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公开(公告)号：US07824631B2
公开(公告)日：2010-11-02
申请号：US12045212
申请日：2008-03-10
申请人： Tsuyoshi Noma , Hidetoshi Ibe , Eiichi Sugiyama , Tadashi Imai , Kazutaka Kojo , Kiyoshi Imai
发明人： Tsuyoshi Noma , Hidetoshi Ibe , Eiichi Sugiyama , Tadashi Imai , Kazutaka Kojo , Kiyoshi Imai
摘要： A nanocarbon generation equipment designed such that organic processed materials can be quickly thermally decomposed therein and the decomposed materials are then quenched and liquefied to obtain liquefied materials is disclosed. This equipment comprises thermal reactor for quickly thermally decomposing the organic processed materials, apparatus for recovering the liquefied materials which are liquefied through quenching of thermally decomposed organic processed materials, a rotary furnace to be filled with a reducing atmosphere and loaded with hydrocarbons to be obtained through vaporization of liquefied materials after impurities contained in the liquefied materials are removed, and metal balls made of a metal selected from stainless steel, iron, nickel, chromium and an optional combination thereof, wherein the hydrocarbon introduced into the rotary furnace is decomposed into carbon and hydrogen, thus enabling nanocarbon to be produced through vapor-phase growth.
摘要翻译： 一种纳米碳发生设备，其设计使得有机处理材料能够快速热分解，然后将分解的材料淬火和液化以获得液化材料。 该设备包括用于快速热分解有机处理材料的热反应器，用于回收通过淬火热分解的有机处理材料液化的液化材料的设备，填充有还原气体的旋转炉，并装载要通过 除去液化材料中含有的杂质之后的液化物质的蒸发，以及由不锈钢，铁，镍，铬及其任意组合的金属制成的金属球，其中引入旋转炉的烃分解成碳和 氢气，从而使得能够通过气相生长生产纳米碳。
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公开(公告)号：US20080260606A1
公开(公告)日：2008-10-23
申请号：US12045212
申请日：2008-03-10
申请人： Tsuyoshi NOMA , Hidetoshi Ibe , Eiichi Sugiyama , Tadashi Imai , Kazutaka Kojo , Kiyoshi Imai
发明人： Tsuyoshi NOMA , Hidetoshi Ibe , Eiichi Sugiyama , Tadashi Imai , Kazutaka Kojo , Kiyoshi Imai
IPC分类号： B01J8/10
摘要： A nanocarbon generation equipment designed such that organic processed materials can be quickly thermally decomposed therein and the decomposed materials are then quenched and liquefied to obtain liquefied materials is disclosed. This equipment comprises thermal reactor for quickly thermally decomposing the organic processed materials, apparatus for recovering the liquefied materials which are liquefied through quenching of thermally decomposed organic processed materials, a rotary furnace to be filled with a reducing atmosphere and loaded with hydrocarbons to be obtained through vaporization of liquefied materials after impurities contained in the liquefied materials are removed, and metal balls made of a metal selected from stainless steel, iron, nickel, chromium and an optional combination thereof, wherein the hydrocarbon introduced into the rotary furnace is decomposed into carbon and hydrogen, thus enabling nanocarbon to be produced through vapor-phase growth.
摘要翻译： 一种纳米碳发生设备，其设计使得有机处理材料能够快速热分解，然后将分解的材料淬火和液化以获得液化材料。 该设备包括用于快速热分解有机处理材料的热反应器，用于回收通过淬火热分解的有机处理材料液化的液化材料的设备，填充有还原气体的旋转炉，并装载要通过 除去液化材料中含有的杂质之后的液化物质的蒸发，以及由不锈钢，铁，镍，铬及其任意组合的金属制成的金属球，其中引入旋转炉的烃分解成碳和 氢气，从而使得能够通过气相生长生产纳米碳。
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公开(公告)号：US20080241018A1
公开(公告)日：2008-10-02
申请号：US11902289
申请日：2007-09-20
申请人： Eiichi Sugiyama , Kazutaka Kojo , Tadashi Imai , Tsuyoshi Noma
发明人： Eiichi Sugiyama , Kazutaka Kojo , Tadashi Imai , Tsuyoshi Noma
IPC分类号： B01J19/00
CPC分类号： B01J6/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/164
摘要： There is disclosed a nanocarbon generating equipment which is designed to execute a process wherein an organic processed material is thermally decomposed at first and then the decomposed matter is cooled and liquefied. The apparatus comprising a thermal reactor for thermally decomposing the organic processed material, a recovering device which is configured to cool and liquefy a decomposed organic processed material and to recover a liquefied product, and a high-temperature furnace for treating the liquefied product, wherein impurities contained in the liquefied product is removed and the resultant liquefied product is introduced into the high-temperature furnace kept in a reducing atmosphere to generate nanocarbon through a vapor-phase growth.
摘要翻译： 公开了一种纳米碳发生设备，其被设计为执行其中有机加工材料首先被热分解，然后将分解的物质冷却和液化的方法。 该装置包括用于热分解有机处理材料的热反应器，用于冷却和液化分解的有机处理材料并回收液化产物的回收装置，以及用于处理液化产物的高温炉，其中杂质 将液化产物中所含的物质除去，将所得到的液化产物引入保持在还原气氛中的高温炉中，通过气相生长生成纳米碳。
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公开(公告)号：US08557191B2
公开(公告)日：2013-10-15
申请号：US13020260
申请日：2011-02-03
申请人： Eiichi Sugiyama , Katsuki Ide , Kazutaka Kojo , Tsuyoshi Noma
发明人： Eiichi Sugiyama , Katsuki Ide , Kazutaka Kojo , Tsuyoshi Noma
摘要： According to one embodiment, a nanocarbon producing apparatus includes a heating vessel which provides a reducing atmosphere therein, a heating source disposed on an outer circumference of the heating vessel, a hydrocarbon injection nozzle disposed on an upstream side of the heating vessel for spraying hydrocarbon into the heating vessel, and a nanocarbon product discharge nozzle disposed on a downstream side of the heating vessel, wherein a metallic substrate is disposed on an inside surface of the heating vessel and the hydrocarbon is continuously sprayed from the hydrocarbon injection nozzle, effecting a reaction to grow nanocarbon on the metallic substrate, and the grown nanocarbon product is peeled off from the metallic substrate and discharged through the discharge nozzle.
摘要翻译： 根据一个实施方案，纳米碳制造装置包括其中提供还原气体的加热容器，设置在加热容器的外圆周上的加热源，设置在加热容器的上游侧用于喷射烃的烃喷射嘴 加热容器和设置在加热容器的下游侧的纳米碳产品排出喷嘴，其中金属基底设置在加热容器的内表面上，烃从烃喷射喷嘴连续喷射，进行反应 在金属基材上生长纳米碳，生长的纳米碳产品从金属基材上剥离并通过排出喷嘴排出。
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公开(公告)号：US5082972A
公开(公告)日：1992-01-21
申请号：US551086
申请日：1990-07-11
申请人： Tadashi Komiyama , Hisaharu Kuboyama , Takashi Jimbo , Hiroyoshi Watanabe , Shuichi Tokumoto , Yumiko Endoh , Eiichi Sugiyama , Yoshitaro Naganuma
发明人： Tadashi Komiyama , Hisaharu Kuboyama , Takashi Jimbo , Hiroyoshi Watanabe , Shuichi Tokumoto , Yumiko Endoh , Eiichi Sugiyama , Yoshitaro Naganuma
IPC分类号： C07C209/16
CPC分类号： C07C209/16
摘要： At least one of ammonia and ethylenediamine is reacted with monoethanolamine in the presence of a catalyst containing phosphoric acid or its condensate in order to prepare acyclic ethyleneamines, and the catalyst can be improved in performance and the life of the catalyst can be prolonged by feeding a phosphorus-containing material to a reaction system during the reaction. In addition, the catalyst having a deteriorated performance can be reactivated by adding the phosphorus-containing material to the catalyst.
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