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    HIGHLY OXIDIZED GRAPHENE OXIDE AND METHODS FOR PRODUCTION THEREOF
    62.
    发明申请
    HIGHLY OXIDIZED GRAPHENE OXIDE AND METHODS FOR PRODUCTION THEREOF 审中-公开
    高度氧化的氧化石墨及其生产方法

    公开(公告)号：WO2011016889A2

    公开(公告)日：2011-02-10

    申请号：PCT/US2010/034905

    申请日：2010-05-14

    Applicant: WILLIAM MARSH RICE UNIVERSITY ,  TOUR, James, M. ,  KOSYNKIN, Dmitry, V.

    Inventor： TOUR, James, M. ,  KOSYNKIN, Dmitry, V.

    IPC: C08F301/00 ,  D01F9/12 ,  C01B31/00 ,  C01B21/082

    CPC classification number: C01B31/0476 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/192 ,  C01B32/23 ,  C09K8/032

    Abstract: A highly oxidized form of graphene oxide and methods for production thereof are described in various embodiments of the present disclosure. In general, the methods include mixing a graphite source with a solution containing at least one oxidant and at least one protecting agent and then oxidizing the graphite source with the at least one oxidant in the presence of the at least one protecting agent to form the graphene oxide. Graphene oxide synthesized by the presently described methods is of a high structural quality that is more oxidized and maintains a higher proportion of aromatic rings and aromatic domains than does graphene oxide prepared in the absence of at least one protecting agent. Methods for reduction of graphene oxide into chemically converted graphene are also disclosed herein. The chemically converted graphene of the present disclosure is significantly more electrically conductive than is chemically converted graphene prepared from other sources of graphene oxide.

    Abstract translation: 在本公开的各种实施方案中描述了高度氧化形式的石墨烯氧化物及其制备方法。 通常，所述方法包括将石墨源与含有至少一种氧化剂和至少一种保护剂的溶液混合，然后在至少一种保护剂存在下用至少一种氧化剂氧化石墨源以形成石墨烯 氧化物。 通过目前描述的方法合成的石墨烯氧化物具有比在不存在至少一种保护剂时制备的氧化石墨烯更高氧化并保持更高比例的芳族环和芳族结构域的高结构质量。 将石墨烯氧化物还原成化学转化的石墨烯的方法也在本文中公开。 本公开的化学转化的石墨烯比由其它氧化石墨烯源制备的化学转化的石墨烯显着更加导电。

    GRAPHENE NANORIBBONS PREPARED FROM CARBON NANOTUBES VIA ALKALI METAL EXPOSURE
    63.
    发明申请
    GRAPHENE NANORIBBONS PREPARED FROM CARBON NANOTUBES VIA ALKALI METAL EXPOSURE 审中-公开
    通过阿尔卡利金属暴露从碳纳米管制备的石墨纳米线

    公开(公告)号：WO2010147860A1

    公开(公告)日：2010-12-23

    申请号：PCT/US2010/038368

    申请日：2010-06-11

    Applicant: WILLIAM MARSH RICE UNIVERSITY ,  TOUR, James, M. ,  KOSYNKIN, Dmitry, V.

    Inventor： TOUR, James, M. ,  KOSYNKIN, Dmitry, V.

    IPC: C01B31/04

    CPC classification number: C01B31/0446 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/15 ,  C01B32/184 ,  C01B32/19 ,  C01B2204/06 ,  C07C1/32 ,  C07C15/20 ,  Y10S977/896

    Abstract: In various embodiments, the present disclosure describes processes for preparing functionalized graphene nanoribbons from carbon nanotubes. In general, the processes include exposing a plurality of carbon nanotubes to an alkali metal source in the absence of a solvent and thereafter adding an electrophile to form functionalized graphene nanoribbons. Exposing the carbon nanotubes to an alkali metal source in the absence of a solvent, generally while being heated, results in opening of the carbon nanotubes substantially parallel to their longitudinal axis, which may occur in a spiralwise manner in an embodiment. The graphene nanoribbons of the present disclosure are functionalized on at least their edges and are substantially defect free. As a result, the functionalized graphene nanoribbons described herein display a very high electrical conductivity that is comparable to that of mechanically exfoliated graphene.

    Abstract translation: 在各种实施方案中，本公开描述了从碳纳米管制备官能化石墨烯纳米带的方法。 通常，该方法包括在不存在溶剂的情况下将多个碳纳米管暴露于碱金属源，然后加入亲电体以形成官能化的石墨烯纳米带。 通常在加热的情况下，将碳纳米管暴露于碱金属源，通常在加热的情况下导致碳纳米管的开放基本上平行于它们的纵向轴线，这在实施例中可能以螺旋方式发生。 本公开的石墨烯纳米带至少在其边缘上被官能化，并且基本上是无缺陷的。 因此，本文所述的功能化石墨烯纳米带显示出与机械剥离的石墨烯相当的非常高的电导率。

    VERTICALLY-STACKED ELECTRONIC DEVICES HAVING CONDUCTIVE CARBON FILMS
    66.
    发明申请
    VERTICALLY-STACKED ELECTRONIC DEVICES HAVING CONDUCTIVE CARBON FILMS 审中-公开
    具有导电碳膜的垂直电子装置

    公开(公告)号：WO2009064842A1

    公开(公告)日：2009-05-22

    申请号：PCT/US2008/083337

    申请日：2008-11-13

    Applicant: WILLIAM MARSH RICE UNVIRSITY ,  TOUR, James, M. ,  LI, Yubao ,  SINITSKIY, Alexander ,  ZHONG, Lin ,  DONG, Mian ,  YAO, Jun

    Inventor： TOUR, James, M. ,  LI, Yubao ,  SINITSKIY, Alexander ,  ZHONG, Lin ,  DONG, Mian ,  YAO, Jun

    IPC: H01L27/24 ,  H01L45/00

    CPC classification number: H01L45/04 ,  H01L27/2481 ,  H01L45/1233 ,  H01L45/124 ,  H01L45/149 ,  H01L45/1616

    Abstract: Vertically-stacked electronic devices having conductive carbon films are disclosed. The vertically-stacked devices exhibit non-linear current-versus-voltage response over a voltage sweep range in various embodiments. The vertically-stacked devices may be assembled into arrays where the vertically-stacked devices may be electrically addressed independently of one another. Uses of the vertically-stacked electronic devices and arrays as two-terminal memory devices, logic units, and sensors are disclosed. Crossbar arrays of vertically-stacked electronic devices having conductive carbon films and nanowire electrodes are disclosed.

    Abstract translation: 公开了具有导电碳膜的垂直堆叠的电子器件。 在各种实施例中，垂直堆叠的器件在电压扫描范围内表现出非线性电流对电压响应。 垂直堆叠的器件可以组装成阵列，其中垂直堆叠的器件可以彼此独立地电寻址。 公开了垂直堆叠的电子设备和阵列作为双端存储器件，逻辑单元和传感器的用途。 公开了具有导电碳膜和纳米线电极的垂直堆叠的电子器件的横杆阵列。

    PROCESSES FOR MAKING COMPOSITES AND BLENDS OF LOOSE SINGLE-WALLED CARBON NANOTUBE ROPES (SWNT-RS) AND OTHER CARBON NANOTUBE ROPES WITH ACID SOLUBLE POLYMERS AND OTHER MATERIALS, AND PRODUCTS MADE THEREFROM
    69.
    发明申请
    PROCESSES FOR MAKING COMPOSITES AND BLENDS OF LOOSE SINGLE-WALLED CARBON NANOTUBE ROPES (SWNT-RS) AND OTHER CARBON NANOTUBE ROPES WITH ACID SOLUBLE POLYMERS AND OTHER MATERIALS, AND PRODUCTS MADE THEREFROM 审中-公开
    制备复合材料和松散单层碳纳米管（SWNT-RS）和其他碳纳米管的混合物与酸溶性聚合物和其他材料的制备方法及其制备方法

    公开(公告)号：WO2008140533A3

    公开(公告)日：2009-02-12

    申请号：PCT/US2007077026

    申请日：2007-08-28

    Applicant: UNIV RICE WILLIAM M ,  HWANG WEN-FANG ,  CHEN ZHEYI ,  TOUR JAMES M

    Inventor： HWANG WEN-FANG ,  CHEN ZHEYI ,  TOUR JAMES M

    IPC: C08J3/21 ,  C08J3/215 ,  C08K9/04

    CPC classification number: C08J5/005 ,  B82Y30/00 ,  C08J3/215 ,  C08K9/04

    Abstract: Processes to make these composite materials or blends, and their shaped articles such as fibers, films and 3-D parts include mixing an acid intercalated SWNT-Rs with an acid soluble polymer and subjecting the resultant mixture to shear stresses. Composites and blends include loose single-walled carbon nanotube ropes (SWNT-Rs) and other acid-intercalatable carbon nanotube ropes with polymers such as aliphatic polyamides (nylon), aromatic polyamides (such as poly-p-phenylene terephthalamide, PPTA), or heterocyclic aromatic polymers (such as poly-p-phenylenebisbenzoxazole, PBO), or other materials which are soluble in common acidic media. Products such as fibers, films, and 3-dimensional articles are made from these materials.

    Abstract translation: 制备这些复合材料或共混物及其成型制品如纤维，膜和3-D部分的方法包括将酸插层的SWNT-Rs与酸溶性聚合物混合并使所得混合物经受剪切应力。 复合材料和共混物包括松散的单壁碳纳米管绳索（SWNT-Rs）和其它具有聚合物如酸性可嵌入碳纳米管绳索的聚合物，例如脂族聚酰胺（尼龙），芳族聚酰胺（例如聚对苯二甲酰对苯二胺，PPTA）或 杂环芳族聚合物（如聚对亚苯基双苯并恶唑，PBO）或其它可溶于普通酸性介质的材料。 诸如纤维，薄膜和三维制品的产品由这些材料制成。

    PREPARATION OF THIN FILM TRANSISTORS (TFTs) OR RADIO FREQUENCY IDENTIFICATION (RFID) TAGS OR OTHER PRINTABLE ELECTRONICS USING INK-JET PRINTER AND CARBON NANOTUBE INKS
    70.
    发明申请
    PREPARATION OF THIN FILM TRANSISTORS (TFTs) OR RADIO FREQUENCY IDENTIFICATION (RFID) TAGS OR OTHER PRINTABLE ELECTRONICS USING INK-JET PRINTER AND CARBON NANOTUBE INKS 审中-公开
    使用喷墨打印机和碳纳米管墨水制备薄膜晶体管（TFT）或无线电频率识别（RFID）标签或其他可打印电子

    公开(公告)号：WO2007089322A3

    公开(公告)日：2008-03-06

    申请号：PCT/US2006045388

    申请日：2006-11-24

    Applicant: UNIV RICE WILLIAM M ,  CHO GYOU-JIN ,  JUNG MIN HUN ,  HUDSON JARED L ,  TOUR JAMES M

    Inventor： CHO GYOU-JIN ,  JUNG MIN HUN ,  HUDSON JARED L ,  TOUR JAMES M

    IPC: H01L51/10

    CPC classification number: H01L51/0005 ,  B82Y10/00 ,  H01L51/0022 ,  H01L51/0048 ,  H01L51/0049 ,  H01L51/0545 ,  Y10S977/847 ,  Y10S977/938

    Abstract: The invented ink-jet printing method for the construction of thin film transistors using all SWNTs on flexible plastic films is a new process. This method is more practical than all of exiting printing methods in the construction TFT and RFID tags because SWNTs have superior properties of both electrical and mechanical over organic conducting oligomers and polymers which often used for TFT. Furthermore, this method can be applied on thin films such as paper and plastic films while silicon based techniques can not used on such flexible films. These are superior to the traditional conducting polymers used in printable devices since they need no dopant and they are more stable. They could be used in conjunction with conducting polymers, or as stand-alone inks.

    Abstract translation: 本发明的用于在柔性塑料薄膜上构造使用所有SWNT的薄膜晶体管的喷墨打印方法是一个新的过程。 该方法比建筑TFT和RFID标签中的所有现有印刷方法更实用，因为SWNT具有优于常用于TFT的有机导电低聚物和聚合物的电和机械性能。 此外，该方法可以应用于诸如纸和塑料膜的薄膜上，而基于硅的技术不能用于这种柔性膜。 它们优于用于可印刷装置的传统导电聚合物，因为它们不需要掺杂剂并且它们更稳定。 它们可以与导电聚合物一起使用，或者作为独立的油墨使用。

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