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    Reversible hydrogen storage materials
    2.
    发明授权
    Reversible hydrogen storage materials 失效
    可逆储氢材料

    公开(公告)号：US08153554B2

    公开(公告)日：2012-04-10

    申请号：US11940651

    申请日：2007-11-15

    申请人： James A. Ritter ,  Tao Wang ,  Armin D. Ebner ,  Charles E. Holland

    发明人： James A. Ritter ,  Tao Wang ,  Armin D. Ebner ,  Charles E. Holland

    IPC分类号： C01B6/24 ,  C01B3/10 ,  B01J20/04

    CPC分类号： B01J20/0248 ,  B01J20/04 ,  B82Y30/00 ,  Y10S420/90

    摘要： In accordance with the present disclosure, a process for synthesis of a complex hydride material for hydrogen storage is provided. The process includes mixing a borohydride with at least one additive agent and at least one catalyst and heating the mixture at a temperature of less than about 600° C. and a pressure of H2 gas to form a complex hydride material. The complex hydride material comprises MAlxByHz, wherein M is an alkali metal or group IIA metal, Al is the element aluminum, x is any number from 0 to 1, B is the element boron, y is a number from 0 to 13, and z is a number from 4 to 57 with the additive agent and catalyst still being present. The complex hydride material is capable of cyclic dehydrogenation and rehydrogenation and has a hydrogen capacity of at least about 4 weight percent.

    摘要翻译： 根据本公开，提供了用于合成氢存储的复合氢化物材料的方法。 该方法包括将硼氢化钠与至少一种添加剂和至少一种催化剂混合，并在小于约600℃的温度和H 2气体的压力下加热混合物以形成复合氢化物材料。 复合氢化物材料包括MAlxByHZ，其中M是碱金属或IIA族金属，Al是元素铝，x是0至1的任何数，B是元素硼，y是0至13的数，z 是从4到57的数字，添加剂和催化剂仍然存在。 复合氢化物材料能够进行环状脱氢和再氢化并具有至少约4重量％的氢容量。

    Hydrogen storage materials
    3.
    发明授权
    Hydrogen storage materials 有权
    储氢材料

    公开(公告)号：US08079464B2

    公开(公告)日：2011-12-20

    申请号：US12981605

    申请日：2010-12-30

    申请人： Jun Yang ,  Andrea Pulskamp ,  Shinichi Hirano

    发明人： Jun Yang ,  Andrea Pulskamp ,  Shinichi Hirano

    IPC分类号： C01B3/08 ,  B01J20/02

    CPC分类号： C01B3/0078 ,  C01B3/0015 ,  C01B3/0031 ,  C01B3/0036 ,  C01B3/0057 ,  Y02E60/327 ,  Y02E60/328 ,  Y02E60/36 ,  Y10S420/90

    摘要： In one embodiment, a hydrogen storage system includes a core of hydrogen sorbent material and a shell of crystalline metal hydride material enclosing at least a portion of the core of hydrogen sorbent material. In another embodiment, the hydrogen storage system further includes an intermediate layer of amorphous metal hydride material, at least a portion of which being positioned between the core of hydrogen sorbent material and the shell of crystalline metal hydride material.

    摘要翻译： 在一个实施方案中，氢存储系统包括氢吸附剂材料的核心和包围氢吸附剂材料芯的至少一部分的结晶金属氢化物材料的壳。 在另一个实施方案中，氢存储系统还包括无定形金属氢化物材料的中间层，其至少一部分位于氢吸附剂材料的核心和结晶金属氢化物材料的壳体之间。

    XLI2MGHN hydrides as hydrogen storage compounds
    4.
    发明授权
    XLI2MGHN hydrides as hydrogen storage compounds 失效
    XLI2MGHN氢化物作为储氢化合物

    公开(公告)号：US08071064B2

    公开(公告)日：2011-12-06

    申请号：US12581209

    申请日：2009-10-19

    申请人： Jan F. Herbst ,  Martin S. Meyer ,  James R. Salvador

    发明人： Jan F. Herbst ,  Martin S. Meyer ,  James R. Salvador

    IPC分类号： C01B6/24 ,  C01F17/00

    CPC分类号： C01B6/24 ,  C01B3/0031 ,  Y02E60/327 ,  Y10S420/90

    摘要： State-of-the-art electronic structure calculations yield results consistent with the observed compound SiLi2Mg and provide likelihood of the availability of IrLi2Mg and RhLi2Mg. Similar calculations provide likelihood of the availability of YLi2MgHn, ZrLi2MgHn, NbLi2MgHn, MoLi2MgHn, TcLi2MgHn, RuLi2MgHn, RhLi2MgHn, LaLi2MgHn, Ce4+Li2MgHn, Ce3+Li2MgHn, PrLi2MgHn, NdLi2MgHn, PmLi2MgHn, SmLi2MgHn, EuLi2MgHn, GdLi2MgHn, TbLi2MgHn, DyLi2MgHn, HoLi2MgHn, ErLi2MgHn, TmLi2MgHn, YbLi2MgHn, LuLi2MgHn, HfLi2MgHn, TaLi2MgHn, ReLi2MgHn, OsLi2MgHn, and IrLi2MgHn (here n is an integer having a value in a particular compound of 4-7) as solid hydrides for the storage and release of hydrogen. Different hydrogen contents may be obtained in compounds having the same XLi2Mg crystal structures. These materials offer utility for hydrogen storage systems.

    摘要翻译： 最先进的电子结构计算产生与观察到的化合物SiLi2Mg一致的结果，并提供IrLi2Mg和RhLi2Mg的可用性的可能性。 类似的计算提供YLi2MgHn，ZrLi2MgHn，NbLi2MgHn，MoLi2MgHn，TcLi2MgHn，RuLi2MgHn，RhLi2MgHn，LaLi2MgHn，四价铈Li2MgHn，Ce3 +的Li2MgHn，PrLi2MgHn，NdLi2MgHn，PmLi2MgHn，SmLi2MgHn，EuLi2MgHn，GdLi2MgHn，TbLi2MgHn，DyLi2MgHn，HoLi2MgHn的可用性的可能性， ErLi2MgHn，TmLi2MgHn，YbLi2MgHn，LuLi2MgHn，HfLi2MgHn，TaLi2MgHn，ReLi2MgHn，OsLi2MgHn和IrLi2MgHn（这里n是具有4-7的特定化合物中的值的整数）作为氢的储存和释放的固体氢化物。 在具有相同XLi2Mg晶体结构的化合物中可以获得不同的氢含量。 这些材料为氢存储系统提供实用性。

    XLi2MgHn hydrides as hydrogen storage compounds
    5.
    发明授权
    XLi2MgHn hydrides as hydrogen storage compounds 有权
    XLi2MgHn氢化物作为储氢化合物

    公开(公告)号：US07968071B2

    公开(公告)日：2011-06-28

    申请号：US12539639

    申请日：2009-08-12

    申请人： Jan F. Herbst

    发明人： Jan F. Herbst

    IPC分类号： C01B6/24 ,  C01F17/00

    CPC分类号： C01B6/246 ,  Y10S420/90

    摘要： State-of-the-art electronic structure calculations provide the likelihood of the availability of AlLi2MgHn, ScLi2MgHn, TiLi2MgHn, VLi2MgHn, CrLi2MgHn, MnLi2MgHn, FeLi2MgHn, CoLi2MgHn, NiLi2MgHn, CuLi2MgHn, ZnLi2MgHn, GaLi2MgHn, GeLi2MgHn, PdLi2MgHn, AgLi2MgHn, CdLi2MgHn, InLi2MgHn, SnLi2MgHn, SbLi2MgHn, PtLi2MgHn, AuLi2MgHn, HgLi2MgHn, TlLi2MgHn, PbLi2MgHn, and BiLi2MgHn (here n is an integer having a value in a particular compound of 4-7) as solid hydrides for the storage and release of hydrogen. Different hydrogen contents may be obtained in compounds having the same XLi2Mg crystal structures. These materials offer utility for hydrogen storage systems.

    摘要翻译： 状态的最先进的电子结构计算提供AlLi2MgHn，ScLi2MgHn，TiLi2MgHn，VLi2MgHn，CrLi2MgHn，MnLi2MgHn，FeLi2MgHn，CoLi2MgHn，NiLi2MgHn，CuLi2MgHn，ZnLi2MgHn，GaLi2MgHn，GeLi2MgHn，PdLi2MgHn，AgLi2MgHn，CdLi2MgHn，InLi2MgHn的可用性的可能性 ，SnLi2MgHn，SbLi2MgHn，PtLi2MgHn，AuLi2MgHn，HgLi2MgHn，TlLi2MgHn，PbLi2MgHn和BiLi2MgHn（这里n是具有4-7的特定化合物中的值的整数）作为氢的储存和释放的固体氢化物。 在具有相同XLi2Mg晶体结构的化合物中可以获得不同的氢含量。 这些材料为氢存储系统提供实用性。

    XLi2MgHn HYDRIDES AS HYDROGEN STORAGE COMPOUNDS
    7.
    发明申请
    XLi2MgHn HYDRIDES AS HYDROGEN STORAGE COMPOUNDS 有权
    XLi2MgHn氢化物作为氢储存化合物

    公开(公告)号：US20110038776A1

    公开(公告)日：2011-02-17

    申请号：US12539639

    申请日：2009-08-12

    申请人： Jan F. Herbst

    发明人： Jan F. Herbst

    IPC分类号： C01B6/24

    CPC分类号： C01B6/246 ,  Y10S420/90

    摘要： State-of-the-art electronic structure calculations provide the likelihood of the availability of AlLi2MgHn, ScLi2MgHn, TiLi2MgHn, VLi2MgHn, CrLi2MgHn, MnLi2MgHn, FeLi2MgHn, CoLi2MgHn, NiLi2MgHn, CuLi2MgHn, ZnLi2MgHn, GaLi2MgHn, GeLi2MgHn, PdLi2MgHn, AgLi2MgHn, CdLi2MgHn, InLi2MgHn, SnLi2MgHn, SbLi2MgHn, PtLi2MgHn, AuLi2MgHn, HgLi2MgHn, TlLi2MgHn, PbLi2MgHn, and BiLi2MgHn (here n is an integer having a value in a particular compound of 4-7) as solid hydrides for the storage and release of hydrogen. Different hydrogen contents may be obtained in compounds having the same XLi2Mg crystal structures. These materials offer utility for hydrogen storage systems.

    摘要翻译： 状态的最先进的电子结构计算提供AlLi2MgHn，ScLi2MgHn，TiLi2MgHn，VLi2MgHn，CrLi2MgHn，MnLi2MgHn，FeLi2MgHn，CoLi2MgHn，NiLi2MgHn，CuLi2MgHn，ZnLi2MgHn，GaLi2MgHn，GeLi2MgHn，PdLi2MgHn，AgLi2MgHn，CdLi2MgHn，InLi2MgHn的可用性的可能性 ，SnLi2MgHn，SbLi2MgHn，PtLi2MgHn，AuLi2MgHn，HgLi2MgHn，TlLi2MgHn，PbLi2MgHn和BiLi2MgHn（这里n是具有4-7的特定化合物中的值的整数）作为氢的储存和释放的固体氢化物。 在具有相同XLi2Mg晶体结构的化合物中可以获得不同的氢含量。 这些材料为氢存储系统提供实用性。

    HYDROCARBON-SOLUBLE MOLYBDENUM CATALYST PRECURSORS AND METHODS FOR MAKING SAME
    10.
    发明申请
    HYDROCARBON-SOLUBLE MOLYBDENUM CATALYST PRECURSORS AND METHODS FOR MAKING SAME 有权
    碳氢化合物可溶性钼酸盐催化剂前体及其制备方法

    公开(公告)号：US20100051507A1

    公开(公告)日：2010-03-04

    申请号：US12616552

    申请日：2009-11-11

    申请人： ZHIHUA WU ,  Zhenhua Zhou ,  Bing Zhou

    发明人： ZHIHUA WU ,  Zhenhua Zhou ,  Bing Zhou

    IPC分类号： C10L1/24 ,  B01J31/02

    CPC分类号： C10G47/06 ,  B01J27/051 ,  B01J31/04 ,  B01J31/2226 ,  B01J2531/64 ,  B82Y30/00 ,  C01B3/0021 ,  C10G47/26 ,  C10G2300/4037 ,  C10G2300/70 ,  Y02E60/325 ,  Y10S420/90 ,  Y10S977/70 ,  Y10S977/84

    摘要： Hydrocarbon-soluble molybdenum catalyst precursors include a plurality of molybdenum cations that are each bonded with a plurality of organic anions to form an oil soluble molybdenum salt. A portion of the molybdenum atoms are in the 3+ oxidation state such that the plurality of molybdenum atoms has an average oxidation state of less than 4+, e.g., less than about 3.8+, especially less than about 3.5+. The catalyst precursors can form a hydroprocessing molybdenum sulfide catalyst in heavy oil feedstocks. The oil soluble molybdenum salts are manufactured in the presence of a reducing agent, such as hydrogen gas, to obtain the molybdenum in the desired oxidation state. Preferably the reaction is performed with hydrogen or an organic reducing agent and at a temperature such that the molybdenum atoms are reduced to eliminate substantially all molybdenum oxide species.

    摘要翻译： 烃可溶性钼催化剂前体包括多个钼阳离子，其各自与多个有机阴离子键合以形成油溶性钼盐。 一部分钼原子处于3+氧化态，使得多个钼原子具有小于4+，例如小于约3.8+，特别是小于约3.5+的平均氧化态。 催化剂前体可以在重油原料中形成加氢处理钼硫化物催化剂。 油溶性钼盐在还原剂如氢气存在下制备，得到所需氧化态的钼。 优选地，反应用氢或有机还原剂进行，并且在使得钼原子被还原以消除基本上所有氧化钼物质的温度下进行。