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    TUNGSTEN OXIDE PHOTOCATALYST AND METHOD FOR PRODUCING THE SAME
    1.
    发明申请
    TUNGSTEN OXIDE PHOTOCATALYST AND METHOD FOR PRODUCING THE SAME 审中-公开
    氧化钨光催化剂及其制备方法

    公开(公告)号：WO2012169390A1

    公开(公告)日：2012-12-13

    申请号：PCT/JP2012/063827

    申请日：2012-05-23

    Applicant: SHOWA DENKO K.K. ,  HOSOGI Yasuhiro ,  KURODA Yasushi

    Inventor： HOSOGI Yasuhiro ,  KURODA Yasushi

    IPC: B01J35/00 ,  B01J37/00 ,  B01J21/06 ,  B01J23/888 ,  B01J37/03

    CPC classification number: B01J23/888 ,  B01J21/063 ,  B01J35/0013 ,  B01J35/002 ,  B01J35/004 ,  B01J37/00 ,  B01J37/033 ,  B82Y40/00 ,  Y10S977/779 ,  Y10S977/811 ,  Y10S977/892

    Abstract: The present invention relates to a method for producing a tungsten oxide photocatalyst having titanium oxide and copper ion supported thereon, comprising dissolving urea in a solution in which copper-ion supporting tungsten oxide particles are uniformly dispersed in a titanium oxide sol, thermally decomposing the urea to thereby allow the titanium oxide to precipitate on the surface of copper ion-supporting tungsten oxide and to be supported thereon; and a tungsten oxide photocatalyst modified by both titanium oxide and copper ion obtained by the method, wherein the rate of change of diffuse reflectivity (at wavelength of 700 nm) is less than 3% before and after the irradiation of ultraviolet and the titanium oxide is supported on the tungsten oxide in an island shape of 1 to 100 nm in size. The tungsten oxide photocatalyst having titanium oxide and copper ion supported thereon of the present invention exhibits high catalyst activity under visible light irradiation.

    Abstract translation: 本发明涉及一种其上负载有氧化钛和铜离子的氧化钨光催化剂的制造方法，其特征在于，将尿素溶解在氧化钛溶胶中均匀分散有铜离子的氧化钨粒子的溶液中， 从而允许氧化钛在负载有铜离子的氧化钨的表面上沉淀并负载在其上; 以及通过该方法获得的氧化钛和铜离子改性的氧化钨光催化剂，其中在紫外线照射前后的漫反射率（波长700nm）的变化率小于3％，氧化钛为 负载在尺寸为1〜100nm的岛状的氧化钨上。 本发明的负载有氧化钛和铜离子的氧化钨光催化剂在可见光照射下显示出高的催化剂活性。

    METHOD AND APPARATUS FOR PRODUCING METAL OXIDE PARTICLES
    5.
    发明申请
    METHOD AND APPARATUS FOR PRODUCING METAL OXIDE PARTICLES 审中-公开

    公开(公告)号：WO2011111848A3

    公开(公告)日：2011-09-15

    申请号：PCT/JP2011/055864

    申请日：2011-03-07

    Applicant: NATIONAL UNIVERSITY CORPORATION HOKKAIDO UNIVERSITY ,  SHOWA DENKO K.K. ,  OHTANI Bunsho ,  SUGISHITA Noriyuki ,  KURODA Yasushi

    Inventor： OHTANI Bunsho ,  SUGISHITA Noriyuki ,  KURODA Yasushi

    IPC: C01B13/22 ,  C01G23/07 ,  C01G1/02

    Abstract: There is provided a method and an apparatus for producing metal oxide particles, which produce metal oxide particles having a high photocatalytic activity with high yield. The method for producing metal oxide particles of the invention is characterized by including combining, in a reaction tube, a preheated metal chloride-containing gas with a preheated first gas which does not contain the metal chloride at a first junction to obtain a first combined gas, and combining the first combined gas with a preheated second gas which does not contain the metal chloride, at a second junction which is further downstream of the first junction, to obtain a second combined gas, wherein at least one of the metal chloride-containing gas and the first gas contains oxygen, and wherein the preheated metal chloride-containing gas is further heated in a region between the first junction and the second junction (referred to as first reaction zone), by combining the first gas with the metal chloride-containing gas at the first junction while setting the preheat temperature of the first gas at a temperature equal to or higher than the preheat temperature of the metal chloride-containing gas, and the first combined gas is further heated in a region downstream of the second junction by combining the second gas with the first combined gas at the second junction while setting the preheat temperature of the second gas at a temperature equal to or higher than the temperature of the first combined gas.

    METHOD AND APPARATUS FOR PRODUCING METAL OXIDE PARTICLES
    8.
    发明申请
    METHOD AND APPARATUS FOR PRODUCING METAL OXIDE PARTICLES 审中-公开
    用于生产金属氧化物颗粒的方法和装置

    公开(公告)号：WO2011111848A2

    公开(公告)日：2011-09-15

    申请号：PCT/JP2011055864

    申请日：2011-03-07

    Applicant: UNIV HOKKAIDO NAT UNIV CORP ,  SHOWA DENKO KK ,  OHTANI BUNSHO ,  SUGISHITA NORIYUKI ,  KURODA YASUSHI

    Inventor： OHTANI BUNSHO ,  SUGISHITA NORIYUKI ,  KURODA YASUSHI

    IPC: C01B13/22

    CPC classification number: C01B13/22 ,  C01G1/02 ,  C01G23/07 ,  C01P2002/30 ,  C01P2004/03 ,  C01P2006/12 ,  C01P2006/90

    Abstract: There is provided a method and an apparatus for producing metal oxide particles, which produce metal oxide particles having a high photocatalytic activity with high yield. The method for producing metal oxide particles of the invention is characterized by including combining, in a reaction tube, a preheated metal chloride-containing gas with a preheated first gas which does not contain the metal chloride at a first junction to obtain a first combined gas, and combining the first combined gas with a preheated second gas which does not contain the metal chloride, at a second junction which is further downstream of the first junction, to obtain a second combined gas, wherein at least one of the metal chloride-containing gas and the first gas contains oxygen, and wherein the preheated metal chloride-containing gas is further heated in a region between the first junction and the second junction (referred to as first reaction zone), by combining the first gas with the metal chloride-containing gas at the first junction while setting the preheat temperature of the first gas at a temperature equal to or higher than the preheat temperature of the metal chloride-containing gas, and the first combined gas is further heated in a region downstream of the second junction by combining the second gas with the first combined gas at the second junction while setting the preheat temperature of the second gas at a temperature equal to or higher than the temperature of the first combined gas.

    Abstract translation: 提供了一种生产金属氧化物颗粒的方法和设备，其以高产率生产具有高光催化活性的金属氧化物颗粒。 本发明的金属氧化物粒子的制造方法的特征在于，在反应管中，将预热的含金属氯化物的气体与在第一接合处不含有金属氯化物的预热的第一气体组合，得到第一组合气体 并且在第二结合处将第一组合气体与不含金属氯化物的预热的第二气体组合，以获得第二组合气体，其中至少一种含金属氯化物的 气体，第一气体含有氧，并且其中预热的含金属氯化物的气体在第一接合点和第二接合点（称为第一反应区域）之间的区域中进一步加热，通过将第一气体与金属氯化物 - 在将第一气体的预热温度设定为等于或高于金属氯化物c的预热温度的温度的同时， 通过在第二连接处组合第二气体与第一组合气体，将第一组合气体在第二接合点的下游区域进一步加热，同时将第二气体的预热温度设定在等于或高于 第一组合气体的温度。

    SOL CONTAINING TITANIUM DIOXIDE, THIN FILM FORMED THEREFROM AND PRODUCTION PROCESS OF THE SOL
    9.
    发明申请
    SOL CONTAINING TITANIUM DIOXIDE, THIN FILM FORMED THEREFROM AND PRODUCTION PROCESS OF THE SOL 审中-公开
    包含二氧化钛的SOL，其形成的薄膜和SOL的生产工艺

    公开(公告)号：WO2005003035A3

    公开(公告)日：2005-03-31

    申请号：PCT/JP2004009888

    申请日：2004-07-05

    Applicant: SHOWA DENKO KK ,  WAKIZAKA YASUAKI ,  KURODA YASUSHI

    Inventor： WAKIZAKA YASUAKI ,  KURODA YASUSHI

    IPC: B01J21/06 ,  B01J23/42 ,  B01J23/52 ,  B01J23/745 ,  B01J35/00 ,  B01J35/10 ,  B01J37/02 ,  B01J37/03 ,  C01G20060101 ,  C01G23/00 ,  C01G23/053 ,  C09C1/36

    CPC classification number: B01J35/004 ,  B01J21/063 ,  B01J21/066 ,  B01J23/42 ,  B01J23/52 ,  B01J23/745 ,  B01J35/1014 ,  B01J35/1019 ,  B01J37/0219 ,  B01J37/033 ,  B82Y30/00 ,  C01G23/047 ,  C01G23/0536 ,  C01P2002/72 ,  C01P2004/64 ,  C01P2006/12 ,  C01P2006/60 ,  C09C1/3607 ,  C09C1/3661

    Abstract: A sol comprising a precipitated component in an amount of less than 10 mass% based on the total solid content of the sol and comprising titanium oxide comprising a transition metal compound. When the sol is mixed with a binder which can be hardened at ambient temperature, the mixture readily forms a thin film having high photocatalytic performance on a substrate of poor heat resistance such as plastics or paper. The titanium oxide sol can readily forms titanium oxide thin film on surfaces of a variety of substrate materials such as ceramics, glass, metal, plastics, wood, or paper. Articles to which photocatalytic performance or hydrophilicity is imparted include building materials, fluorescent lamps, glass panes, machinery, vehicles, glass products, household electrical appliances, water purifying apparatuses, agricultural materials, electronic apparatus, tools, tableware, bath products, toiletry products, furniture, clothing, cloth products, fibers, leather products, paper products, sporting goods, beauty-related instruments, health improvement instruments, medical goods, futon, containers, eyeglasses, signboards, piping, wiring, brackets, sanitary materials, and automobile parts as well as environmental purification apparatuses/units.

    Abstract translation: 一种溶胶，其包含基于所述溶胶的总固体含量小于10质量％的沉淀组分，并包含包含过渡金属化合物的氧化钛。 当溶胶与可在环境温度下硬化的粘合剂混合时，混合物容易在耐热性差的基材上形成具有高光催化性能的薄膜，例如塑料或纸。 氧化钛溶胶可以容易地在各种基材如陶瓷，玻璃，金属，塑料，木材或纸张的表面上形成氧化钛薄膜。 赋予光催化性能或亲水性的制品包括建筑材料，荧光灯，玻璃板，机械，车辆，玻璃制品，家用电器，净水装置，农用材料，电子仪器，工具，餐具，沐浴用品，化妆品， 家具，服装，布制品，纤维，皮革制品，纸制品，运动用品，美容仪器，健康改善仪器，医疗用品，日式，集装箱，眼镜，招牌，管道，布线，支架，卫生材料和汽车部件 以及环境净化设备/单位。

    SOL CONTAINING TITANIUM DIOXIDE, THIN FILM FORMED THEREFROM AND PRODUCTION PROCESS OF THE SOL
    10.
    发明申请
    SOL CONTAINING TITANIUM DIOXIDE, THIN FILM FORMED THEREFROM AND PRODUCTION PROCESS OF THE SOL 审中-公开
    含有二氧化钛的溶胶，由其形成的薄膜及其制造方法

    公开(公告)号：WO2005003035A2

    公开(公告)日：2005-01-13

    申请号：PCT/JP2004/009888

    申请日：2004-07-05

    Applicant: SHOWA DENKO K.K. ,  WAKIZAKA, Yasuaki ,  KURODA, Yasushi

    Inventor： WAKIZAKA, Yasuaki ,  KURODA, Yasushi

    IPC: C01G

    CPC classification number: B01J35/004 ,  B01J21/063 ,  B01J21/066 ,  B01J23/42 ,  B01J23/52 ,  B01J23/745 ,  B01J35/1014 ,  B01J35/1019 ,  B01J37/0219 ,  B01J37/033 ,  B82Y30/00 ,  C01G23/047 ,  C01G23/0536 ,  C01P2002/72 ,  C01P2004/64 ,  C01P2006/12 ,  C01P2006/60 ,  C09C1/3607 ,  C09C1/3661

    Abstract: A sol comprising a precipitated component in an amount of less than 10 mass% based on the total solid content of the sol and comprising titanium oxide comprising a transition metal compound. When the sol is mixed with a binder which can be hardened at ambient temperature, the mixture readily forms a thin film having high photocatalytic performance on a substrate of poor heat resistance such as plastics or paper. The titanium oxide sol can readily forms titanium oxide thin film on surfaces of a variety of substrate materials such as ceramics, glass, metal, plastics, wood, or paper. Articles to which photocatalytic performance or hydrophilicity is imparted include building materials, fluorescent lamps, glass panes, machinery, vehicles, glass products, household electrical appliances, water purifying apparatuses, agricultural materials, electronic apparatus, tools, tableware, bath products, toiletry products, furniture, clothing, cloth products, fibers, leather products, paper products, sporting goods, beauty-related instruments, health improvement instruments, medical goods, futon, containers, eyeglasses, signboards, piping, wiring, brackets, sanitary materials, and automobile parts as well as environmental purification apparatuses/units.

    Abstract translation: 包含基于溶胶的总固体含量小于10质量％的量的沉淀组分并且包含含有过渡金属化合物的氧化钛的溶胶。 当溶胶与可在环境温度下硬化的粘合剂混合时，该混合物容易在耐热性差的基材如塑料或纸上形成具有高光催化性能的薄膜。 氧化钛溶胶可容易地在陶瓷，玻璃，金属，塑料，木材或纸等各种基板材料的表面上形成氧化钛薄膜。 具有光催化性能或亲水性的物品包括建筑材料，荧光灯，玻璃窗，机械，车辆，玻璃制品，家用电器，净水器，农业材料，电子设备，工具，餐具，沐浴产品，化妆品， 家具，服装，布料制品，纤维，皮革制品，纸制品，体育用品，美容相关器具，健康改善工具，医疗用品，被褥，容器，眼镜，招牌，管道，接线，支架，卫生材料和汽车部件 以及环境净化设备/单元。

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