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公开(公告)号：US3962251A
公开(公告)日：1976-06-08
申请号：US571164
申请日：1975-04-24
CPC分类号： C09B5/20 , C09B67/0025
摘要： A process for producing a new crystalline polymorphic form of flavanthrone is disclosed which comprises treating crude flavanthrone with nitric acid. This new form exhibits only one prominent X-ray diffraction peak between 7.00 and 8.00 dA and only two prominent peaks between 3.30 and 3.75 dA. In contrast to the known form of flavanthrone, the new form exhibits desirable transparent mass tones when employed as a pigment.
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2.发明授权
公开(公告)号：US5247088A
公开(公告)日：1993-09-21
申请号：US738086
申请日：1991-07-30
申请人： Thomas R. Flatt
发明人： Thomas R. Flatt
IPC分类号： C07D471/06 , C09B5/62
CPC分类号： C09B5/62
摘要： This invention relates to a novel process for the continuous preparation of perylenetetracarboxylic diimides by fusion of a naphthalimide in a mixture of an alkali metal hydroxide and, optionally, an alkali metal carboxylate to form an initial leuko condensation product that is subsequently oxidized in an aqueous medium to form the perylenetetracarboxylic diimide.
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公开(公告)号：US6068695A
公开(公告)日：2000-05-30
申请号：US352896
申请日：1999-07-13
申请人： Thomas R. Flatt , Mark A. Putnam , Ulrich Feldhues
发明人： Thomas R. Flatt , Mark A. Putnam , Ulrich Feldhues
IPC分类号： C07D471/04 , C09B48/00 , C07D515/00
CPC分类号： C09B48/00
摘要： This invention relates to a continuous process for the preparation of quinacridone pigments by(a) preparing a reaction mixture by mixing(i) a 2,5-dianilinoterephthalic acid or ester thereof, and(ii) at least about 0.5 parts by weight, per part of component (a)(i), of a dehydrating agent;(b) passing the reaction mixture through a continuous reactor having one or more heated zones at a temperature of about 80.degree. C. to about 300.degree. C. to form a crude quinacridone composition; and(c) mixing a continuous stream of the crude quinacridone composition with a liquid in which the quinacridone pigment is substantially insoluble at a ratio of about 0.5 to about 15 parts by weight of the liquid per part by weight of the crude quinacridone composition.
摘要翻译： 本发明涉及通过以下方法制备喹吖啶酮颜料的连续方法：（a）通过混合（i）2,5-二苯胺基对苯二甲酸或其酯制备反应混合物，和（ii）至少约0.5重量份， 脱水剂组分（a）（i）的一部分; （b）使反应混合物通过具有一个或多个加热区域的连续反应器，温度在约80℃至约300℃，以形成粗喹吖酮酮组合物; 和（c）将粗喹吖啶酮组合物的连续流与其中喹吖啶酮颜料基本上不溶的液体以每重量份粗喹吖啶酮组合物约0.5至约15重量份的液体的比例混合。
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公开(公告)号：US5753030A
公开(公告)日：1998-05-19
申请号：US645368
申请日：1996-05-13
申请人： Thomas R. Flatt , Mark W. Johnson
发明人： Thomas R. Flatt , Mark W. Johnson
CPC分类号： C09B5/62 , C09B67/0017 , C09B67/0025 , C09B67/0033
摘要： This invention relates to pigment compositions prepared by precipitating a blend of (a) about 60 to about 95 percent by weight of a perylene pigment having the formula ##STR1## wherein R.sup.1 and R.sup.2 are independently C.sub.1 -C.sub.6 alkyl, C.sub.5 -C.sub.7 cycloalkyl, C.sub.7 -C.sub.16 aralkyl, or C.sub.6 -C.sub.10 aryl; and (b) about 5 to about 40 percent by weight of a polycyclic aromatic compound containg at least 5 aromatic rings wherein at least one ring is substituted with at least one keto group.
摘要翻译： 本发明涉及通过沉淀（a）约60至约95重量％的具有下式的苝颜料的共混物制备的颜料组合物：其中R1和R2独立地为C1-C6烷基，C5-C7环烷基，C7 -C16芳烷基或C6-C10芳基; 和（b）约5至约40重量％的包含至少5个芳环的多环芳族化合物，其中至少一个环被至少一个酮基取代。
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公开(公告)号：US06432193B1
公开(公告)日：2002-08-13
申请号：US09461918
申请日：1999-12-15
IPC分类号： C09B562
CPC分类号： C09B67/0096 , C09B3/14 , C09B5/62
摘要： This invention relates to a continuous process for preparing perylenes by (a) continuously mixing a melt of the leuco form of a perylene tetracarboxylic diimide obtained by alkaline fusion of naphthalimide with a continuous water-containing stream containing (1) 2 to 50 parts of water per part of melt, (2) 0 to X1 moles of oxidizing agent per mole of the leuco form, (3) 0 to Y1 parts by weight of processing additives, based on the leuco form, and (4) 0 to Z1 parts by weight of an acid, based on the leuco form of the perylene tetracarboxylic diimide, to form a slurry; and (b) optionally mixing the slurry in one or more continuous or batchwise steps with a second stream containing (1) 0 to 10 parts by weight of water, based on the slurry, (2) 0 to X2 moles of oxidizing agent per mole of the leuco form of the perylene tetracarboxylic diimide, with the proviso the total of X1 and X2 represents at least the molar amount of oxidizing agent theoretically needed to oxidize all of the leuco form of the perylene tetracarboxylic diimide, (3) 0 to Y2 parts by weight of processing additives, based on the leuco form of the perylene tetracarboxylic diimide, with the proviso that the total of Y1 and Y2 is from 0 to 5 parts, and (4) 0 to Z2 parts by weight of an acid, based on the leuco form of the perylene tetracarboxylic diimide, to give a perylene pigment.
摘要翻译： 本发明涉及通过以下方法制备苝的连续方法：（a）将由萘二甲酰亚胺碱熔融获得的无色形式的苝四羧酸二酰亚胺的熔融物与含有（1）2至50份水的连续含水流连续混合 （2）每摩尔无色形式为0至1摩尔氧化剂，（3）0至Y1重量份的加工添加剂，基于无色形式，和（4）0至Z1份由 基于苝四羧酸二酰亚胺的无色形式的酸的重量以形成浆料; 和（b）任选地将浆料以一个或多个连续或分批步骤与含有（1）0至10重量份水的第二料流混合，基于浆料，（2）每摩尔0至2摩尔氧化剂 的苝四羧酸二酰亚胺的无色形式，条件是X1和X2的总和至少表示氧化所有无色形式的苝四羧酸二酰亚胺的氧化剂的摩尔量，（3）0至Y2部分 基于苝四羧酸二酰亚胺的无色形式的加工添加剂，条件是Y1和Y2的总和为0-5份，和（4）0至Z2重量份的酸，基于 苝四羧酸二酰亚胺的无色形式，得到苝颜料。
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公开(公告)号：US6013126A
公开(公告)日：2000-01-11
申请号：US200272
申请日：1998-11-25
CPC分类号： C09B67/0017 , C09B67/0014
摘要： This invention relates to a process for conditioning organic pigments by(a) grinding a crude organic pigment at a temperature of about 0.degree. C. to about 100.degree. C. in the presence of (i) about 1 to about 10 parts by weight, relative to the organic pigment, of an inorganic salt and (ii) about 1 to about 5 parts by weight, relative to the organic pigment, of a liquid in which the organic pigment and salt are substantially insoluble, to form a pigment paste;(b) grinding the pigment paste at a temperature of about 0.degree. C. to about 100.degree. C. in the presence of about 0.05 to about 1 parts by weight, relative to the organic pigment, of a C.sub.8 -C.sub.10 alkanoic acid to form a treated pigment paste;(c) stirring the treated pigment paste with water or water containing an acid and/or an organic liquid to complete the conditioning of the organic pigment; and(d) isolating the conditioned organic pigment.
摘要翻译： 本发明涉及一种通过以下步骤调理有机颜料的方法：（a）在（i）约1至约10重量份的存在下，在约0℃至约100℃的温度下研磨粗有机颜料， 相对于有机颜料，无机盐和（ii）相对于有机颜料约1至约5重量份的有机颜料和盐基本上不溶的液体，以形成颜料糊料; （b）在相对于有机颜料约0.05至约1重量份的存在下，在约0℃至约100℃的温度下研磨颜料糊状物以形成C 8 -C 10链烷酸 经处理的颜料糊; （c）用含有酸和/或有机液体的水或水搅拌经处理的颜料糊，以完成有机颜料的调理; 和（d）分离调节的有机颜料。
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公开(公告)号：US4493734A
公开(公告)日：1985-01-15
申请号：US497379
申请日：1983-05-23
申请人： Thomas R. Flatt
发明人： Thomas R. Flatt
CPC分类号： C09B67/0022
摘要： Process for the conditioning of a pigment by applying shear to a crude pigment in the presence of a liquid conditioning agent selected from the group consisting of corn syrup, corn syrup solids and molasses and optionally in the presence of a viscosity modifying agent, in a medium which is essentially free from an added inorganic salt.
摘要翻译： 在选自玉米糖浆，玉米糖浆固体和糖蜜以及任选在粘度调节剂存在下的液体调节剂存在下，在培养基中对颜料施加剪切以调节颜料的方法 其基本上不含添加的无机盐。
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