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    Finishing process incorporating improved catalyst systems to produce durable flameproofed cellulosic textile products with an excellent hand
    1.
    发明授权
    Finishing process incorporating improved catalyst systems to produce durable flameproofed cellulosic textile products with an excellent hand 失效
    完善工艺，改进的催化剂体系，生产具有优异手感的耐用易燃纤维素纺织品

    公开(公告)号：US3796596A

    公开(公告)日：1974-03-12

    申请号：US3796596D

    申请日：1972-05-05

    申请人： US AGRICULTURE

    发明人： DAIGLE D ,  PEPPERMAN A ,  REEVES W ,  DRAKE G

    IPC分类号： D06M15/431 ,  D06M15/667 ,  C09D5/18 ,  C09K3/28

    CPC分类号： D06M15/667 ,  D06M15/431

    摘要： IMPROVED CATALYST SYSTEMS HAVE BEEN FOUND THAT CAN BE USED IN PLACE OF THE CATALYST SYSTEMS PREVIOUSLY REQUIRED TO CURE FLAME-RETARDANT FINISHES FOR CELLULOSE TEXTILES. THESE IMPROVED CATALYST SYSTEMS CONSIST OF A MIXTURE OF ALUMINUM CHLORHYDROXIDE AND AN ACID SELECTED FROM THE GROUP PHOSPHORIC ACID, AXALIC ACID, LACTIC ACID OR A MIXTURE SELECTED FROM THE GOLLOWING: ZINC CHLORIDEGLYCOLIC ACID, MAGNESIUM CHLORIDE-CITRIC ACID, AND MAGNESIUM CHLORIDE-GLYCOLIC ACID. UNLIKE CELLULOSIC FABRICS TREATED WITH THE THP-AMIDE OR THPOH-AMIDE FINISHES WITH OR WITHOUT OTHER CATALYST SYSTEMS, FABRICS SIMILARLY PROCESSED WITH THE IMPROVED CATALYST SYSTEM, THAT IS, THE ONES CONTAINING ALUMINUM CHLORHYDROXIDE HAVE LOWER STIFFNESS VALUE AND A MUCH BETTER HAND.

    Process of treating fibrous materials with the reaction product of methylolphosphine adducts and nitrogenous compounds
    3.
    发明授权
    Process of treating fibrous materials with the reaction product of methylolphosphine adducts and nitrogenous compounds 失效
    用甲基磷酰胺和硝基化合物的反应产物处理纤维材料的方法

    公开(公告)号：US3844824A

    公开(公告)日：1974-10-29

    申请号：US30677472

    申请日：1972-11-15

    申请人： US AGRICULTURE

    发明人： REEVES W ,  DONALDSON D ,  BENINATE J ,  DAIGLE D ,  DRAKE G

    IPC分类号： C07F9/50 ,  C07F9/53 ,  C08G79/02 ,  D06M15/431 ,  D06M15/673 ,  C09D5/18

    CPC分类号： D06M15/673 ,  C07F9/5004 ,  C07F9/5304 ,  C08G79/02 ,  D06M15/431 ,  Y10S428/921 ,  Y10T442/268

    摘要： Soluble methylol phosphine adducts which contain one or more methylol phosphine radicals (PCH2OH) are prepared by reacting in a suitable solvent tris(hydroxymethyl)phosphine with an amide or amine which contains one or more hydrogens attached to trivalent nitrogen. These soluble adducts are particularly valuable for the preparation of thermosetting flame resistant polymers by reacting them with nitrogenous compounds which contain two or more hydrogen and methylol groups attached to trivalent nitrogen. The adducts are also valuable for the preparation of flame-, glow-, wrinkle-, and shrink-resistant knit and woven textiles by causing the adducts to react with nitrogenous compounds in or on the textile structure by application of heat.

    摘要翻译： 含有一个或多个羟甲基膦基（PCH 2 OH）的可溶性羟甲基膦加合物通过在合适的溶剂中将三（羟甲基）膦与含有一个或多个与三价氮连接的氢的酰胺或胺反应来制备。 这些可溶性加合物通过与含有两个或多个连接到三价氮的氢和羟甲基的含氮化合物反应来制备热固性阻燃聚合物是特别有价值的。 加合物对于制备阻燃，发光，抗皱和抗收缩的针织和纺织织物也是有价值的，它们通过加热使加合物与织物结构中或其上的含氮化合物反应。

    Flame-resistant organic textiles through treatment with halogen containing soluble methylol phosphine adducts
    7.
    发明授权
    Flame-resistant organic textiles through treatment with halogen containing soluble methylol phosphine adducts 失效
    通过含有可溶性甲基酚磷酸盐添加剂的卤素进行处理的抗阻抗有机纺织品

    公开(公告)号：US3745191A

    公开(公告)日：1973-07-10

    申请号：US3745191D

    申请日：1971-05-07

    申请人： US AGRICULTURE

    发明人： DRAKE G ,  DAIGLE D ,  REEVES W

    IPC分类号： C07F9/50 ,  C08G79/02 ,  D06M13/285

    CPC分类号： C08G79/02 ,  C07F9/50 ,  C08G79/025 ,  D06M13/285 ,  Y10S260/24 ,  Y10T442/268

    摘要： SOLUBLE METHYLOL PHOSPHINE ADDUCTS WHICH CONTAIN HALOGEN ATOMS ATTACHED TO AROMATIC CARBON ATOMS ARE PREPARED BY REACTING TRIS(HYDROXYMETHYL)PHOSPHINE WITH HALOGEN SUBSTITUTED PHENOLS WHICH CONTAIN ONE OR MORE HYDROGENS ORTHO OR PARA TO THE PHENOLIC HYDROXYL GROUP. THESE ADDUCTS ARE CONVENIENT AND USEFUL FOR (A) THE PREPARATION OF FLAMES-RESISTANT POLYMERS AND (B) THE PREPARATION OF FLAME-RESISTANT ORGANIC FIBROUS MATERIALS AND FLAME-, GLOW-, WRINKLE-, AND SHRINK-RESISTANT WOVEN AND KNIT TEXTILES WHICH CONTAIN ABOUT 25% OR MORE CELLULOSIC FIBERS.

    摘要翻译： 含有与芳族碳原子连接的卤素原子的可溶性羟甲基膦加合物通过使三羟甲基膦与含酚一羟基的邻位或对位上的一个或多个氢的卤素取代的苯酚反应来制备。 这些加合物对于（a）制备阻燃聚合物和（b）制备阻燃和耐光的有机纤维材料和阻燃，发光，起皱和抗收缩的织造和针织物是方便和有用的 含有约25％或更多纤维素纤维的纺织品。