公开(公告)号：US08317503B2

公开(公告)日：2012-11-27

申请号：US12776737

申请日：2010-05-10

申请人： Stefan Zikeli ,  Michael Longin

发明人： Stefan Zikeli ,  Michael Longin

IPC分类号： B29C47/92 ,  D01D5/06 ,  D01F2/02

CPC分类号： D01F2/00 ,  B29C47/0014 ,  B29C47/8895 ,  B29C47/92 ,  B29C2947/92314 ,  B29C2947/92409 ,  B29C2947/92809 ,  B29C2947/92904 ,  C08B1/003 ,  D01D1/02 ,  D01D5/06

摘要： A device for producing Lyocell fibers which are extruded from a cellulose solution of water, cellulose and tertiary amine oxide in a spinning head (25). The cellulose solution is obtained in a number of process steps directly from the cellulose (3, 4) or with the formation of a cellulose suspension. Since the degree of polymerization decreases in the course of processing the cellulose through to its extrusion in the cellulose solution, with the processing of celluloses with a low degree of polymerization there is the risk that the endless molded bodies (2) extruded in the spinning head (25) exhibit defective quality. In order to also be able to process celluloses (3, 4) with a low degree of polymerization without having to accept reduced quality, according to the invention, the residence time of the cellulose from its introduction into the device (1) through to the extrusion of the cellulose (3, 4) in the cellulose solution is set in dependence of the degree of polymerization of the cellulose, of the cellulose suspension and/or of the cellulose solution.

摘要翻译： 一种用于生产从纺丝头（25）中的水，纤维素和叔胺氧化物的纤维素溶液挤出的莱赛尔纤维的装置。 纤维素溶液在直接由纤维素（3,4））或纤维素悬浮液的形成的多个工艺步骤中获得。 由于在将纤维素加工成在纤维素溶液中挤出的过程中聚合度降低，由于聚合度低的纤维素的加工存在在纺丝头中挤出的环形成型体（2）的风险 （25）品质不佳。 为了也能够以低聚合度处理纤维素（3,4），而不必接受质量降低，根据本发明，纤维素从其引入到装置（1）中的停留时间到达 依赖于纤维素，纤维素悬浮液和/或纤维素溶液的聚合度，将纤维素（3,4）挤出在纤维素溶液中。

公开(公告)号：US06644845B1

公开(公告)日：2003-11-11

申请号：US10182851

申请日：2002-10-07

申请人： Stefan Zikeli ,  Michael Longin ,  Friedrich Ecker

发明人： Stefan Zikeli ,  Michael Longin ,  Friedrich Ecker

IPC分类号： B01F1502

CPC分类号： B29C47/368 ,  B29C47/0009 ,  B29C47/54 ,  B29C47/92 ,  B29C2947/92514 ,  B29C2947/92952 ,  D01D1/06 ,  D01F2/00

摘要： The present invention relates to a buffer tank as is substantially used for ensuring a constant supply of the spinning machine with a polymer melt in spinning machines. To this end the buffer tank is provided with a compensation chamber whose volume is variable in response to a pressure prevailing in the polymer melt and to a volume flow variation. The polymer melt flows from a polymer melt entry opening to a polymer melt exit opening through the compensation chamber. It is the object of the present invention to make the flow through the compensation chamber uniform. The residence time of the polymer melt in the compensation chamber shall thereby be prevented from having a wide range, the latter resulting in an irregular quality of the yarns produced by the spinning machine because of the time-dependent, mechanical and chemical properties of the polymer melt. To achieve said object, the compensation chamber is provided for flow optimization with at least to one flow guiding element projecting into the flow of the polymer melt, which is smaller than the flow cross-section of the compensation chamber and by which the velocity profile in the direction of flow through the compensation chamber is made uniform at least in sections.

摘要翻译： 本发明涉及一种缓冲罐，其基本上用于确保纺丝机在纺丝机中恒定供应聚合物熔体。 为此，缓冲罐设置有补偿室，其补偿室的响应于聚合物熔体中存在的压力和体积流量变化而变化。 聚合物熔体从聚合物熔体入口通过补偿室流到聚合物熔体出口。 本发明的目的是使通过补偿室的流动均匀。 因此，防止聚合物熔体在补偿室中的停留时间范围很大，后者由于聚合物的时间依赖性，机械和化学性质而导致由纺丝机产生的纱线的不规则质量 熔化。 为了实现所述目的，补偿室被提供用于流动优化，其中至少一个流动引导元件突出到聚合物熔体的流动中，其小于补偿室的流动横截面，并且通过该补偿腔的速度分布 通过补偿室的流动方向至少在部分中是均匀的。

公开(公告)号：US5890504A

公开(公告)日：1999-04-06

申请号：US817809

申请日：1997-04-17

申请人： Stefan Zikeli ,  Klaus Weidinger ,  Friedrich Ecker ,  Michael Longin

发明人： Stefan Zikeli ,  Klaus Weidinger ,  Friedrich Ecker ,  Michael Longin

IPC分类号： F16K17/14 ,  F16K17/16

CPC分类号： F16K17/16 ,  Y10T137/0318 ,  Y10T137/1714 ,  Y10T137/2642

摘要： The invention is concerned with a process for transporting a thermally unstable viscous mass through a pipe having a predetermined breaking point to release excess pressure, which predetermined breaking point breaks when the excess pressure is reached, the excess pressure thus being released, and is characterized in that the predetermined breaking point is provided in the interior of the pipe, provided that the predetermined breaking point is not provided as a portion of the inner wall of the pipe.

摘要翻译： PCT No.PCT / AT96 / 00152 Sec。 371日期1997年04月17日 102（e）日期1997年4月17日PCT 1996年8月16日PCT公布。 出版物WO97 / 08482 日期1997年3月6日本发明涉及一种通过具有预定断裂点的管道输送热不稳定粘性物质以释放过压的方法，当达到过压时该预定断裂点断裂，从而释放过量压力 并且其特征在于，如果没有将预定的断裂点设置为管的内壁的一部分，则在管的内部设置预定的断裂点。

公开(公告)号：US20110224463A1

公开(公告)日：2011-09-15

申请号：US13128255

申请日：2009-11-10

申请人： Stefan Zikeli ,  Friedrich Ecker ,  Michael Longin ,  Klause Weidinger

发明人： Stefan Zikeli ,  Friedrich Ecker ,  Michael Longin ,  Klause Weidinger

IPC分类号： C07C205/06 ,  B01J19/00

CPC分类号： B01J19/0093 ,  B01J2219/00783 ,  B01J2219/0081 ,  B01J2219/00873 ,  B01J2219/00889

摘要： Modular microreactors are provided composed of microreactor parts including a plate body which has, on one plate side, a groove-shaped depression in which a reactor tube is accommodated, and the reaction tube has connection ends on the outer sides of the plate body. Also disclosed are reaction tubes for turbulent mixing, kits for producing the reactors and the use thereof for commencing chemical reactions.

摘要翻译： 模块化微反应器由微反应器部件组成，其包括板体，板体在一个板侧具有容纳反应器管的槽形凹部，反应管在板体的外侧具有连接端。 还公开了用于湍流混合的反应管，用于生产反应器的试剂盒及其用于开始化学反应的用途。

公开(公告)号：US20080048358A1

公开(公告)日：2008-02-28

申请号：US11569061

申请日：2005-02-28

申请人： Stefan Zikeli ,  Michael Longin

发明人： Stefan Zikeli ,  Michael Longin

IPC分类号： D01F2/24

CPC分类号： D01F2/00 ,  B29C48/05 ,  B29C48/919 ,  B29C48/92 ,  B29C2948/92314 ,  B29C2948/92409 ,  B29C2948/92809 ,  B29C2948/92904 ,  C08B1/003 ,  D01D1/02 ,  D01D5/06

摘要： The invention relates to a method and a device for producing Lyocell fibres which are extruded from a cellulose solution of water, cellulose and tertiary amine oxide in a spinning head (25). The cellulose solution is obtained in a number of process steps directly from the cellulose (3, 4) or with the formation of a cellulose suspension. Since the degree of polymerisation decreases in the course of processing the cellulose through to its extrusion in the cellulose solution, with the processing of celluloses with a low degree of polymerisation there is the risk that the endless moulded bodies (2) extruded in the spinning head (25) exhibit defective quality. In order to also be able to process celluloses (3, 4) with a low degree of polymerisation without having to accept reduced quality, according to the invention, the residence time of the cellulose from its introduction into the device (1) through to the extrusion of the cellulose (3, 4) in the cellulose solution is set in dependence of the degree of polymerisation of the cellulose, of the cellulose suspension and/or of the cellulose solution.

摘要翻译： 本发明涉及一种用于生产从纺丝头（25）中的水，纤维素和叔胺氧化物的纤维素溶液中挤出的莱赛尔纤维的方法和装置。 纤维素溶液在直接由纤维素（3,4））或纤维素悬浮液的形成的多个工艺步骤中获得。 由于在纤维素加工过程中纤维素在纤维素溶液中的挤出过程中聚合度降低，随着聚合度低的纤维素的加工，存在在纺丝头中挤出的环形成型体（2）的风险 （25）品质不佳。 为了也能够以低聚合度处理纤维素（3,4），而不必接受降低的质量，根据本发明，纤维素从其引入到装置（1）中的停留时间到达 依赖于纤维素，纤维素悬浮液和/或纤维素溶液的聚合度来设定纤维素（3,4）的纤维素溶液的挤出。

公开(公告)号：US09101903B2

公开(公告)日：2015-08-11

申请号：US13128255

申请日：2009-11-10

申请人： Stefan Zikeli ,  Friedrich Ecker ,  Michael Longin ,  Klaus Weidinger

发明人： Stefan Zikeli ,  Friedrich Ecker ,  Michael Longin ,  Klaus Weidinger

IPC分类号： B01J8/00 ,  B01J19/00

CPC分类号： B01J19/0093 ,  B01J2219/00783 ,  B01J2219/0081 ,  B01J2219/00873 ,  B01J2219/00889

摘要： Modular microreactors are provided composed of microreactor parts including a plate body which has, on one plate side, a groove-shaped depression in which a reactor tube is accommodated, and the reaction tube has connection ends on the outer sides of the plate body. Also disclosed are reaction tubes for turbulent mixing, kits for producing the reactors and the use thereof for commencing chemical reactions.

摘要翻译： 模块化微反应器由微反应器部件组成，其包括板体，板体在一个板侧具有容纳反应器管的凹槽状凹部，反应管在板体的外侧具有连接端。 还公开了用于湍流混合的反应管，用于生产反应器的试剂盒及其用于开始化学反应的用途。

公开(公告)号：US5794642A

公开(公告)日：1998-08-18

申请号：US814258

申请日：1997-03-10

申请人： Stefan Zikeli ,  Michael Longin ,  Friedrich Ecker

发明人： Stefan Zikeli ,  Michael Longin ,  Friedrich Ecker

IPC分类号： B29C41/34 ,  D01D1/06 ,  D01F2/00 ,  E03B1/00

CPC分类号： D01D1/06 ,  D01F2/00 ,  Y10T137/0335 ,  Y10T137/0391 ,  Y10T137/85938

摘要： The invention is concerned with a process for transporting a thermally unstable viscous mass through pipes and is characterized in that (a) during transportation, the mass is divided into X.sub.1 partial flows T.sub.1, X.sub.1 being calculated according to the relation X.sub.1 =Q.sup.(N-1), (I) wherein Q and N indicate positive integers independent from each other, and (b) the viscous mass in the partial flows is transported at the same rate.

摘要翻译： 本发明涉及通过管道输送热不稳定粘性物质的方法，其特征在于：（a）运输过程中，质量分为X1部分流T1，X1根据关系X 1 = Q（N-1 ），（I）其中Q和N表示彼此独立的正整数，和（b）部分流中的粘性质量以相同的速率运输。

公开(公告)号：US20100219547A1

公开(公告)日：2010-09-02

申请号：US12776737

申请日：2010-05-10

申请人： Stefan Zikeli ,  Michael Longin

发明人： Stefan Zikeli ,  Michael Longin

IPC分类号： B29C47/92 ,  B29C47/10

CPC分类号： D01F2/00 ,  B29C47/0014 ,  B29C47/8895 ,  B29C47/92 ,  B29C2947/92314 ,  B29C2947/92409 ,  B29C2947/92809 ,  B29C2947/92904 ,  C08B1/003 ,  D01D1/02 ,  D01D5/06

摘要： The invention relates to a method and a device for producing Lyocell fibres which are extruded from a cellulose solution of water, cellulose and tertiary amine oxide in a spinning head (25). The cellulose solution is obtained in a number of process steps directly from the cellulose (3, 4) or with the formation of a cellulose suspension. Since the degree of polymerisation decreases in the course of processing the cellulose through to its extrusion in the cellulose solution, with the processing of celluloses with a low degree of polymerisation there is the risk that the endless moulded bodies (2) extruded in the spinning head (25) exhibit defective quality. In order to also be able to process celluloses (3, 4) with a low degree of polymerisation without having to accept reduced quality, according to the invention, the residence time of the cellulose from its introduction into the device (1) through to the extrusion of the cellulose (3, 4) in the cellulose solution is set in dependence of the degree of polymerisation of the cellulose, of the cellulose suspension and/or of the cellulose solution.

摘要翻译： 本发明涉及一种用于生产从纺丝头（25）中的水，纤维素和叔胺氧化物的纤维素溶液中挤出的莱赛尔纤维的方法和装置。 纤维素溶液在直接由纤维素（3,4））或纤维素悬浮液的形成的多个工艺步骤中获得。 由于在纤维素加工过程中纤维素在纤维素溶液中的挤出过程中聚合度降低，随着聚合度低的纤维素的加工，存在在纺丝头中挤出的环形成型体（2）的风险 （25）品质不佳。 为了也能够以低聚合度处理纤维素（3,4），而不必接受降低的质量，根据本发明，纤维素从其引入到装置（1）中的停留时间到达 依赖于纤维素，纤维素悬浮液和/或纤维素溶液的聚合度来设定纤维素（3,4）的纤维素溶液的挤出。

公开(公告)号：US20080042309A1

公开(公告)日：2008-02-21

申请号：US11569058

申请日：2005-02-28

申请人： Stefan Zikeli ,  Werner Schumann ,  Lutz Glaser ,  Michael Longin

发明人： Stefan Zikeli ,  Werner Schumann ,  Lutz Glaser ,  Michael Longin

IPC分类号： B29C45/76 ,  D01F2/02

CPC分类号： D01F2/00 ,  D01D1/02 ,  D01D5/06

摘要： The invention relates to a method and a device (1) for the production of a cellulose solution, from which endless moulded bodies (2) can be extruded. First, a cellulose suspension is produced from cellulose (3, 4) and water (6) in a pulper (5). The cellulose suspension is then expressed by a press device (10). After expressing, a tertiary amine oxide, in particular N-methylmorpholine-N-oxide, is fed as a solvent to the cellulose suspension, thus producing a cellulose solution. The efficiency of the method and the device and their environmental compatibility can be improved in that the press water (11) expressed by the press device (10) is at least in part fed back to the pulper (5). In a further development the proportion of the press water (15) in the water (6) is varied depending on the metal content of the cellulose (3, 4) and/or of the cellulose solution.

摘要翻译： 本发明涉及一种用于生产纤维素溶液的方法和装置（1），可从中挤出环形模制体（2）。 首先，在碎浆机（5）中由纤维素（3,4）和水（6）生产纤维素悬浮液。 然后由压制装置（10）表示纤维素悬浮液。 表达后，将叔胺氧化物，特别是N-甲基吗啉-N-氧化物作为溶剂加入到纤维素悬浮液中，从而制备纤维素溶液。 可以提高方法和装置的效率及其环境兼容性，因为由压力装置（10）表达的压力水（11）至少部分地被反馈到碎浆机（5）。 在进一步的发展中，水（6）中的压榨水（15）的比例根据纤维素（3,4）和/或纤维素溶液的金属含量而变化。

公开(公告)号：US20070210481A1

公开(公告)日：2007-09-13

申请号：US11569056

申请日：2005-03-01

申请人： Stefan Zikeli ,  Werner Schumann ,  Lutz Glaser ,  Michael Longin

发明人： Stefan Zikeli ,  Werner Schumann ,  Lutz Glaser ,  Michael Longin

IPC分类号： D01D5/06 ,  D01F2/02

CPC分类号： D01F2/00 ,  D01D1/02 ,  D01D13/02

摘要： The invention relates to a method and a device for producing Lyocell fibers, which are extruded from a spinning mass containing water, cellulose and tertiary amine oxide. The spinning mass is obtained from cellulose in a number of process steps, wherein a treatment medium is added to the cellulose, cellulose suspension and/or cellulose solution. In order to be able to implement a stable and environmentally compatible spinning method irrespective of the type of cellulose used, according to the invention, provision is made that the content of at least one type of metal ion destabilising the cellulose suspension and/or cellulose solution is monitored in the cellulose, cellulose suspension and/or cellulose solution and adjusted below a stability limit. With the device according to the invention, the metal ion content is measured via sensors (23, 23′) and the metal ion content is adjusted using a control device (17).

摘要翻译： 本发明涉及从含有水，纤维素和叔胺氧化物的纺丝组织挤出的用于生产Lyocell纤维的方法和装置。 纺丝物质在多个工艺步骤中由纤维素获得，其中将处理介质加入到纤维素，纤维素悬浮液和/或纤维素溶液中。 为了能够实现与所使用的纤维素类型无关的稳定和环境友好的纺丝方法，根据本发明，规定使至少一种类型的金属离子的含量使纤维素悬浮液和/或纤维素溶液不稳定 在纤维素，纤维素悬浮液和/或纤维素溶液中进行监测，并调节到稳定极限以下。 利用根据本发明的装置，通过传感器（23,23'）测量金属离子含量，并且使用控制装置（17）调节金属离子含量。