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公开(公告)号：WO2013074259A1
公开(公告)日：2013-05-23
申请号：PCT/US2012/061647
申请日：2012-10-24
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , THOMPSON, Wendy L. , NELSON, James M. , SCHULTZ, William J.
Inventor： THOMPSON, Wendy L. , NELSON, James M. , SCHULTZ, William J.
CPC classification number: C08K9/06 , B82Y30/00 , C08J5/005 , C08J5/10 , C08J5/24 , C08J2379/04 , C08K9/04 , C08L79/04
Abstract: There are provided curable resin sols having a curable polycyanate ester resin and at least 30 weight percent of an essentially volatile-free, colloidal dispersion of substantially spherical surface-modified silica nanoparticles; wherein the curable resin sol comprises no greater than 200 parts per million by weight alkali metal and alkaline earth metal ions based on the total weight of the silica nanoparticles and curable polycyanate ester resin. There are also provided compositions comprising such curable resin sol and reinforcing fibers, a process for preparing such compositions, and various articles made using such curable resin sols and compositions.
Abstract translation: 提供了具有可固化的聚氰酸酯树脂和至少30重量％的基本上无挥发性的基本上为球形的表面改性的二氧化硅纳米颗粒的胶体分散体的可固化树脂溶胶; 其中所述可固化树脂溶胶基于所述二氧化硅纳米颗粒和可固化聚氰酸酯树脂的总重量，包含不大于200重量份的碱金属和碱土金属离子。 还提供了包含这种可固化树脂溶胶和增强纤维的组合物，制备这种组合物的方法，以及使用这种可固化树脂溶胶和组合物制备的各种制品。
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公开(公告)号：WO2010080459A1
公开(公告)日：2010-07-15
申请号：PCT/US2009/068359
申请日：2009-12-17
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , SCHULTZ, William J., , HARALDSON, Chad A., , SCHULTZ, Nathan E., , THOMPSON, Wendy L., , THORSON, James E., , GOETZ, Douglas P., , HACKETT, Steven C., , NELSON, James M.,
Inventor： SCHULTZ, William J., , HARALDSON, Chad A., , SCHULTZ, Nathan E., , THOMPSON, Wendy L., , THORSON, James E., , GOETZ, Douglas P., , HACKETT, Steven C., , NELSON, James M.,
CPC classification number: C08L63/00
Abstract: Compositions comprising surface-modified nanocalcite particles dispersed in a curable resin, and to coatings and fibrous composites incorporating such compositions are described. The surface-modifying agents include a binding group ionically associated with the calcite and a compatiblizing segment, compatible with the curable resin. The surface-modifying agent may also include a reactive group capable of reacting with the curable resin. Methods of preparing nanocalcite composites and coating a fibrous composites prepared from such nanocalcite composites are also described.
Abstract translation: 描述了包含分散在可固化树脂中的表面改性纳米碳酸钙颗粒的组合物，以及包含这种组合物的涂料和纤维复合材料。 表面改性剂包括与方解石离子键合的结合基团和与可固化树脂相容的相容片段。 表面改性剂也可以包括能够与可固化树脂反应的反应性基团。 还描述了制备纳米碳酸钙复合材料和涂覆由这种纳米碳酸钙复合材料制备的纤维复合材料的方法。
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公开(公告)号：WO2009152301A3
公开(公告)日：2010-02-11
申请号：PCT/US2009047000
申请日：2009-06-11
Applicant: 3M INNOVATIVE PROPERTIES CO , GOENNER EMILY S , GREGAR TRAVIS Q , KOLB BRANT U , SCHULTZ WILLIAM J , THUNHORST KRISTIN L , HINE ANDREW M , NELSON JAMES M
Inventor： GOENNER EMILY S , GREGAR TRAVIS Q , KOLB BRANT U , SCHULTZ WILLIAM J , THUNHORST KRISTIN L , HINE ANDREW M , NELSON JAMES M
CPC classification number: C09C1/3081 , B82Y30/00 , C01P2004/03 , C01P2004/64 , C01P2006/22 , C08J5/005 , C08J2333/06 , C08K3/36 , C08K9/04 , C09C1/3063 , C09C1/3072 , C09D7/62
Abstract: Various methods of treating surface-modified nanoparticles are described. Dual-ion exchange procedures (anion exchange and cation exchange), as well-as subsequent end-capping are described. Both ionically-bonded and covalently-bonded end-capping agents are discussed. The resulting low ion content, particularly low alkali metal and alkaline metal oxide ion content, treated, surface-modified nanoparticles, including such nanoparticles in a resin system, are also disclosed. Effects of low ion content on various properties of the resulting resin system, including blister-resistance, optical clarity, and rheology are included.
Abstract translation: 描述了处理表面改性纳米颗粒的各种方法。 描述了双离子交换程序（阴离子交换和阳离子交换）以及随后的封端。 讨论了离子键合和共价键合的封端剂。 还公开了所得到的低离子含量，特别是低碱金属和碱金属氧化物离子含量，在树脂体系中处理的包括这种纳米颗粒的表面改性纳米颗粒。 包括低离子含量对所得树脂体系的各种性能的影响，包括防起泡，光学透明度和流变性。
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公开(公告)号：WO2009120846A3
公开(公告)日：2010-01-07
申请号：PCT/US2009038367
申请日：2009-03-26
Applicant: 3M INNOVATIVE PROPERTIES CO , TIEFENBRUCK GRANT F , ARCHIBALD MATTHEW N , NELSON JAMES M , THOMPSON WENDY L , SCHULTZ WILLIAM J , CONDO PETER D , KOLB BRANT U , BARAN JIMMIE R JR
Inventor： TIEFENBRUCK GRANT F , ARCHIBALD MATTHEW N , NELSON JAMES M , THOMPSON WENDY L , SCHULTZ WILLIAM J , CONDO PETER D , KOLB BRANT U , BARAN JIMMIE R JR
CPC classification number: C09C3/12 , B82Y30/00 , C01P2004/10 , C01P2004/32 , C01P2004/62 , C01P2004/64 , C09C1/3063 , C09C1/3081 , C09C1/309 , C09C3/08
Abstract: A method for the preparation of functionalized particles includes providing a feedstock that includes particles, a surface treatment agent reactive with the particles and solvent. The feedstock is direct through a continuous hydrothermal reactor maintained at a temperature sufficient to react the particles with the surface treatment agents to thereby provide functionalized particles. The method of the invention is capable of providing the functionalized particles in less than about 4 hours.
Abstract translation: 制备官能化颗粒的方法包括提供包含颗粒的原料，与颗粒和溶剂反应的表面处理剂。 原料直接通过维持在足以使颗粒与表面处理剂反应的温度的连续水热反应器，由此提供官能化的颗粒。 本发明的方法能够在少于约4小时内提供官能化颗粒。
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公开(公告)号：WO2007102984A1
公开(公告)日：2007-09-13
申请号：PCT/US2007/004426
申请日：2007-02-20
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , MARX, Ryan E. , NELSON, James M. , PINNOW, Matthew J. , SCHMID, Matthew J. , DAMS, Rudolf J. , DE WITTE, Johan E.
Inventor： MARX, Ryan E. , NELSON, James M. , PINNOW, Matthew J. , SCHMID, Matthew J. , DAMS, Rudolf J. , DE WITTE, Johan E.
IPC: C08F299/00 , C08F220/22 , C08F220/38 , C08F220/34
CPC classification number: C08F299/00
Abstract: A block copolymer; a method of reducing the surface tension of a liquid comprising adding to said liquid less than 10 wt % of a surface active agent derived from the block copolymer; a method for modifying the surface chemistry of a polymeric substrate comprising adding less than 10 wt % of a surface active agent derived from the block copolymer; a polymerized foam composition made from a mixture containing one or more of monomers, oligomers, and polymers, the mixture comprising less than 10 wt % of a surface active agent derived from the block copolymer and an article comprising the polymerized foam. A block copolymer comprising at least one block having a quaternary ammonium ion.
Abstract translation: 嵌段共聚物; 一种降低液体表面张力的方法，包括向所述液体中加入少于10重量％的衍生自嵌段共聚物的表面活性剂; 一种用于改性聚合物基材的表面化学性质的方法，包括加入少于10重量％的衍生自嵌段共聚物的表面活性剂; 由含有一种或多种单体，低聚物和聚合物的混合物制成的聚合泡沫组合物，所述混合物包含少于10重量％的衍生自嵌段共聚物的表面活性剂和包含聚合泡沫的制品。 包含至少一个具有季铵离子的嵌段的嵌段共聚物。
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Patent Agency Ranking
公开(公告)号：WO2013063057A1
公开(公告)日：2013-05-02
申请号：PCT/US2012/061609
申请日：2012-10-24
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , NELSON, James M. , THOMPSON, Wendy L. , SCHULTZ, William J.
Inventor： NELSON, James M. , THOMPSON, Wendy L. , SCHULTZ, William J.
CPC classification number: B29C70/48 , B29C70/52 , B82Y30/00 , C08J5/005 , C08K7/06 , C08K7/10 , C08K9/04 , C08L79/08 , C08L79/085 , Y10T442/20
Abstract: There are provided curable resin sols comprising an essentially volatile-free, colloidal dispersion of substantially spherical nanosilica particles in a curable bisimide resin, said particles having surface-bonded organic groups which render said particles compatible with said curable bisimide resin. There are also provided compositions comprising such curable resin sol and reinforcing fibers, a process for preparing such compositions, and various articles made using such curable resin sols and compositions.
Abstract translation: 提供了可固化树脂溶胶，其包含在可固化双酰亚胺树脂中基本上无挥发性的基本上为球形的纳米二氧化硅颗粒的胶态分散体，所述颗粒具有使所述颗粒与所述可固化双酰亚胺树脂相容的表面键合有机基团。 还提供了包含这种可固化树脂溶胶和增强纤维的组合物，制备这种组合物的方法，以及使用这种可固化树脂溶胶和组合物制备的各种制品。
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公开(公告)号：WO2009152404A1
公开(公告)日：2009-12-17
申请号：PCT/US2009/047150
申请日：2009-06-12
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , NELSON, James, M. , DECABOOTER, Daniel, P. , THORSON, James, E. , WU, Jung-sheng
Inventor： NELSON, James, M. , DECABOOTER, Daniel, P. , THORSON, James, E. , WU, Jung-sheng
IPC: C08F2/44
Abstract: Methods of compounding nanoparticles (e.g., surface-modified silica nanoparticles) with a resin (e.g., a curable resin) are described. The methods use continuous wet milling technology and can be used to compound nanoparticles, including highly aggregated and agglomerated surface-modified nanoparticles, into a resin or resin precursor.
Abstract translation: 描述了将纳米颗粒（例如表面改性的二氧化硅纳米颗粒）与树脂（例如可固化树脂）混合的方法。 该方法使用连续湿法研磨技术，可用于将纳米颗粒（包括高度聚集和附聚的表面改性纳米粒子）复合到树脂或树脂前体中。
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公开(公告)号：WO2009152296A1
公开(公告)日：2009-12-17
申请号：PCT/US2009/046992
申请日：2009-06-11
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , GOENNER, Emily, S. , GREGAR, Travis, Q. , KOLB, Brant, U. , SCHULTZ, William, J. , THUNHORST, Kristin, L. , HINE, Andrew, M. , NELSON, James, M.
Inventor： GOENNER, Emily, S. , GREGAR, Travis, Q. , KOLB, Brant, U. , SCHULTZ, William, J. , THUNHORST, Kristin, L. , HINE, Andrew, M. , NELSON, James, M.
CPC classification number: C09C1/3081 , B82Y30/00 , C01P2004/03 , C01P2004/64 , C01P2006/22 , C08J5/005 , C08J2333/06 , C08K3/36 , C08K9/04 , C09C1/3063 , C09C1/3072 , C09D7/62
Abstract: End-capped, surface-modified, silica nanoparticles are described. The resulting treated, surface-modified nanoparticles, including such nanoparticles in a resin system, are also disclosed. Effects of such surface treatments on various properties of the resulting resin system, including blister-resistance, optical clarity, and rheology are included.
Abstract translation: 描述了封端的表面改性的二氧化硅纳米颗粒。 还公开了在树脂体系中包含这些纳米颗粒的经处理的表面改性纳米粒子。 包括这种表面处理对所得树脂体系的各种性能的影响，包括耐起泡性，光学透明度和流变性。
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公开(公告)号：WO2009120868A3
公开(公告)日：2009-12-17
申请号：PCT/US2009038408
申请日：2009-03-26
Applicant: 3M INNOVATIVE PROPERTIES CO , NELSON JAMES M , ARCHIBALD MATTHEW N , KOLB BRANT U , THOMPSON WENDY L , SCHULTZ WILLIAM J , HACKETT STEVEN C
Inventor： NELSON JAMES M , ARCHIBALD MATTHEW N , KOLB BRANT U , THOMPSON WENDY L , SCHULTZ WILLIAM J , HACKETT STEVEN C
CPC classification number: C08J3/20 , B82Y30/00 , C08J5/005 , C08J2323/04
Abstract: A method of making a filled resin includes providing functionalized particles; and combining and homogenously mixing the functionalized particles with an organic matrix in a vacuum kneader to provide the filled resin so that the functionalized particles comprise at least about 20% by weight of the filled resin. The step of providing functionalized particles can also include providing a feedstock of (i) untreated particles, (ii) a surface treatment agent reactive with the particles, and (iii) solvent, and directing the feedstock through a continuous reactor maintained at a temperature sufficient to react the particles with the surface treatment agent to provide the functionalized particles in less than about 4 hours; and directing the functionalized particles from the continuous reactor directly into the vacuum kneader. In another aspect, the a finished resin comprises at least about 20% by weight of functionalized particles in an organic matrix
Abstract translation: 制备填充树脂的方法包括提供官能化颗粒; 并在真空捏合机中将官能化颗粒与有机基质混合并均匀混合以提供填充的树脂，使得官能化颗粒占填充树脂的至少约20重量％。 提供官能化颗粒的步骤还可以包括提供（i）未处理颗粒的原料，（ii）与颗粒反应的表面处理剂，和（iii）溶剂，并引导原料通过维持在足够温度的连续反应器 使颗粒与表面处理剂反应以在小于约4小时内提供官能化颗粒; 并将来自连续反应器的官能化颗粒直接引入真空捏合机中。 在另一方面，成品树脂包含至少约20重量％的有机基质中的官能化颗粒
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公开(公告)号：WO2009055403A2
公开(公告)日：2009-04-30
申请号：PCT/US2008080677
申请日：2008-10-22
Applicant: 3M INNOVATIVE PROPERTIES CO , MOLNAR ATTILA , NELSON JAMES M , D SOUZA ANDREW S
Inventor： MOLNAR ATTILA , NELSON JAMES M , D SOUZA ANDREW S
IPC: C09J4/00
CPC classification number: C08L23/10 , C08L23/26 , C09J4/06 , C09J123/26 , Y10T428/31515 , C08L2666/02
Abstract: A binder or sizing composition that is provided that demonstrates improved hydrolytic stability of the bond between a SiO containing substrate, such as glass, and a matrix polymer, such as polypropylene, which is especially useful in reinforced plastics. A water-based composition is provided that contains at least one amino-functional coupling agent, and acid or anhydride modified polyolefin, and an epoxy functional compound. This composition is useful as a glass binder or sizing to provide a strong bond between glass and a polymer.
Abstract translation: 所提供的粘合剂或施胶组合物提供了在含SiO的基材如玻璃与基体聚合物如聚丙烯之间的结合的改进的水解稳定性，所述基体聚合物特别用于增强塑料。 提供了含有至少一种氨基官能化偶联剂，酸或酸酐改性聚烯烃和环氧官能化合物的水基组合物。 该组合物可用作玻璃粘合剂或施胶剂以提供玻璃与聚合物之间的强结合。
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