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公开(公告)号：US20170009018A1
公开(公告)日：2017-01-12
申请号：US15224884
申请日：2016-08-01
Applicant: Ticona LLC
Inventor： Hendrich Chiong , Michael Haubs , Damian Feord , Mark Shatzer , Jacob Grayson
CPC classification number: C08G75/14 , B01J19/24 , B01J19/245 , B01J2219/00736 , B01J2219/00759 , B01J2219/24 , C08G75/16 , C08J3/203 , C08J2381/04
Abstract: Methods of forming a polyarylene sulfide and systems as may be utilized in carrying out the methods are described. Included in the formation method is a filtration process for treatment of a mixture, the mixture including a polyarylene sulfide, a salt byproduct of the polyarylene sulfide formation reaction, and a solvent. The filtration process includes maintaining the downstream side of the filter medium at an increased pressure. The downstream pressure can such that the boiling temperature of the mixture at the downstream pressure can be higher than the temperature at which the polyarylene sulfide is insoluble in the solvent.
Abstract translation: 描述形成聚芳硫醚的方法和可用于实施该方法的体系。 形成方法中包括用于处理混合物的过滤方法，该混合物包括聚芳硫醚，聚亚芳基硫醚形成反应的副产物和溶剂。 过滤过程包括将过滤介质的下游侧保持在增加的压力。 下游压力可以使得混合物在下游压力下的沸腾温度可以高于聚芳硫醚不溶于溶剂的温度。
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公开(公告)号：US20150087776A1
公开(公告)日：2015-03-26
申请号：US14481257
申请日：2014-09-09
Applicant: Ticona LLC
Inventor： Hendrich Chiong , Michael Haubs , Damian Feord , Stanley Leonard , Jacob Grayson , Venkata Nekkanti
CPC classification number: C08G75/14 , B01J19/0046 , B01J19/1862 , B01J2208/00176 , B01J2208/00274 , B01J2208/00283 , B01J2208/00539 , B01J2219/0013
Abstract: A multi-stage process and system for formation of a polyarylene sulfide is described. The multi-stage process can include at least three separate formation stages that can take place in three different reactors. The first stage of the formation process can include reaction of an alkali metal sulfide with an organic amide solvent to form a complex including a hydrolysis product of the solvent and an alkali metal hydrogen sulfide. The second stage of the formation process can include reaction of the complex formed in the first stage with a dihaloaromatic monomer to form a prepolymer, and the third stage can include further polymerization of the prepolymer with additional monomers to form the final product.
Abstract translation: 描述了用于形成聚芳硫醚的多阶段方法和系统。 多级方法可以包括可以在三个不同的反应器中进行的至少三个分开的形成阶段。 形成方法的第一阶段可以包括碱金属硫化物与有机酰胺溶剂的反应以形成包括溶剂和碱金属硫化氢的水解产物的络合物。 形成方法的第二阶段可以包括在第一阶段中形成的络合物与二卤代芳族单体的反应以形成预聚物，第三阶段可以包括使预聚物与另外的单体进一步聚合以形成最终产物。
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公开(公告)号：US09938379B2
公开(公告)日：2018-04-10
申请号：US15224884
申请日：2016-08-01
Applicant: Ticona LLC
Inventor： Hendrich Chiong , Michael Haubs , Damian Feord , Mark Shatzer , Jacob Grayson
CPC classification number: C08G75/14 , B01J19/24 , B01J19/245 , B01J2219/00736 , B01J2219/00759 , B01J2219/24 , C08G75/16 , C08J3/203 , C08J2381/04
Abstract: Methods of forming a polyarylene sulfide and systems as may be utilized in carrying out the methods are described. Included in the formation method is a filtration process for treatment of a mixture, the mixture including a polyarylene sulfide, a salt byproduct of the polyarylene sulfide formation reaction, and a solvent. The filtration process includes maintaining the downstream side of the filter medium at an increased pressure. The downstream pressure can such that the boiling temperature of the mixture at the downstream pressure can be higher than the temperature at which the polyarylene sulfide is insoluble in the solvent.
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公开(公告)号：US09403948B2
公开(公告)日：2016-08-02
申请号：US14481199
申请日：2014-09-09
Applicant: Ticona LLC
Inventor： Hendrich Chiong , Michael Haubs , Damian Feord , Mark Shatzer , Jacob Grayson
CPC classification number: C08G75/14 , B01J19/24 , B01J19/245 , B01J2219/00736 , B01J2219/00759 , B01J2219/24 , C08G75/16 , C08J3/203 , C08J2381/04
Abstract: Methods of forming a polyarylene sulfide and systems as may be utilized in carrying out the methods are described. Included in the formation method is a filtration process for treatment of a mixture, the mixture including a polyarylene sulfide, a salt byproduct of the polyarylene sulfide formation reaction, and a solvent. The filtration process includes maintaining the downstream side of the filter medium at an increased pressure. The downstream pressure can such that the boiling temperature of the mixture at the downstream pressure can be higher than the temperature at which the polyarylene sulfide is insoluble in the solvent.
Abstract translation: 描述形成聚芳硫醚的方法和可用于实施该方法的体系。 形成方法中包括用于处理混合物的过滤方法，该混合物包括聚芳硫醚，聚亚芳基硫醚形成反应的副产物和溶剂。 过滤过程包括将过滤介质的下游侧保持在增加的压力。 下游压力可以使得混合物在下游压力下的沸腾温度可以高于聚芳硫醚不溶于溶剂的温度。
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公开(公告)号：US09868824B2
公开(公告)日：2018-01-16
申请号：US15202730
申请日：2016-07-06
Applicant: Ticona LLC
Inventor： Hendrich Chiong , Michael Haubs , Damian Feord , Stanley Leonard , Jacob Grayson , Venkata Nekkanti
CPC classification number: C08G75/16 , C08J3/203 , C08J2381/04
Abstract: A method for formation of a semi-crystalline polyarylene sulfide is described. The method can include reaction of sulfur-containing monomer with a dihaloaromatic monomer in an organic amide solvent to form a polymer following by combination of the polymer with a crystallization solution. The crystallization solution is pre-heated and the mixture formed is slowly cooled to crystallize the polymer.
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Patent Agency Ranking
公开(公告)号：US20160244567A1
公开(公告)日：2016-08-25
申请号：US15045296
申请日：2016-02-17
Applicant: Ticona LLC
Inventor： Venkata M. Nekkanti , Hendrich A. Chiong , Jacob Grayson
CPC classification number: C08G75/14 , B01D11/0288 , B01D21/02 , C08G85/002
Abstract: A method for washing a polyarylene sulfide with a washing solution that contains a carefully controlled solvent content is provided. More particularly, the washing solution typically contains water (e.g., deionized water) in an amount of from about 30 wt. % to about 70 wt. % and an aprotic organic solvent in an amount of from about 30 wt. % to about 70 wt. %. Within such carefully controlled ranges, the present inventors have discovered that the polyarylene sulfide can retain a relatively high oligomer content, which in turn, helps minimize the melt viscosity.
Abstract translation: 提供了一种用含有精心控制的溶剂含量的洗涤溶液洗涤聚芳硫醚的方法。 更具体地，洗涤溶液通常含有约30重量％的水（例如去离子水）。 ％至约70wt。 ％和非质子有机溶剂，其量为约30wt。 ％至约70wt。 ％。 在这样仔细控制的范围内，本发明人已经发现，聚芳硫醚可以保持相对高的低聚物含量，这又有助于使熔体粘度最小化。
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公开(公告)号：US09388283B2
公开(公告)日：2016-07-12
申请号：US14481285
申请日：2014-09-09
Applicant: Ticona LLC
Inventor： Hendrich Chiong , Michael Haubs , Damian Feord , Stanley Leonard , Jacob Grayson , Venkata Nekkanti
CPC classification number: C08G75/16 , C08J3/203 , C08J2381/04
Abstract: A method for formation of a semi-crystalline polyarylene sulfide is described. The method can include reaction of sulfur-containing monomer with a dihaloaromatic monomer in an organic amide solvent to form a polymer following by combination of the polymer with a crystallization solution. The crystallization solution is pre-heated and the mixture formed is slowly cooled to crystallize the polymer.
Abstract translation: 描述了形成半结晶聚芳硫醚的方法。 该方法可以包括在有机酰胺溶剂中含硫单体与二卤代芳族单体的反应，以便通过聚合物与结晶溶液的组合形成聚合物。 将结晶溶液预热，并将形成的混合物缓慢冷却以使聚合物结晶。
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公开(公告)号：US20150087779A1
公开(公告)日：2015-03-26
申请号：US14481199
申请日：2014-09-09
Applicant: Ticona LLC
Inventor： Hendrich Chiong , Michael Haubs , Damian Feord , Mark Shatzer , Jacob Grayson
CPC classification number: C08G75/14 , B01J19/24 , B01J19/245 , B01J2219/00736 , B01J2219/00759 , B01J2219/24 , C08G75/16 , C08J3/203 , C08J2381/04
Abstract: Methods of forming a polyarylene sulfide and systems as may be utilized in carrying out the methods are described. Included in the formation method is a filtration process for treatment of a mixture, the mixture including a polyarylene sulfide, a salt byproduct of the polyarylene sulfide formation reaction, and a solvent. The filtration process includes maintaining the downstream side of the filter medium at an increased pressure. The downstream pressure can such that the boiling temperature of the mixture at the downstream pressure can be higher than the temperature at which the polyarylene sulfide is insoluble in the solvent.
Abstract translation: 描述形成聚芳硫醚的方法和可用于实施该方法的体系。 形成方法中包括用于处理混合物的过滤方法，该混合物包括聚芳硫醚，聚亚芳基硫醚形成反应的副产物和溶剂。 过滤过程包括将过滤介质的下游侧保持在增加的压力。 下游压力可以使得混合物在下游压力下的沸腾温度可以高于聚芳硫醚不溶于溶剂的温度。
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公开(公告)号：US20150087780A1
公开(公告)日：2015-03-26
申请号：US14481285
申请日：2014-09-09
Applicant: Ticona LLC
Inventor： Hendrich Chiong , Michael Haubs , Damian Feord , Stanley Leonard , Jacob Grayson , Venkata Nekkanti
CPC classification number: C08G75/16 , C08J3/203 , C08J2381/04
Abstract: A method for formation of a semi-crystalline polyarylene sulfide is described. The method can include reaction of sulfur-containing monomer with a dihaloaromatic monomer in an organic amide solvent to form a polymer following by combination of the polymer with a crystallization solution. The crystallization solution is pre-heated and the mixture formed is slowly cooled to crystallize the polymer.
Abstract translation: 描述了形成半结晶聚芳硫醚的方法。 该方法可以包括在有机酰胺溶剂中含硫单体与二卤代芳族单体的反应，以便通过聚合物与结晶溶液的组合形成聚合物。 将结晶溶液预热，并将形成的混合物缓慢冷却以使聚合物结晶。
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公开(公告)号：US09809681B2
公开(公告)日：2017-11-07
申请号：US15045296
申请日：2016-02-17
Applicant: Ticona LLC
Inventor： Venkata M. Nekkanti , Hendrich A. Chiong , Jacob Grayson
CPC classification number: C08G75/14 , B01D11/0288 , B01D21/02 , C08G85/002
Abstract: A method for washing a polyarylene sulfide with a washing solution that contains a carefully controlled solvent content is provided. More particularly, the washing solution typically contains water (e.g., deionized water) in an amount of from about 30 wt. % to about 70 wt. % and an aprotic organic solvent in an amount of from about 30 wt. % to about 70 wt. %. Within such carefully controlled ranges, the present inventors have discovered that the polyarylene sulfide can retain a relatively high oligomer content, which in turn, helps minimize the melt viscosity.
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