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1.发明申请PROCESS FOR OBTAINING CARBOXYMETHYL CELLULOSE FROM AGRO-INDUSTRIAL RESIDUES AND CARBOXYMETHYL CELLULOSE AND USE THEREOF 审中-公开从农业工业残留物和羧甲基纤维素获得羧甲基纤维素的方法及其用途
公开(公告)号：WO2013166575A9
公开(公告)日：2014-07-03
申请号：PCT/BR2013000159
申请日：2013-05-09
Applicant: VALE SA , UNIV FED DO ESPÍRITO SANTO , STEGMILLER LEONIDIO , REIS JOSE ANTONINO ALVES E SILVA , DE JESUS REINALDO WALMIR , COSTA LILIANE DURANS DE MORAES , FERNANDES ANTONIO ALBERTO RIBEIRO , ALBUQUERQUE ERICA DUTRA , CORR A JEFERSON DA SILVA , CUNHA MAURICIO KUSTER , BASTOS MARLON CHRISTIAN MARIANELLI , FERNANDES PATRICIA MACHADO BUENO , ZORZAL POLIANA BELISÁRIO
Inventor： STEGMILLER LEONIDIO , REIS JOSE ANTONINO ALVES E SILVA , DE JESUS REINALDO WALMIR , COSTA LILIANE DURANS DE MORAES , FERNANDES ANTONIO ALBERTO RIBEIRO , ALBUQUERQUE ERICA DUTRA , CORR A JEFERSON DA SILVA , CUNHA MAURICIO KUSTER , BASTOS MARLON CHRISTIAN MARIANELLI , FERNANDES PATRICIA MACHADO BUENO , ZORZAL POLIANA BELISÁRIO
CPC classification number: C08B11/02 , A23L29/262 , A61K9/1652 , C08B1/06 , C08B11/12 , C08H8/00 , C08L1/286 , D21C5/00 , D21C9/002 , D21H11/12 , D21H11/16 , D21H11/20 , D21H17/20 , D21H17/26
Abstract: The present invention describes an advantageous and effective process for obtaining carboxymethyl cellulose (CMC) from agro-industrial residues, comprising the steps of a) Preparing the raw material, wherein the raw material is washed, dried, grounded and washed again; b) a pumping step, wherein the product obtained from the step a) is reacted with sodium hydroxide; c) a synthesis step, wherein consists in grounding the pulp; adding a solution of isopropanol and distilled water under stirring at room temperature; adding NaOH aqueous solution up to the alkalization of the mixture; adding monochloroacetic acid in isopropanol; filtrating; suspending in methanol solution and neutralizing with acetic acid. The present invention also relates to the CMC obtained from the said process which can be employed in a several industrial processes.
Abstract translation: 本发明描述了从农业工业残留物获得羧甲基纤维素（CMC）的有利和有效的方法，包括以下步骤：a）制备原料，其中将原料洗涤，干燥，接地并再次洗涤; b）泵送步骤，其中从步骤a）获得的产物与氢氧化钠反应; c）合成步骤，其中包括将纸浆接地; 在室温搅拌下加入异丙醇和蒸馏水的溶液; 加入NaOH水溶液直至混合物碱化; 在异丙醇中加入一氯乙酸; 过滤; 悬浮在甲醇溶液中并用乙酸中和。 本发明还涉及从所述方法获得的CMC，其可以用于几种工业方法。
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2.发明申请PROCESS FOR OBTAINING CARBOXYMETHYL CELLULOSE FROM AGRO-INDUSTRIAL RESIDUES AND CARBOXYMETHYL CELLULOSE AND USE THEREOF 审中-公开从农业工业残留物和羧甲基纤维素获得羧甲基纤维素的方法及其用途
公开(公告)号：WO2013166575A1
公开(公告)日：2013-11-14
申请号：PCT/BR2013/000159
申请日：2013-05-09
Applicant: VALE S.A. , UNIVERSIDADE FEDERAL DO ESPÍRITO SANTO , STEGMILLER, Leonidio , REIS, Jose Antonino Alves e Silva , DE JESUS, Reinaldo Walmir , COSTA, Liliane Durans de Moraes , FERNANDES, Antonio Alberto Ribeiro , ALBUQUERQUE, Erica Dutra , CORRÊA, Jeferson da Silva , CUNHA, Mauricio Kuster , BASTOS, Marlon Christian Marianelli , FERNANDES, Patricia Machado Bueno , ZORZAL, Poliana Belisário
Inventor： STEGMILLER, Leonidio , REIS, Jose Antonino Alves e Silva , DE JESUS, Reinaldo Walmir , COSTA, Liliane Durans de Moraes , FERNANDES, Antonio Alberto Ribeiro , ALBUQUERQUE, Erica Dutra , CORRÊA, Jeferson da Silva , CUNHA, Mauricio Kuster , BASTOS, Marlon Christian Marianelli , FERNANDES, Patricia Machado Bueno , ZORZAL, Poliana Belisário
CPC classification number: C08B11/02 , A23L29/262 , A61K9/1652 , C08B1/06 , C08B11/12 , C08H8/00 , C08L1/286 , D21C5/00 , D21C9/002 , D21H11/12 , D21H11/16 , D21H11/20 , D21H17/20 , D21H17/26
Abstract: The present invention describes an advantageous and effective process for obtaining carboxymethyl cellulose (CMC) from agro-industrial residues, comprising the steps of a) Preparing the raw material, wherein the raw material is washed, dried, grounded and washed again; b) a pumping step, wherein the product obtained from the step a) is reacted with sodium hydroxide; c) a synthesis step, wherein consists in grounding the pulp; adding a solution of isopropanol and distilled water under stirring at room temperature; adding NaOH aqueous solution up to the alkalization of the mixture; adding monochloroacetic acid in isopropanol; filtrating; suspending in methanol solution and neutralizing with acetic acid. The present invention also relates to the CMC obtained from the said process which can be employed in a several industrial processes.
Abstract translation: 本发明描述了从农业工业残留物获得羧甲基纤维素（CMC）的有利和有效的方法，包括以下步骤：a）制备原料，其中将原料洗涤，干燥，接地并再次洗涤; b）泵送步骤，其中从步骤a）获得的产物与氢氧化钠反应; c）合成步骤，其中包括将纸浆接地; 在室温搅拌下加入异丙醇和蒸馏水的溶液; 加入NaOH水溶液直至混合物碱化; 在异丙醇中加入一氯乙酸; 过滤; 悬浮在甲醇溶液中并用乙酸中和。 本发明还涉及从所述方法获得的CMC，其可以用于几种工业方法。
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公开(公告)号：WO2008022420A1
公开(公告)日：2008-02-28
申请号：PCT/BR2007/000213
申请日：2007-08-22
Applicant: COMPANHIA VALE DO RIO DOCE , REIS, Jose, Antonino, Alves e Silva , STEGMILLER, Leonidio , JUNIOR, Aldo, Gamberini , FERREIRA, Romeu, Venturott , JESUS, Romero, Santana, Azeredo de , ROCHA, Gelson, Luis , CESARIO, Claudio, Marcio, Oliveira , SANTOS, Ely, Valeriano doss , MAIA, Jose, , SANTOS, Antonio, Fernando, Pereira dos , FAUSTINO, Edvaldo, Marcelino , SILVA, Altair, Barbosa da , CARVALHO, Emerson, William de
Inventor： REIS, Jose, Antonino, Alves e Silva , STEGMILLER, Leonidio , JUNIOR, Aldo, Gamberini , FERREIRA, Romeu, Venturott , JESUS, Romero, Santana, Azeredo de , ROCHA, Gelson, Luis , CESARIO, Claudio, Marcio, Oliveira , SANTOS, Ely, Valeriano doss , MAIA, Jose, , SANTOS, Antonio, Fernando, Pereira dos , FAUSTINO, Edvaldo, Marcelino , SILVA, Altair, Barbosa da , CARVALHO, Emerson, William de
CPC classification number: C22B1/2406 , C22B1/2413 , C22B3/00 , C22B3/02 , Y02P10/234
Abstract: "An Ore Heap Leaching Process for metal production with the aid of solar energy ", Liquid or Pulp Aeration Device that projects liquid or pulp (P) through a spreading nozzle on a chain curtain (C) and captures air bubbles from the liquid or pulp (P) while the fluid outflows through the curtain links (C) by gravity forming films by virtue of an interaction of the surface strain and wettability between the three surfaces in question. As far as the outflow is concerned, these films end up interacting between themselves capturing the remaining air between them, thus forming profuse bubbles, resulting in the formation of liquid or foaming pulp (P) by virtue of the chain discharge (C).
Abstract translation: “借助太阳能进行金属生产的矿石浸出工艺”，液体或纸浆曝气装置，通过链帘（C）上的喷嘴投射液体或纸浆（P），并从液体或纸浆中捕获气泡 （P），同时由于所考虑的三个表面之间的表面应变和润湿性的相互作用，液体通过重力形成膜而流过帘式连杆（C）。 就流出而言，这些膜最终在它们之间相互作用，捕获它们之间的剩余空气，从而形成大量气泡，从而通过链条排放（C）形成液体或发泡纸浆（P）。
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