiometric formula A.sub.x B.sub.5.0, wherein A is La or a mixture of La with at least one rare earth metal other than La, B is at least one metal selected from a group consisting of Al, Co, Cr, Cu, Fe, Mn, Ni, Ti, V, Zn and Zr, and x is a rational number in the range 0.95.ltoreq..times..ltoreq.1.00; and has a texture in which only the intermetallic compound phase named AB.sub.5 phase is present and every other intermetallic compound phase is absent: and a method of producing said alloy and an electrode using the same.

    摘要翻译: 公开了一种储氢合金,其含有比例为30-500ppm的碳并由化学计量式AxB5.0表示,其中A是La或La与除La,B之外的至少一种稀土金属的混合物 是选自Al,Co,Cr,Cu,Fe,Mn,Ni,Ti,V,Zn和Zr中的至少一种金属,x是0.95≤x≤0.0的范围内的有理数。 1.00; 并且具有仅存在名称为AB5相的金属间化合物相的结构,并且不存在每隔一个金属间化合物相;以及使用其制造所述合金的方法和使用该金属间化合物相的电极。