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    PROCESS FOR PRODUCING ETHYLENE GLYCOL CATALYZED BY IONIC LIQUID
    1.
    发明申请
    PROCESS FOR PRODUCING ETHYLENE GLYCOL CATALYZED BY IONIC LIQUID 有权
    生产由离子液体催化的乙烯甘油的方法

    公开(公告)号：US20130072727A1

    公开(公告)日：2013-03-21

    申请号：US13520008

    申请日：2010-06-07

    申请人： Suojiang Zhang ,  Jian Sun ,  Weiguo Cheng ,  Jinquan Wang ,  Jianxin Zhang ,  Zengzeng Fu ,  Ziangping Zhang

    发明人： Suojiang Zhang ,  Jian Sun ,  Weiguo Cheng ,  Jinquan Wang ,  Jianxin Zhang ,  Zengzeng Fu ,  Ziangping Zhang

    IPC分类号： C07C27/02

    CPC分类号： C07C29/106 ,  C07C29/12 ,  Y02P20/52 ,  C07C31/202

    摘要： Disclosed is a process for producing ethylene glycol catalyzed by an ionic liquid, characterized in that the process includes the following three steps: (a) a carbonylation step of ethylene oxide and CO2 catalyzed by an ionic liquid composite catalyst comprising a hydroxyl functionalized ionic liquid and an alkali metal salt under an aqueous condition to produce ethylene carbonate and ethylene glycol; (b) a hydrolysis step of reacting the reaction solution containing ethylene carbonate and the ionic liquid composite catalyst obtained in step (a) with water to produce ethylene glycol; (c) a purification step of dehydrating and refining ethylene glycol from the aqueous solution containing ethylene glycol and the catalyst produced in step (b). The present process has the following advantages: the catalyst has high activity, high suitability, and good stability, the reaction condition is wild, the conversion of ethylene oxide is high, the selectivity of ethylene glycol is high, and the process is simple.

    摘要翻译： 公开了一种由离子液体催化的生产乙二醇的方法，其特征在于该方法包括以下三个步骤：（a）由包含羟基官能化的离子液体的离子液体复合催化剂催化的环氧乙烷和CO 2的羰基化步骤，和 在水溶液条件下制备碱金属盐以制备碳酸亚乙酯和乙二醇; （b）使含有碳酸亚乙酯的反应溶液和步骤（a）中得到的离子液体复合催化剂与水反应以产生乙二醇的水解步骤; （c）从含有乙二醇的水溶液和步骤（b）中制备的催化剂中脱水和精制乙二醇的纯化步骤。 本方法具有以下优点：催化剂活性高，适用性好，稳定性好，反应条件野生，环氧乙烷转化率高，乙二醇选择性高，工艺简单。

    Process for producing ethylene glycol catalyzed by ionic liquid
    2.
    发明授权
    Process for producing ethylene glycol catalyzed by ionic liquid 有权
    由离子液体催化生产乙二醇的方法

    公开(公告)号：US08658842B2

    公开(公告)日：2014-02-25

    申请号：US13520008

    申请日：2010-06-07

    申请人： Suojiang Zhang ,  Jian Sun ,  Weiguo Cheng ,  Jinquan Wang ,  Jianxin Zhang ,  Zengzeng Fu ,  Xiangping Zhang

    发明人： Suojiang Zhang ,  Jian Sun ,  Weiguo Cheng ,  Jinquan Wang ,  Jianxin Zhang ,  Zengzeng Fu ,  Xiangping Zhang

    IPC分类号： C07C29/09

    CPC分类号： C07C29/106 ,  C07C29/12 ,  Y02P20/52 ,  C07C31/202

    摘要： Disclosed is a process for producing ethylene glycol catalyzed by an ionic liquid, characterized in that the process includes the following three steps: (a) a carbonylation step of ethylene oxide and CO2 catalyzed by an ionic liquid composite catalyst comprising a hydroxyl functionalized ionic liquid and an alkali metal salt under an aqueous condition to produce ethylene carbonate and ethylene glycol; (b) a hydrolysis step of reacting the reaction solution containing ethylene carbonate and the ionic liquid composite catalyst obtained in step (a) with water to produce ethylene glycol; (c) a purification step of dehydrating and refining ethylene glycol from the aqueous solution containing ethylene glycol and the catalyst produced in step (b). The present process has the following advantages: the catalyst has high activity, high suitability, and good stability, the reaction condition is wild, the conversion of ethylene oxide is high, the selectivity of ethylene glycol is high, and the process is simple.

    摘要翻译： 公开了一种由离子液体催化的生产乙二醇的方法，其特征在于该方法包括以下三个步骤：（a）由包含羟基官能化的离子液体的离子液体复合催化剂催化的环氧乙烷和CO 2的羰基化步骤，和 在水溶液条件下制备碱金属盐以制备碳酸亚乙酯和乙二醇; （b）使含有碳酸亚乙酯的反应溶液和步骤（a）中得到的离子液体复合催化剂与水反应以产生乙二醇的水解步骤; （c）从含有乙二醇的水溶液和步骤（b）中制备的催化剂中脱水和精制乙二醇的纯化步骤。 本方法具有以下优点：催化剂活性高，适用性好，稳定性好，反应条件野生，环氧乙烷转化率高，乙二醇选择性高，工艺简单。

    CRYSTAL OF 6-[4-(4-PYRIDYLAMINO) PHENYL]-4,5-DIHYDRO-3(2H-PYRIDAZINONE HYDROCHLORIDE TRIHYDRATE
    3.
    发明申请
    CRYSTAL OF 6-[4-(4-PYRIDYLAMINO) PHENYL]-4,5-DIHYDRO-3(2H-PYRIDAZINONE HYDROCHLORIDE TRIHYDRATE 审中-公开
    6- [4-（4-吡啶基）苯基] -4,5-二氢-3（2H-吡啶酮氢氯化物三水合物）的晶体

    公开(公告)号：US20090005392A1

    公开(公告)日：2009-01-01

    申请号：US12029208

    申请日：2008-02-11

    申请人： Haruki Asatani ,  Akio Tsuboi ,  Suojiang Zhang ,  Shinji Ohura

    发明人： Haruki Asatani ,  Akio Tsuboi ,  Suojiang Zhang ,  Shinji Ohura

    IPC分类号： A61K31/501 ,  C07D401/12 ,  A61P9/12 ,  A61P9/00

    CPC分类号： C07D401/12 ,  A61K31/501

    摘要： The present invention provides crystals of 6-[4-(4-pyridylamino)phenyl]-4,5-dihydro-3(2H)-pyridazinone hydrochloride trihydrate useful as a medicament for therapeutic treatment of cardiac failure, and the like; and a pharmaceutical composition comprising said crystals as an active ingredient.The crystal of the present invention has characteristic absorption peaks (2θ degrees) at 12.9 (±0.2°) and 19.0 (±0.2°), for example, in powder X-ray diffractometry.

    摘要翻译： 本发明提供可用作治疗心力衰竭的药物的6- [4-（4-吡啶基氨基）苯基] -4,5-二氢-3（2H） - 哒嗪酮盐酸盐三水合物的晶体等。 以及包含所述晶体作为活性成分的药物组合物。 本发明的晶体在例如粉末X射线衍射中具有12.9（±0.2°）和19.0（±0.2°）的特征吸收峰（2θ）。

    Process for absorbing methylacrolein with ionic liquid
    6.
    发明授权
    Process for absorbing methylacrolein with ionic liquid 有权
    用离子液体吸收甲基丙烯醛的方法

    公开(公告)号：US07964756B2

    公开(公告)日：2011-06-21

    申请号：US12529906

    申请日：2008-03-10

    申请人： Suojiang Zhang ,  Qiong Chen ,  Ruiyi Yan ,  Lei Wang ,  Yuhuan Chen ,  Xiaoliang Yuan

    发明人： Suojiang Zhang ,  Qiong Chen ,  Ruiyi Yan ,  Lei Wang ,  Yuhuan Chen ,  Xiaoliang Yuan

    IPC分类号： C07C45/80

    CPC分类号： C07C45/79 ,  C07C47/22

    摘要： Disclosed is a process for absorbing methylacrolein, characterized in that it absorbs methylacrolein by an absorbent comprising an ionic liquid. The absorbent can absorb methylacrolein effectively, and it is easy to be separated from methylacrolein, regenerated and recycled. It is a green absorbent. The technique is a green methylacrolein absorbing and separating technique.

    摘要翻译： 公开了一种吸收甲基丙烯醛的方法，其特征在于它由包含离子液体的吸收剂吸收甲基丙烯醛。 吸收剂可有效吸收甲基丙烯醛，易于与甲基丙烯醛分离，再生和再循环。 它是一种绿色吸收剂。 该技术是绿色甲基丙烯醛吸收和分离技术。