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公开(公告)号:US20130011775A1
公开(公告)日:2013-01-10
申请号:US13537387
申请日:2012-06-29
申请人: Tsuyoshi Itou , Motonari Udo , Kazuhisa Takeda , Takayasu Aoki , Masahiro Ikuta , Takafumi Hara
发明人: Tsuyoshi Itou , Motonari Udo , Kazuhisa Takeda , Takayasu Aoki , Masahiro Ikuta , Takafumi Hara
CPC分类号: G03G9/09371 , G03G9/09307 , G03G9/09321 , G03G9/0935 , G03G9/09392
摘要: Disclosed is a toner obtained by coating surfaces of core particles including at least a binder resin having a carboxyl group and a coloring agent with successive coatings of a water-soluble crosslinking agent capable of crosslinking with a carboxyl group and a water-soluble polymer having a carboxyl group, which have been successively applied on the core particles and crosslinked with each other. The thus-formed toner is provided with a good harmony of favorable fixability represented by a low lowest fixable temperature and favorable storage stability represented by little aggregation after standing at 50° C. for 8 hours.
摘要翻译: 公开了一种调色剂,其通过将至少包含具有羧基的粘合剂树脂和着色剂的核心颗粒的表面涂覆到能够与羧基交联的水溶性交联剂的连续涂层和具有羧基的水溶性聚合物 羧基,其已经连续地施加在核心颗粒上并彼此交联。 这样形成的调色剂具有以低最低定影温度表示的良好的定影性和由在50℃下放置8小时后几乎没有聚集性而获得的有利的储存稳定性的良好的调和性。
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公开(公告)号:US20120328977A1
公开(公告)日:2012-12-27
申请号:US13525627
申请日:2012-06-18
申请人: Masahiro Ikuta , Takayasu Aoki , Tsuyoshi Itou , Motonari Udo , Takafumi Hara , Kazuhisa Takeda
发明人: Masahiro Ikuta , Takayasu Aoki , Tsuyoshi Itou , Motonari Udo , Takafumi Hara , Kazuhisa Takeda
IPC分类号: G03G9/093
CPC分类号: G03G9/0928 , G03G9/09307 , G03G9/0935 , G03G9/09392
摘要: Encapsulated toner particles are formed by: aggregating core material particles containing at least a colorant and a core material resin in an aqueous dispersion medium to form core particles; adding coating resin particles into the aqueous dispersion medium during progress of the formation of the core material at a point of time when the volume-based median particle diameter of the core particles formed by the aggregation reaches 30 to 83% of that of desired toner particles; and continuing the aggregation to form a coating layer composed of a composite aggregate of the core material particles and the coating resin particles on the core material. In the thus-obtained toner, the colorant is uniformly and well incorporated in the toner particles, and therefore, the coloring ability is improved without causing a problem of release of fine powder.
摘要翻译: 通过以下方法形成封装的调色剂颗粒:将含有至少着色剂的芯材颗粒和芯材树脂在水分散介质中聚集以形成芯颗粒; 在由聚集体形成的芯颗粒的基于体积的中值粒径达到期望的调色剂颗粒的30至83%的时间点时,在芯材料的形成过程中将涂料树脂颗粒加入到水性分散介质中 ; 并且继续聚集以形成由芯材料颗粒和涂覆树脂颗粒在芯材上的复合骨料组成的涂层。 在这样得到的调色剂中,着色剂均匀且良好地结合到调色剂颗粒中,因此着色能力得到改善,而不会引起细粉的释放。
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公开(公告)号:US08790857B2
公开(公告)日:2014-07-29
申请号:US13537387
申请日:2012-06-29
申请人: Tsuyoshi Itou , Motonari Udo , Kazuhisa Takeda , Takayasu Aoki , Masahiro Ikuta , Takafumi Hara
发明人: Tsuyoshi Itou , Motonari Udo , Kazuhisa Takeda , Takayasu Aoki , Masahiro Ikuta , Takafumi Hara
IPC分类号: G03G9/00
CPC分类号: G03G9/09371 , G03G9/09307 , G03G9/09321 , G03G9/0935 , G03G9/09392
摘要: Disclosed is a toner obtained by coating surfaces of core particles including at least a binder resin having a carboxyl group and a coloring agent with successive coatings of a water-soluble crosslinking agent capable of crosslinking with a carboxyl group and a water-soluble polymer having a carboxyl group, which have been successively applied on the core particles and crosslinked with each other. The thus-formed toner is provided with a good harmony of favorable fixability represented by a low lowest fixable temperature and favorable storage stability represented by little aggregation after standing at 50° C. for 8 hours.
摘要翻译: 公开了一种调色剂,其通过将至少包含具有羧基的粘合剂树脂和着色剂的核心颗粒的表面涂覆到能够与羧基交联的水溶性交联剂的连续涂层和具有羧基的水溶性聚合物 羧基,其已经连续地施加在核心颗粒上并彼此交联。 这样形成的调色剂具有以低最低定影温度表示的良好的定影性和由在50℃下放置8小时后几乎没有聚集性而获得的有利的储存稳定性的良好的调和性。
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公开(公告)号:US20100310981A1
公开(公告)日:2010-12-09
申请号:US12792132
申请日:2010-06-02
申请人: Junichi Ishikawa , Takayasu Aoki , Tsuyoshi Itou , Yasuhito Noda , Motonari Udo , Satoshi Araki , Masahiro Ikuta , Takafumi Hara , Takashi Urabe , Taishi Takano , Yasuo Goto
发明人: Junichi Ishikawa , Takayasu Aoki , Tsuyoshi Itou , Yasuhito Noda , Motonari Udo , Satoshi Araki , Masahiro Ikuta , Takafumi Hara , Takashi Urabe , Taishi Takano , Yasuo Goto
CPC分类号: G03G9/08795 , G03G9/0804 , G03G9/081 , G03G9/0819 , G03G9/08755
摘要: According to one embodiment, a method for producing a developing agent includes pulverizing a mixture in the form of coarse particles of a toner material including a coloring agent and a binder resin by mechanical shearing, aggregating and fusing the resulting fine particles. The solid content concentration in a dispersion liquid including the aggregated particles is from 5.0% to 40.0%, the volume average particle diameter of the aggregated particles is from 1.0 μm to 10.0 μm, and the ratio of the standard deviation to the volume average particle diameter is 30.0% or less.
摘要翻译: 根据一个实施方案,用于生产显影剂的方法包括通过机械剪切来粉碎包括着色剂和粘合剂树脂的调色剂材料的粗颗粒形式的混合物,使所得到的微粒聚集和熔融。 包含凝集粒子的分散液中的固体成分浓度为5.0〜40.0%,凝集粒子的体积平均粒径为1.0〜10.0μm,标准偏差与体积平均粒径的比率 为30.0%以下。
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公开(公告)号:US20100209840A1
公开(公告)日:2010-08-19
申请号:US12638145
申请日:2009-12-15
申请人: Masahiro Ikuta , Takayasu Aoki , Takashi Urabe , Tsuyoshi Itou , Satoshi Araki , Motonari Udo , Takafumi Hara
发明人: Masahiro Ikuta , Takayasu Aoki , Takashi Urabe , Tsuyoshi Itou , Satoshi Araki , Motonari Udo , Takafumi Hara
CPC分类号: G03G9/09392 , G03G9/0804 , G03G9/08797 , G03G9/09328 , G03G9/09371
摘要: As a first dispersion liquid containing first fine particles and a second dispersion liquid containing second fine particles, those satisfy the relationship represented by the following formula (1) are used, and these two dispersion liquids are mixed with each other, and an aggregating agent and a pH adjusting agent are added thereto in sequence, whereby encapsulation is achieved by selective formation of core particles through aggregation of the first fine particles and shells through aggregation of the second fine particles. 15 mV≧|Z2−Z1|≧5 mV (1) In the formula, Z1 and Z2 represent zeta potentials of the first dispersion liquid and the second dispersion liquid, respectively, measured when aluminum sulfate is added to each dispersion liquid in an amount of 1% by weight based on the solid content in each dispersion liquid.
摘要翻译: 作为含有第一细小颗粒的第一分散液和含有第二细颗粒的第二分散液,使用满足由下式(1)表示的关系的第二分散液,将这两种分散液彼此混合,并将聚集剂和 依次加入pH调节剂,由此通过使第一细颗粒和壳通过第二细颗粒的聚集而聚集而选择性形成核心颗粒来实现包封。 15mV≥| Z2-Z1 |≥5mV(1)在式中,Z1和Z2分别表示当将各种分散液中的硫酸铝加入量时测定的第一分散液和第二分散液的ζ电位 相对于各分散液中的固体成分为1重量%。
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公开(公告)号:US20100009281A1
公开(公告)日:2010-01-14
申请号:US12500085
申请日:2009-07-09
申请人: Tsuyoshi Itou , Takayasu Aoki , Takashi Urabe , Yasuhito Noda , Motonari Udo , Satoshi Araki , Masahiro Ikuta , Takafumi Hara , Asumi Matsumoto
发明人: Tsuyoshi Itou , Takayasu Aoki , Takashi Urabe , Yasuhito Noda , Motonari Udo , Satoshi Araki , Masahiro Ikuta , Takafumi Hara , Asumi Matsumoto
CPC分类号: G03G9/08795 , G03G9/0804 , G03G9/0808 , G03G9/0819 , G03G9/08755 , G03G9/08797 , G03G9/09708
摘要: The method for producing a developing agent according to the invention contains subjecting the toner material dispersion liquid to mechanical shearing to make the granular mixture into fine particles, thereby providing a dispersion liquid containing fine particles having a smaller particle diameter than a particle diameter of the granular mixture. The toner material dispersion liquid is subjected to mechanical shearing under a temperature of a glass transition point Tg of the binder resin or more and a pressure of 10 MPa or more, and the resulting dispersion liquid containing the fine particles is depressurized with two or more stages while maintaining the temperature of a glass transition point Tg of the binder resin or more and then cooled to a temperature of a glass transition point Tg of the binder resin or less.
摘要翻译: 根据本发明的显影剂的制造方法包括使调色剂分散液进行机械剪切以使颗粒状混合物成为细颗粒,从而提供包含比颗粒的粒径小的粒径的分散液 混合物。 调色剂分散液在粘合剂树脂的玻璃化转变点Tg的温度和10MPa以上的压力的温度下进行机械剪切,将所得到的含有微粒的分散液用两级以上的级 同时保持粘合剂树脂的玻璃化转变点Tg的温度以上,然后冷却至粘合剂树脂的玻璃化转变点Tg的温度以下。
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公开(公告)号:US08785097B2
公开(公告)日:2014-07-22
申请号:US13537426
申请日:2012-06-29
申请人: Takayasu Aoki , Motonari Udo , Tsuyoshi Itou , Masahiro Ikuta , Takafumi Hara
发明人: Takayasu Aoki , Motonari Udo , Tsuyoshi Itou , Masahiro Ikuta , Takafumi Hara
CPC分类号: G03G9/0928 , G03G9/0806 , G03G9/0812 , G03G9/08711 , G03G9/08753 , G03G9/08755 , G03G9/08766 , G03G9/08768 , G03G9/08791 , G03G9/08793 , G03G9/08795 , G03G9/08797 , G03G9/09 , G03G9/0926
摘要: Disclosed is a decolorable toner produced by aggregating dispersed fine particles of a color material containing at least a color-forming compound, a color-developing agent and a decoloring agent with dispersed fine particles containing at least a binder resin having a carboxyl group, then adding a compound having a carbodiimide group or an epoxy group reactive with the carboxyl group of the binder resin, and thereafter fusing the aggregate particles, respectively in an aqueous medium. The thus obtained decolorable toner can suppress the generation of fine powder by the release of erasable color material fine particles from the toner particles.
摘要翻译: 公开了通过使至少含有成色化合物,显色剂和脱色剂的着色材料的分散微粒聚集到至少含有具有羧基的粘合剂树脂的分散细小颗粒而制成的脱色调色剂,然后加入 具有碳化二亚胺基团或与粘合剂树脂的羧基反应的环氧基的化合物,然后分别在水性介质中熔融骨料颗粒。 由此获得的无色调色剂可以通过从调色剂颗粒中释放可擦除的着色材料细颗粒来抑制细粉的产生。
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公开(公告)号:US08227167B2
公开(公告)日:2012-07-24
申请号:US12500085
申请日:2009-07-09
申请人: Tsuyoshi Itou , Takayasu Aoki , Takashi Urabe , Yasuhito Noda , Motonari Udo , Satoshi Araki , Masahiro Ikuta , Takafumi Hara , Asumi Matsumoto
发明人: Tsuyoshi Itou , Takayasu Aoki , Takashi Urabe , Yasuhito Noda , Motonari Udo , Satoshi Araki , Masahiro Ikuta , Takafumi Hara , Asumi Matsumoto
IPC分类号: G03G9/08
CPC分类号: G03G9/08795 , G03G9/0804 , G03G9/0808 , G03G9/0819 , G03G9/08755 , G03G9/08797 , G03G9/09708
摘要: The method for producing a developing agent according to the invention contains subjecting the toner material dispersion liquid to mechanical shearing to make the granular mixture into fine particles, thereby providing a dispersion liquid containing fine particles having a smaller particle diameter than a particle diameter of the granular mixture. The toner material dispersion liquid is subjected to mechanical shearing under a temperature of a glass transition point Tg of the binder resin or more and a pressure of 10 MPa or more, and the resulting dispersion liquid containing the fine particles is depressurized with two or more stages while maintaining the temperature of a glass transition point Tg of the binder resin or more and then cooled to a temperature of a glass transition point Tg of the binder resin or less.
摘要翻译: 根据本发明的显影剂的制造方法包括使调色剂分散液进行机械剪切以使颗粒状混合物成为细颗粒,从而提供包含比颗粒的粒径小的粒径的分散液 混合物。 调色剂分散液在粘合剂树脂的玻璃化转变点Tg的温度和10MPa以上的压力的温度下进行机械剪切,将所得到的含有微粒的分散液用两级以上的级 同时保持粘合剂树脂的玻璃化转变点Tg的温度以上,然后冷却至粘合剂树脂的玻璃化转变点Tg的温度以下。
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公开(公告)号:US20110014558A1
公开(公告)日:2011-01-20
申请号:US12832380
申请日:2010-07-08
申请人: Masahiro Ikuta , Takayasu Aoki , Takashi Urabe , Tsuyoshi Itou , Motonari Udo , Satoshi Araki , Takafumi Hara , Yasuhito Noda , Taishi Takano , Yasuo Goto , Junichi Ishikawa
发明人: Masahiro Ikuta , Takayasu Aoki , Takashi Urabe , Tsuyoshi Itou , Motonari Udo , Satoshi Araki , Takafumi Hara , Yasuhito Noda , Taishi Takano , Yasuo Goto , Junichi Ishikawa
IPC分类号: G03G9/08
CPC分类号: G03G9/0806 , G03G9/0823 , G03G9/0827 , G03G9/08755 , G03G9/0918
摘要: According to one embodiment, a method for producing a developing agent including aggregating fine particles of a toner material containing a binder resin and a coloring agent in a dispersion liquid in which the fine particles are dispersed in an aqueous medium to form aggregated particles, and washing the aggregated particles and drying the washed aggregated particles, forming toner particles is provided. An electrical conductivity of the toner particles is measured by a toner electrical conductivity evaluation method. A sample toner is prepared by adhering an additive to surfaces of the toner particles, and a content ratio of a sodium element to a carbon element in a region to which the additive is not adhered of the toner is measured. The washing of the toner particles is repeated until each of the measurement values becomes a predetermined reference value or less.
摘要翻译: 根据一个实施方案,一种生产显影剂的方法,包括在分散液中含有粘合剂树脂和着色剂的调色剂材料的细颗粒,其中细颗粒分散在水性介质中以形成凝集颗粒,并洗涤 提供聚集的颗粒并干燥洗涤的聚集颗粒,形成调色剂颗粒。 通过调色剂导电性评估方法测量调色剂颗粒的电导率。 通过将添加剂粘附到调色剂颗粒的表面,并测量在调色剂未附着添加剂的区域中的钠元素与碳元素的含量比,来制备样品调色剂。 重复调色剂颗粒的洗涤,直到每个测量值变为预定的参考值或更小。
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公开(公告)号:US07851120B2
公开(公告)日:2010-12-14
申请号:US12330992
申请日:2008-12-09
申请人: Takashi Urabe , Takayasu Aoki , Tsuyoshi Itou , Yasuhito Noda , Motonari Udo , Satoshi Araki , Masahiro Ikuta , Takafumi Hara , Asumi Matsumoto
发明人: Takashi Urabe , Takayasu Aoki , Tsuyoshi Itou , Yasuhito Noda , Motonari Udo , Satoshi Araki , Masahiro Ikuta , Takafumi Hara , Asumi Matsumoto
IPC分类号: G03G9/18
CPC分类号: G03G9/0804 , G03G9/0815 , G03G9/0819 , G03G9/0827 , G03G9/08755 , G03G9/08795 , G03G9/08797
摘要: The dispersion liquid including toner material particles is introduced into a mechanical shearing device including a heating unit, a mechanical shearing unit, and a cooling unit, heated to a temperature not lower than the glass transition temperature of the polyester resin under a condition that satisfies the following relationship (1), subjected to mechanical shearing, and thereafter cooled, whereby fine particles are obtained. −2
摘要翻译: 将包含调色剂材料颗粒的分散液引入包括加热单元,机械剪切单元和冷却单元的机械剪切装置中,在满足下述条件的条件下加热到不低于聚酯树脂的玻璃化转变温度的温度 (1),进行机械剪切,然后冷却,得到微粒子。 -2
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