公开(公告)号：WO2012075076A2

公开(公告)日：2012-06-07

申请号：PCT/US2011/062529

申请日：2011-11-30

Applicant: NALCO COMPANY ,  BANKS, Rodney H. ,  CIOTA, Steven R. ,  WELZ, Sascha

Inventor： BANKS, Rodney H. ,  CIOTA, Steven R. ,  WELZ, Sascha

IPC: G01N21/75 ,  G01N21/31

CPC classification number: G01N21/643 ,  G01N21/05 ,  G01N21/6428 ,  G01N21/7703 ,  G01N21/80 ,  G01N21/82 ,  G01N31/22 ,  G01N31/221 ,  G01N33/1813 ,  G01N35/08 ,  G01N2021/6421 ,  G01N2021/6491 ,  Y10T436/11 ,  Y10T436/193333 ,  Y10T436/25125

Abstract: The invention provides a method and apparatus for determining the amount of various materials in a liquid sample. Because the apparatus is particularly resilient it can be used repeatedly with very harsh liquid samples such as boot water from an oil refinery. The apparatus uses at least one volume and/or concentration independent optical analysis method to determine at least one of: the pH, amount of chloride, and/or amount of iron in the sample. The optical property can be colorimetric, fluorescent or both and result from adding dyes, complexing agents, turbidity inducing compounds, and other optically effecting reagents to the sample. Because the measurements are concentration and volume independent they can be done continuously, quickly, and avoid the inconvenient start and stop procedures in prior art measurement regimens. The method further includes using a BDD cell to oxidize materials (such as sulfoxy compounds) that would otherwise interfere with the optical analysis and/or to sparge the sample with gas.

Abstract translation: 本发明提供一种用于确定液体样品中各种材料的量的方法和装置。 因为该装置特别弹性，所以可以用非常苛刻的液体样品反复使用，例如来自炼油厂的靴子水。 该装置使用至少一种体积和/或浓度的光学分析方法来确定样品中的pH，氯化物量和/或铁量中的至少一种。 光学特性可以是比色，荧光或两者，并且由添加染料，络合剂，浊度诱导化合物和其它光学效应试剂引起。 由于测量是集中和体积独立的，因此可以连续，快速地完成测量，并避免现有技术测量方案中的不便之处。 该方法还包括使用BDD电池来氧化否则会干扰光学分析和/或用气体喷射样品的材料（例如磺氧基化合物）。

公开(公告)号：WO2012149076A3

公开(公告)日：2013-03-14

申请号：PCT/US2012035075

申请日：2012-04-26

Applicant: NALCO CO ,  BANKS RODNEY H ,  CIOTA STEVEN R ,  WELZ SASCHA

Inventor： BANKS RODNEY H ,  CIOTA STEVEN R ,  WELZ SASCHA

IPC: G01N21/75 ,  G01N33/22

CPC classification number: G01N21/77 ,  G01N1/34 ,  G01N17/00 ,  G01N21/6428 ,  G01N21/643 ,  G01N21/78 ,  G01N21/80 ,  G01N21/82 ,  G01N21/83 ,  G01N31/22 ,  G01N33/2835 ,  G01N35/08 ,  G01N2021/6421 ,  G01N2021/6432 ,  G01N2021/6441 ,  G01N2021/6491 ,  G01N2021/7786 ,  Y10T436/19 ,  Y10T436/25125

Abstract: The invention provides a method and apparatus for determining the amount of various materials in a liquid sample. Because the apparatus is particularly resilient It can be used repeatedly with very harsh liquid samples such as boot water from an oil refinery. The apparatus uses at least one volume and/or concentration independent optical analysis method to determine at least one of: the pH, amount of chloride, and/or amount of iron in the sample. The optical property can be eolorimetrie, fluorescent, or both and result from adding dyes, complexlrsg agents, turbidity inducing compounds, and other optically effecting reagents to the sample. Because the measurements are concentration and volume independent they can be done continuously, quickly, and avoid the inconvenient start and stop procedures in prior art measurement regimens. The method further includes using a BDD cell to oxidize materials (such, as sulfoxy compounds) that would otherwise interfere with the optical analysis and/or to sparge the sample with gas.

Abstract translation: 本发明提供一种用于确定液体样品中各种材料的量的方法和装置。 因为设备特别有弹性它可以用非常苛刻的液体样品反复使用，例如来自炼油厂的靴子水。 该装置使用至少一种体积和/或浓度的光学分析方法来确定样品中的pH，氯化物量和/或铁量中的至少一种。 光学性质可以是变色，荧光或两者，并且由添加染料，复合物剂，浊度诱导化合物和其它光学效应试剂引起。 由于测量是集中和体积独立的，因此可以连续，快速地完成测量，并避免现有技术测量方案中的不便之处。 该方法还包括使用BDD电池来氧化否则会干扰光学分析和/或用气体喷射样品的材料（如磺氧基化合物）。

公开(公告)号：WO2009111455A1

公开(公告)日：2009-09-11

申请号：PCT/US2009/035848

申请日：2009-03-03

Applicant: NALCO COMPANY ,  HESSEFORT, Yin Z. ,  HOLLAND, Brian T. ,  ATKINS, Jeffrey M. ,  WELZ, Sascha ,  LI, Xiaojin

Inventor： HESSEFORT, Yin Z. ,  HOLLAND, Brian T. ,  ATKINS, Jeffrey M. ,  WELZ, Sascha ,  LI, Xiaojin

IPC: A61K8/81 ,  A61Q5/12

CPC classification number: A61K8/817 ,  A61K8/8147 ,  A61Q5/12

Abstract: A method of treating one or more hair shafts, each hair shaft including a cuticle layer and a cortex enclosed in the cuticle layer is disclosed. The method comprises: selecting one or more polymers that can penetrate the hair shafts with a pore size of about 5 angstroms to about 5000 angstroms; and treating the hair shafts by applying an effective amount of a composition containing said polymers to said hair shafts.

Abstract translation: 公开了一种处理一个或多个毛发轴的方法，每个毛发轴包括角质层和包围在角质层中的皮质。 该方法包括：选择一种或多种可以以大约5埃至大约5000埃的孔径穿透毛干的聚合物; 以及通过将有效量的含有所述聚合物的组合物施用到所述毛干来处理毛干。

公开(公告)号：WO2012149076A8

公开(公告)日：2012-11-01

申请号：PCT/US2012/035075

申请日：2012-04-26

Applicant: NALCO COMPANY ,  BANKS, Rodney H. ,  CIOTA, Steven R. ,  WELZ, Sascha

Inventor： BANKS, Rodney H. ,  CIOTA, Steven R. ,  WELZ, Sascha

IPC: G01N21/75 ,  G01N33/22

Abstract: The invention provides a method and apparatus for determining the amount of various materials in a liquid sample. Because the apparatus is particularly resilient It can be used repeatedly with very harsh liquid samples such as boot water from an oil refinery. The apparatus uses at least one volume and/or concentration independent optical analysis method to determine at least one of: the pH, amount of chloride, and/or amount of iron in the sample. The optical property can be colorimetric, fluorescent, or both and result from adding dyes, complexing agents, turbidity inducing compounds, and other optically effecting reagents to the sample. Because the measurements are concentration and volume independent they can be done continuously, quickly, and avoid the inconvenient start and stop procedures in prior art measurement regimens. The method further includes using a BDD cell to oxidize materials (such, as sulfoxy compounds) that would otherwise interfere with the optical analysis and/or to sparge the sample with gas.

公开(公告)号：WO2012149076A2

公开(公告)日：2012-11-01

申请号：PCT/US2012035075

申请日：2012-04-26

Applicant: NALCO CO ,  BANKS RODNEY H ,  CIOTA STEVEN R ,  WELZ SASCHA

Inventor： BANKS RODNEY H ,  CIOTA STEVEN R ,  WELZ SASCHA

IPC: G01N21/75 ,  G01N33/22

CPC classification number: G01N21/77 ,  G01N1/34 ,  G01N17/00 ,  G01N21/6428 ,  G01N21/643 ,  G01N21/78 ,  G01N21/80 ,  G01N21/82 ,  G01N21/83 ,  G01N31/22 ,  G01N33/2835 ,  G01N35/08 ,  G01N2021/6421 ,  G01N2021/6432 ,  G01N2021/6441 ,  G01N2021/6491 ,  G01N2021/7786 ,  Y10T436/19 ,  Y10T436/25125

Abstract: The invention provides a method and apparatus for determining the amount of various materials in a liquid sample. Because the apparatus is particularly resilient It can be used repeatedly with very harsh liquid samples such as boot water from an oil refinery. The apparatus uses at least one volume and/or concentration independent optical analysis method to determine at least one of: the pH, amount of chloride, and/or amount of iron in the sample. The optical property can be eolorimetrie, fluorescent, or both and result from adding dyes, complexlrsg agents, turbidity inducing compounds, and other optically effecting reagents to the sample. Because the measurements are concentration and volume independent they can be done continuously, quickly, and avoid the inconvenient start and stop procedures in prior art measurement regimens. The method further includes using a BDD cell to oxidize materials (such, as sulfoxy compounds) that would otherwise interfere with the optical analysis and/or to sparge the sample with gas.

Abstract translation: 本发明提供一种用于确定液体样品中各种材料的量的方法和装置。 因为设备特别有弹性它可以用非常苛刻的液体样品反复使用，例如来自炼油厂的靴子水。 该装置使用至少一种体积和/或浓度的光学分析方法来确定样品中的pH，氯化物量和/或铁量中的至少一种。 光学性质可以是变色，荧光或两者，并且由添加染料，复合物剂，浊度诱导化合物和其它光学效应试剂引起。 由于测量是集中和体积独立的，因此可以连续，快速地完成测量，并避免现有技术测量方案中的不便之处。 该方法还包括使用BDD电池来氧化否则会干扰光学分析和/或用气体喷射样品的材料（如磺氧基化合物）。

公开(公告)号：WO2010078288A2

公开(公告)日：2010-07-08

申请号：PCT/US2009/069636

申请日：2009-12-29

Applicant: NALCO COMPANY ,  HESSEFORT, Yin Z. ,  HOLLAND, Brian T. ,  ATKINS, Jeffery M. ,  WELZ, Sascha ,  LI, Xiaojin Harry ,  KOMPALITCH, Viginie

Inventor： HESSEFORT, Yin Z. ,  HOLLAND, Brian T. ,  ATKINS, Jeffery M. ,  WELZ, Sascha ,  LI, Xiaojin Harry ,  KOMPALITCH, Viginie

IPC: A61Q5/04 ,  A61Q5/12 ,  A61K8/81

CPC classification number: A61K8/8147 ,  A61K8/8158 ,  A61K2800/5424 ,  A61Q5/04 ,  A61Q5/12

Abstract: A method of treating one or more hair shafts, each hair shaft including a cuticle layer and a cortex enclosed in the cuticle layer is disclosed. The method comprises: selecting one or more polymers that can penetrate the hair shafts with a pore size of about 5 angstroms to about 5000 angstroms; and treating the hair shafts by applying an effective amount of a composition containing said polymers to said hair shafts.

Abstract translation: 公开了一种处理一个或多个毛发轴的方法，每个毛发轴包括角质层和包围在角质层中的皮质。 该方法包括：选择一种或多种可以以大约5埃至大约5000埃的孔径穿透毛干的聚合物; 以及通过将有效量的含有所述聚合物的组合物施用到所述毛干来处理毛干。

公开(公告)号：WO2012075076A3

公开(公告)日：2012-10-04

申请号：PCT/US2011062529

申请日：2011-11-30

Applicant: NALCO CO ,  BANKS RODNEY H ,  CIOTA STEVEN R ,  WELZ SASCHA

Inventor： BANKS RODNEY H ,  CIOTA STEVEN R ,  WELZ SASCHA

IPC: G01N21/75 ,  G01N21/31

CPC classification number: G01N21/643 ,  G01N21/05 ,  G01N21/6428 ,  G01N21/7703 ,  G01N21/80 ,  G01N21/82 ,  G01N31/22 ,  G01N31/221 ,  G01N33/1813 ,  G01N35/08 ,  G01N2021/6421 ,  G01N2021/6491 ,  Y10T436/11 ,  Y10T436/193333 ,  Y10T436/25125

Abstract: The invention provides a method and apparatus for determining the amount of various materials in a liquid sample. Because the apparatus is particularly resilient it can be used repeatedly with very harsh liquid samples such as boot water from an oil refinery. The apparatus uses at least one volume and/or concentration independent optical analysis method to determine at least one of: the pH, amount of chloride, and/or amount of iron in the sample. The optical property can be colorimetric, fluorescent or both and result from adding dyes, complexing agents, turbidity inducing compounds, and other optically effecting reagents to the sample. Because the measurements are concentration and volume independent they can be done continuously, quickly, and avoid the inconvenient start and stop procedures in prior art measurement regimens. The method further includes using a BDD cell to oxidize materials (such as sulfoxy compounds) that would otherwise interfere with the optical analysis and/or to sparge the sample with gas.

Abstract translation: 本发明提供了用于确定液体样品中各种材料的量的方法和设备。 由于该设备特别具有弹性，因此可以对非常苛刻的液体样品（如炼油厂的启动水）重复使用。 该设备使用至少一种体积和/或浓度无关的光学分析方法来确定样品中的pH，氯化物的量和/或铁的量中的至少一个。 光学性质可以是比色法，荧光法或两者兼而有之，并且由于向样品中加入染料，络合剂，浊度诱导化合物和其他光学影响试剂而产生。 由于测量值是浓度和体积独立的，因此可以连续快速地完成测量，并避免现有技术测量方案中不便的启动和停止程序。 该方法进一步包括使用BDD细胞来氧化原本会干扰光学分析和/或用气体喷射样品的材料（例如亚砜氧化物）。

公开(公告)号：WO2010078288A3

公开(公告)日：2010-08-26

申请号：PCT/US2009069636

申请日：2009-12-29

Applicant: NALCO CO ,  HESSEFORT YIN Z ,  HOLLAND BRIAN T ,  ATKINS JEFFERY M ,  WELZ SASCHA ,  LI XIAOJIN HARRY ,  KOMPALITCH VIGINIE

Inventor： HESSEFORT YIN Z ,  HOLLAND BRIAN T ,  ATKINS JEFFERY M ,  WELZ SASCHA ,  LI XIAOJIN HARRY ,  KOMPALITCH VIGINIE

IPC: A61K8/81 ,  A61Q5/04 ,  A61Q5/12

CPC classification number: A61K8/8147 ,  A61K8/8158 ,  A61K2800/5424 ,  A61Q5/04 ,  A61Q5/12

Abstract: A method of treating one or more hair shafts, each hair shaft including a cuticle layer and a cortex enclosed in the cuticle layer is disclosed. The method comprises: selecting one or more polymers that can penetrate the hair shafts with a pore size of about 5 angstroms to about 5000 angstroms; and treating the hair shafts by applying an effective amount of a composition containing said polymers to said hair shafts.

Abstract translation: 公开了一种处理一个或多个毛干的方法，每个毛干包括表皮层和包围在表皮层中的皮质。 该方法包括：选择一种或多种能够穿透孔径为约5埃至约5000埃的毛干的聚合物; 以及通过将有效量的含有所述聚合物的组合物施加到所述毛干来处理所述毛干。

公开(公告)号：WO2010078311A1

公开(公告)日：2010-07-08

申请号：PCT/US2009/069670

申请日：2009-12-29

Applicant: NALCO COMPANY ,  HESSEFORT, Yin Z. ,  HOLLAND, Brian T. ,  ATKINS, Jeffery M. ,  WELZ, Sascha ,  LI, Xiaojin Harry

Inventor： HESSEFORT, Yin Z. ,  HOLLAND, Brian T. ,  ATKINS, Jeffery M. ,  WELZ, Sascha ,  LI, Xiaojin Harry

IPC: A61K8/81 ,  A61Q5/12

CPC classification number: A61K8/8147 ,  A61K8/817 ,  A61Q5/12

Abstract: A method of treating one or more hair shafts, each hair shaft including a cuticle layer and a cortex enclosed in the cuticle layer is disclosed. The method comprises: selecting one or more polymers that can penetrate the hair shafts with a pore size of about 5 angstroms to about 5000 angstroms; and treating the hair shafts by applying an effective amount of a composition containing said polymers to said hair shafts

Abstract translation: 公开了一种处理一个或多个毛发轴的方法，每个毛发轴包括角质层和包围在角质层中的皮质。 该方法包括：选择一种或多种可以以大约5埃至大约5000埃的孔径穿透毛干的聚合物; 以及通过将有效量的含有所述聚合物的组合物施用到所述毛干来处理毛干

公开(公告)号：WO2010030878A3

公开(公告)日：2010-05-06

申请号：PCT/US2009056659

申请日：2009-09-11

Applicant: NALCO CO ,  HOLLAND BRIAN T ,  WELZ SASCHA

Inventor： HOLLAND BRIAN T ,  WELZ SASCHA

IPC: C01B33/00 ,  C01B33/12

CPC classification number: C01B33/126 ,  C01B33/193 ,  C01P2006/12 ,  C01P2006/14 ,  C01P2006/16 ,  Y10T428/2982 ,  Y10T428/2991

Abstract: Non-spherical siliceous particles having a plurality of porous branches are disclosed and claimed. The porous branches are randomly oriented and elongated, ring-like, and/or aggregated. An additive introduced during synthesis of the particles modifies pore volume and morphology. The tunability of the pore volume includes an inner diameter ranging from about 2 to about 50,000. Synthesizing the particles includes mixing under constant or intermittent stirring in a reaction vessel an aqueous silicic acid solution with an acidic heel solution to form a mixture. The stirring may optionally be performed at a variable speed. An additive is introduced into the mixture at a controlled rate, wherein the additive imposes a pH change from a lower pH to a higher pH to the mixture to induce siliceous particle precipitation. Optionally, a metal dopand may be introduced into the particles and/or at least a portion of an outer surface located outside of the pores and/or an inner surface located inside of the pores may be modified.

Abstract translation: 公开并要求保护的具有多个多孔分支的非球形硅质颗粒。 多孔分支是随机定向的并且伸长，环状和/或聚集。 在颗粒合成期间引入的添加剂改变了孔体积和形态。 孔体积的可调性包括约2至约50,000的内径。 合成颗粒包括在恒定或间歇搅拌下在反应容器中混合硅酸水溶液与酸性踵溶液以形成混合物。 搅拌可以可选地以可变的速度进行。 将添加剂以受控速率引入混合物中，其中添加剂施加从较低pH至较高pH的pH变化至混合物以诱导硅质粒子沉淀。 任选地，可以将金属掺杂物引入到颗粒中和/或位于孔外部的外表面的至少一部分和/或位于孔内部的内表面可以被改性。