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公开(公告)号：US20030207220A1
公开(公告)日：2003-11-06
申请号：US10351366
申请日：2003-01-27
发明人： Mitsuo Saitou , Masaaki Miki , Katsuhisa Ohzeki
IPC分类号： G03C001/015 , G03C001/035
CPC分类号： G03C1/015
摘要： A producing method of a silver halide emulsion comprising the steps of adding silver halide fine grains AgX0 having an to a silver halide seed crystal emulsion containing at least water, dispersion medium 1 and silver halide crystal, and growing the seed crystal by dissolving the added AgX0, wherein AgX0 are formed in dispersion medium solution 2 containing dispersion medium 2, the pH of dispersion medium solution 2 of the time when AgX0 are formed is from 7.3 to 12.2, the average equivalent-circle projected area diameter of AgX0 is from 0.001 to 0.2 nullm, and AgX0 are non-twin crystal grains not substantially having twin planes.
摘要翻译： 一种卤化银乳剂的制备方法，包括以下步骤：向至少含有水，分散介质1和卤化银晶体的卤化银晶种乳液中加入具有卤化银细粒AgX0的步骤，并通过将所加入的AgX0 其中AgX0在含有分散介质2的分散介质溶液2中形成，AgX0形成时的分散介质溶液2的pH为7.3〜12.2，AgX0的平均当量圆投影面积直径为0.001〜0.2 妈妈和AgX0是基本上不具有双平面的非双晶晶粒。
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2.发明申请公开(公告)号：US20020068249A1
公开(公告)日：2002-06-06
申请号：US10053374
申请日：2001-11-09
IPC分类号： G03C001/015
CPC分类号： G03C1/0051 , G03C1/043 , G03C2200/43 , G03C2200/44
摘要： The invention relates to a method for preparing photographic silver halide tabular grains emulsions. The method of the invention comprises a first single nucleation step wherein stable tabular seeds of silver halide are formed, and a second step wherein different batches of seeds obtained in the first step are grown to yield identical or different emulsions. This combination of steps represent a robust process for preparing tabular grain emulsions at different scales.
摘要翻译： 本发明涉及一种制备照相卤化银片状颗粒乳剂的方法。 本发明的方法包括形成稳定的卤化银片状种子的第一单一成核步骤，第二步是生长第一步中获得的不同批次的种子以产生相同或不同的乳液。 这种步骤的组合代表了制备不同尺度的片状颗粒乳剂的可靠工艺。
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公开(公告)号：US20020058215A1
公开(公告)日：2002-05-16
申请号：US09962078
申请日：2001-09-26
IPC分类号： G03C001/035 , G03C001/015
CPC分类号： G03C1/0051 , G03C1/047 , G03C1/07 , G03C2001/0153 , G03C2001/0357 , G03C2200/03
摘要： A silver halide photographic light-sensitive material is disclosed, comprising at least one silver halide emulsion characterized in that 50% or more of the projected area of all silver halide grains comprises tabular silver halide grains satisfying all of the following requirements (i) to (iii) and the coefficient of variation in the thickness of the tabular silver halide grains is less than 40%: (i) to have a grain thickness of less than 0.05 nullm and an equivalent-circle diameter of 0.6 nullm or more; (ii) to be silver iodobromide or silver chloroiodobromide having a silver bromide content of 70 mol% or more; (iii) to be a tabular silver halide grain having two parallel main planes comprising a (111) face.
摘要翻译： 公开了一种卤化银照相感光材料，其包含至少一种卤化银乳剂，其特征在于所有卤化银颗粒的投影面积的50％或更多包括满足以下所有要求（I）至（ iii）并且片状卤化银颗粒的厚度变化系数小于40％：（i）具有小于0.05μm的颗粒厚度和0.6μm或更大的当量圆直径; （ii）为碘溴化银或溴化银含量为70摩尔％以上的氯碘溴化银; （iii）为具有包括（111）面的两个平行主平面的片状卤化银颗粒。
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4.发明申请Method and apparatus for forming silver halide emulsion particles and method for forming fine particles 失效用于形成卤化银乳剂颗粒的方法和设备及形成细颗粒的方法公开(公告)号：US20030224308A1
公开(公告)日：2003-12-04
申请号：US10420926
申请日：2003-04-23
发明人： Yasunori Ichikawa , Katsuhisa Ohzeki , Fumiko Shiraishi , Tetsurou Mitsui , Shigeharu Urabe , Nobuo Nishida , Kenichi Harashima
IPC分类号： G03C001/015
CPC分类号： B01F5/0256 , B01F2215/0409 , B01J19/26 , G03C1/015 , Y10S423/09 , Y10S423/11 , Y10T137/87603 , Y10T137/87652
摘要： The mixing state of static mixing is optimized, so that it is possible to form silver halide emulsion particles in small sizes with an excellent mono-dispersion characteristic. An aqueous solution of haloid salt is blown out from a first nozzle into a mixing chamber as a rectilinear flow of turbulent flow, and before eddy viscosity formed when the rectilinear flow is blown out from the first nozzle of a small diameter to the mixing chamber of a greater diameter reaches a maximum, or before a maximum flow speed of the rectilinear flow is reduced to {fraction (1/10)} or below, an aqueous solution of silver nitrate is blown out from a second nozzle as a crossflow of turbulent flow which crosses the rectilinear flow at a substantially right angle and is entrained by the rectilinear flow, so that the two solutions are allowed to mix and react with each other instantaneously, and a liquid resulting from the mixing and reaction is discharged from a discharge duct.
摘要翻译： 优化静态混合的混合状态，从而可以形成具有优异的单分散特性的小尺寸的卤化银乳剂颗粒。 将卤素盐的水溶液从第一喷嘴吹入混合室，作为湍流的直线流动，并且在直线流从小直径的第一喷嘴吹送到混合室的混合室之前形成的涡流粘度 更大的直径达到最大值，或者在直线流量的最大流速降低到{分数（1/10或更低）之前，硝酸银的水溶液从第二喷嘴吹出，作为湍流的交叉流， 直线流以基本上直角流动并被直线流动夹带，使得两种溶液瞬间混合和反应，并且从混合和反应产生的液体从排出管排出。
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5.发明申请Silver halide photographic emulsion and light-sensitive material containing the same 失效卤化银照相乳剂和含有相同的感光材料公开(公告)号：US20030077550A1
公开(公告)日：2003-04-24
申请号：US10186975
申请日：2002-07-02
发明人： Makoto Kikuchi , Naohiro Takeda , Yoichi Maruyama , Yuzo Toda , Masaaki Miki
IPC分类号： G03C001/015
CPC分类号： G03C1/0051 , G03C1/047 , G03C2001/0055 , G03C2001/0058 , G03C2001/03511
摘要： A silver halide photographic emulsion comprising silver halide grains is disclosed, which is obtained through a process including at least one step of forming grains using a dispersion medium having a low viscosity, wherein 50% or more of the entire projected area of all silver halide grains in the emulsion is occupied by silver halide tabular grains having an aspect ratio of 4 or more and a twin plane spacing of 0.012 nullm or less. Further disclosed is a silver halide color photographic light-sensitive material using the emulsion.
摘要翻译： 公开了包含卤化银颗粒的卤化银照相乳剂，其通过包括使用具有低粘度的分散介质形成晶粒的至少一个步骤的方法获得，其中所有卤化银颗粒的整个投影面积的50％或更多 在乳液中占据了长宽比为4以上，双面间隔为0.012μm以下的卤化银片状颗粒。 进一步公开了使用该乳液的卤化银彩色照相感光材料。
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6.发明申请Silver halide emulsion, production process thereof and novel pyridinium compound 失效卤化银乳剂，其制备方法和新型吡啶鎓化合物公开(公告)号：US20020155399A1
公开(公告)日：2002-10-24
申请号：US10059003
申请日：2002-01-30
IPC分类号： G03C001/015 , G03C001/035 , G03C001/047
CPC分类号： G03C1/07 , G03C1/0051 , G03C1/047 , G03C2001/0153 , G03C2200/03 , G03C2200/43
摘要： A silver halide emulsion comprising tabular grains having a very small thickness with the main surfaces thereof having a very large surface area and being (111) face, is disclosed. More specifically, a silver halide emulsion is disclosed, comprising light-sensitive silver halide grains having a silver bromide content of 70 mol % or more, with 60% or more of the entire projected area of said silver halide grains being occupied by tabular grains having an average grain thickness of less than 0.04 nullm, an average equivalent-circle diameter of 4 nullm or more, and (111) face as main surfaces.
摘要翻译： 公开了一种卤化银乳剂，其包含具有非常小的厚度的片状颗粒，其主表面具有非常大的表面积并且为（111）面。 更具体地，公开了一种卤化银乳剂，其包含具有70摩尔％以上的溴化银含量的感光卤化银颗粒，所述卤化银颗粒的整个投影面积的60％或更多被片状颗粒所占据， 平均粒度小于0.04μm，平均当量圆直径为4μm以上，（111）面为主面。
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公开(公告)号：US20030232291A1
公开(公告)日：2003-12-18
申请号：US10387220
申请日：2003-03-13
IPC分类号： G03C001/015 , G03C001/035
CPC分类号： G03C1/035 , G03C1/015 , G03C2001/03511 , G03C2001/03517 , G03C2001/03535 , G03C2001/0357 , G03C2200/60
摘要： The invention provides a silver halide emulsion, comprising: silver halide grains containing silver chloride as a primary component and further containing silver bromide; wherein, when an average value of a silver bromide content of the silver halide grains is represented by Y (mol %), a silver bromide content of at least 68% of the silver halide grains is from 0.82nullY (mol %) to 1.18nullY (mol %). Further, the invention provides a method of producing the silver halide emulsion, comprising the step of reacting at least a silver ion, a chlorine ion and a bromine ion; wherein a growth speed at a time of forming a silver bromine-containing phase in the reaction process is at least 60% of a critical growth speed.
摘要翻译： 本发明提供一种卤化银乳剂，其包含：含有氯化银作为主要成分并且还含有溴化银的卤化银颗粒; 其中，当卤化银颗粒的溴化银含量的平均值由Y（mol％）表示时，卤化银颗粒的至少68％的溴化银含量为0.82×Y（mol％）至1.18×Y （mol％）。 此外，本发明提供了一种制备卤化银乳剂的方法，包括使至少一种银离子，氯离子和溴离子反应的步骤; 其中在反应过程中形成含溴的相的相时的生长速度为临界生长速度的至少60％。
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公开(公告)号：US20030224305A1
公开(公告)日：2003-12-04
申请号：US10391642
申请日：2003-03-20
发明人： Mitsuo Saitou , Satoshi Aiba , Sumito Yamada , Eiichi Okutsu
IPC分类号： G03C001/015 , G03C001/035
CPC分类号： G03C1/035 , G03C1/015 , G03C1/49818 , G03C2001/03558 , G03C2001/03594 , G03C2200/01
摘要： A silver halide emulsion comprises at least a dispersion medium, water and a silver halide grain, wherein grains occupying from 40 to 100% of the total projected area of said gains have an AgI content of 85 to 100 mol %, a single kind of outer shape except for size and the equivalent-circle projected diameter of from 0.002 to 20 nullm
摘要翻译： 卤化银乳剂至少包括分散介质，水和卤化银颗粒，其中占所述增益总投影面积的40-100％的颗粒的AgI含量为85-100mol％，一种外部的 形状，除了尺寸和等效圆投影直径为0.002至20毫米
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公开(公告)号：US20030148234A1
公开(公告)日：2003-08-07
申请号：US10252433
申请日：2002-09-24
发明人： Mitsuo Saitou , Masaaki Miki , Katsuhisa Ohzeki
IPC分类号： G03C001/015 , G03C001/035
CPC分类号： G03C1/015
摘要： A producing method of a silver halide emulsion comprising the steps of adding silver halide fine grains AgX0 having an to a silver halide seed crystal emulsion containing at least water, dispersion medium 1 and silver halide crystal, and growing the seed crystal by dissolving the added AgX0, wherein AgX0 are formed in dispersion medium solution 2 containing dispersion medium 2, the pH of dispersion medium solution 2 of the time when AgX0 are formed is from 7.3 to 12.2, the average equivalent-circle projected area diameter of AgX0 is from 0.001 to 0.2 nullm, and AgX0 are non-twin crystal grains not substantially having twin planes.
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公开(公告)号：US20030108828A1
公开(公告)日：2003-06-12
申请号：US10186392
申请日：2002-07-01
IPC分类号： G03C001/015
摘要： In the apparatus for liquid preparation, the silver halide emulsion contained in a dedicated pot is transferred as liquid by a mohno pump via a piping into a measuring tank. The silver halide emulsion transferred into the measuring tank is measured with a load cell and is melted by heating with a jacket while being stirred by a stirrer. Accordingly, even when a small amount is used as in the case of the silver halide emulsion used in the heat-developable photosensitive material, the time for heating the silver halide emulsion, within the time range from the liquid preparation of the silver halide emulsion to its utilization, can be made short to the utmost, and hence the time elapse in melt can be suppressed. Thus, the time elapse in melt, reagent loss, and mutual contamination in the liquid preparation of photographic reagents can be effectively prevented. Under the preparation condition that the silver halide grains are prepared by adding a solution of a water soluble silver salt at an addition rate equal to or larger than 4 kg/min as converted to the weight of silver, the circulating flux of the circulating current at an opening for circulation is set to be equal to or larger than 500 L/min. By setting the circulating flux of the circulating current to be equal to or larger than 500 L/min., the two solutions added from reacting solution feeding pipes can be instantly diluted by a colloidal solution. Thus, the grain diameter and distribution width thereof can be made small in the preparation of silver halide grains for the purpose of producing a silver halide emulsion.
摘要翻译： 在用于液体制备的装置中，包含在专用罐中的卤化银乳剂通过管状泵通过管状泵作为液体转移到测量罐中。 转移到测量罐中的卤化银乳剂用称重传感器测量，并在用搅拌器搅拌的同时用夹套加热熔化。 因此，即使使用少量，如在可热显影的感光材料中使用的卤化银乳剂的情况下，在从卤化银乳剂的液体制备到时间范围内加热卤化银乳剂的时间 其利用率可以最小化，因此可以抑制熔体中的时间流逝。 因此，可以有效地防止在照相试剂的液体制剂中的熔融时间，试剂损失和相互污染的时间。 在制备条件下，通过以等于或大于4kg /分钟的加入速率加入水溶性银盐溶液来制备卤化银颗粒，转化为银的重量，循环电流的循环通量在 用于循环的开口设定为等于或大于500L / min。 通过将循环电流的循环通量设定为500L / min以上，从反应溶液供给管添加的两种溶液可以立即用胶体溶液稀释。 因此，为了制造卤化银乳剂，可以使制备卤化银颗粒的粒径和分布宽度变小。
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