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    PROCESS FOR PREPARING FLUORINATED, INORGANIC HOLLOW NANOSPHERES USING WATER-BASED SILICA PRECURSORS
    1.
    发明申请
    PROCESS FOR PREPARING FLUORINATED, INORGANIC HOLLOW NANOSPHERES USING WATER-BASED SILICA PRECURSORS 审中-公开
    使用水基二氧化硅前体制备无色无色中空纳米微球的方法

    公开(公告)号：WO2015138156A1

    公开(公告)日：2015-09-17

    申请号：PCT/US2015/017903

    申请日：2015-02-27

    Applicant: E I DU PONT DE NEMOURS AND COMPANY

    Inventor： LEE, Hau-Nan ,  LASIO, Jelena ,  RAGHAVANPILLAI, Anilkumar ,  BERNARD, Stephanie A

    IPC: C09C1/30

    CPC classification number: C09C1/3081 ,  A61K8/0279 ,  A61K8/25 ,  A61K9/501 ,  A61K9/5089 ,  A61K2800/10 ,  A61Q19/00 ,  B01J13/16 ,  C01P2004/04 ,  C01P2004/34 ,  C01P2004/62 ,  C01P2004/64

    Abstract: The disclosure provides a process for preparing a fluorinated silica hollow nanosphere comprising: providing a mixture comprising water, at least one non-reactive solvent, at least one fluorosilane, at least one water based silica precursor solution, such as sodium silicate, potassium silicate, ammonium silicate or pre-formed silicic acid, and at least one surfactant; shearing the components of the mixture with high shear energy at an energy density of at least 10^6 J/m^3 to form a mini-emulsion; initiating a one-step sol-gel reaction by adjusting the pH to about 4 to 10 and then initiating a one-step sol-gel forming fluorinated hollow silica nanospheres having a particle size of less than about 400nm.

    Abstract translation: 本公开提供了一种制备氟化二氧化硅中空纳米球的方法，其包括：提供包含水，至少一种非反应性溶剂，至少一种氟硅烷，至少一种水基二氧化硅前体溶液如硅酸钠，硅酸钾， 硅酸铵或预形成的硅酸，和至少一种表面活性剂; 以至少10 6 J / m 3的能量密度以高剪切能剪切混合物的组分以形成微乳液; 通过将pH调节至约4至10，然后引发一步溶胶 - 凝胶形成具有小于约400nm的粒度的氟化中空二氧化硅纳米球，开始一步溶胶 - 凝胶反应。

    PROCESS FOR PREPARING FUNCTIONALIZED HOLLOW SILICA PARTICLES WITH LOW POROSITY
    2.
    发明申请
    PROCESS FOR PREPARING FUNCTIONALIZED HOLLOW SILICA PARTICLES WITH LOW POROSITY 审中-公开
    制备具有低孔隙度的功能性中性硅石颗粒的方法

    公开(公告)号：WO2015138141A1

    公开(公告)日：2015-09-17

    申请号：PCT/US2015/017799

    申请日：2015-02-26

    Applicant: E I DU PONT DE NEMOURS AND COMPANY

    Inventor： LASIO, Jelena ,  RAGHAVANPILLAI, Anilkumar ,  WOERNER, Francis J.

    IPC: C09C1/30 ,  C01B33/12 ,  C01B33/149 ,  C08F2/10 ,  C08F8/50

    CPC classification number: C09C1/3081 ,  C01B33/18 ,  C01P2004/62 ,  C01P2006/12 ,  C01P2006/14 ,  C08F2/22 ,  C09C1/3054 ,  C09C1/3063

    Abstract: The disclosure provides a process for preparing the functionalized hollow silica particles comprising: providing a core-shell silica particle comprising a template core particle and a silica treatment, wherein the core-shell silica particle has an outer surface; and wherein the silica treatment is prepared using a solvent-based silica precursor; creating a functionalized surface on the core-shell silica particle, wherein the functionalized surface is prepared using sulfonic acid, phosphonic esters, carboxylic acid, amines, epoxides, or boronic acids, and removing the template core particle to form a functionalized hollow silica particle. These inorganic hollow particles are useful as hiding or opacifying agents in coating and molding compositions. They are also useful as photonic band gap or thermal insulation materials.

    Abstract translation: 本发明提供一种制备功能化中空二氧化硅颗粒的方法，包括：提供包含模板芯颗粒和二氧化硅处理的核 - 壳二氧化硅颗粒，其中所述核 - 壳二氧化硅颗粒具有外表面; 并且其中所述二氧化硅处理是使用溶剂基二氧化硅前体制备的; 在核 - 壳二氧化硅颗粒上形成功能化表面，其中功能化表面使用磺酸，膦酸酯，羧酸，胺，环氧化物或硼酸制备，并除去模板核心颗粒以形成官能化的中空二氧化硅颗粒。 这些无机中空颗粒可用作涂料和模塑组合物中的遮盖剂或不透明剂。 它们也可用作光子带隙或保温材料。

    COATING COMPOSITIONS COMPRISING FUNCTIONALIZED HOLLOW SILICA PARTICLES WITH LOW POROSITY PREPARED USING WATER-BASED SILICA PRECURSORS
    3.
    发明申请
    COATING COMPOSITIONS COMPRISING FUNCTIONALIZED HOLLOW SILICA PARTICLES WITH LOW POROSITY PREPARED USING WATER-BASED SILICA PRECURSORS 审中-公开
    包含使用水基二氧化硅前体制备的具有低孔隙率的功能性中性硅石颗粒的涂料组合物

    公开(公告)号：WO2015138162A1

    公开(公告)日：2015-09-17

    申请号：PCT/US2015/017912

    申请日：2015-02-27

    Applicant: E I DU PONT DE NEMOURS AND COMPANY

    Inventor： LASIO, Jelena

    IPC: C08K3/36 ,  C09D175/04 ,  C08K7/26 ,  C08K9/06

    CPC classification number: C09C1/309 ,  C01P2004/34 ,  C08K3/36 ,  C08K7/26 ,  C08K9/06 ,  C09C1/3063 ,  C09C1/3072 ,  C09C1/3081 ,  C09D175/04 ,  C08L25/04

    Abstract: The disclosure provides a coating composition comprising functionalized hollow silica particles, wherein the functionalized hollow silica particles are prepared by a process comprising: providing a core/shell silica particle comprising a template core particle and a silica treatment, wherein the core/shell silica particle has an outer surface; and wherein the silica treatment is prepared using a water-based silica precursor; creating a functionalized surface on the core/shell silica particle, wherein the functionalized surface is prepared using sulfonic acid, phosphonic esters, carboxylic acid, amines, epoxides, or boronic acids, and removing the template core particle to form a functionalized hollow silica particle. These coating compositions comprise inorganic hollow particles which are useful as hiding or opacifying agents.

    Abstract translation: 本发明提供了包含官能化中空二氧化硅颗粒的涂料组合物，其中所述官能化中空二氧化硅颗粒通过包括以下方法制备的方法包括：提供包含模板核心颗粒和二氧化硅处理的核/壳二氧化硅颗粒，其中所述核/壳二氧化硅颗粒具有 外表面 并且其中所述二氧化硅处理是使用水基二氧化硅前体制备的; 在核/壳二氧化硅颗粒上形成功能化表面，其中功能化表面使用磺酸，膦酸酯，羧酸，胺，环氧化物或硼酸制备，并除去模板核心颗粒以形成官能化的中空二氧化硅颗粒。 这些涂料组合物包含可用作遮盖剂或不透明剂的无机中空颗粒。

    PROCESS FOR PREPARING SURFACE FUNCTIONALIZED POLYMERIC AND POLYMERIC/SILICA HYBRID HOLLOW NANOSPHERES
    5.
    发明申请
    PROCESS FOR PREPARING SURFACE FUNCTIONALIZED POLYMERIC AND POLYMERIC/SILICA HYBRID HOLLOW NANOSPHERES 审中-公开
    表面官能化聚合物和聚合物/二氧化硅混合中空纳米微粒的制备方法

    公开(公告)号：WO2015138164A1

    公开(公告)日：2015-09-17

    申请号：PCT/US2015/017916

    申请日：2015-02-27

    Applicant: E I DU PONT DE NEMOURS AND COMPANY

    Inventor： LEE, Hau-Nan ,  BERNARD, Stephanie A. ,  LASIO, Jelena ,  DUNCAN, Andrew Jay

    IPC: C08F2/22 ,  C08F2/44 ,  B82Y30/00

    CPC classification number: C08F2/22 ,  A61K8/0279 ,  A61K8/25 ,  A61K8/8117 ,  A61K8/8152 ,  A61K2800/10 ,  A61K2800/413 ,  A61K2800/614 ,  A61Q19/00 ,  B01J13/14 ,  B82Y40/00 ,  C08F2/44

    Abstract: The disclosure provides a process for preparing a surface functionalized polymeric or polymeric/silica hybrid hollow nanospheres comprising: providing a mixture comprising water, at least one non-reactive solvent, at least one acrylic or styrenic monomer; at least one functionalized acrylic or styrenic monomer; an initiator; at least one surfactant; and, optionally, a polymerizable silane if the polymeric/silica hybrid hollow particles are desired; and shearing the components of the mixture with high shear energy at an energy density of at least 10^6 J/m^3 to form a mini-emulsion; and heating to at least about 50°C, more typically about 50°C to about 90°C; and still more typically about 60°C to about 80°C to form, in one step, a surface functionalized polymeric or polymeric/silica hybrid hollow nanosphere.

    Abstract translation: 本公开提供了制备表面官能化聚合物或聚合物/二氧化硅混合中空纳米球的方法，其包括：提供包含水，至少一种非反应性溶剂，至少一种丙烯酸或苯乙烯单体的混合物; 至少一种官能化丙烯酸或苯乙烯单体; 发起者 至少一种表面活性剂; 如果需要聚合物/二氧化硅混合中空颗粒，可选地包含可聚合硅烷; 并以至少10 6 J / m 3的能量密度以高剪切能剪切混合物的组分以形成微乳液; 并加热至至少约50℃，更典型地约50℃至约90℃; 并且还更典型地约60℃至约80℃，以在一个步骤中形成表面官能化的聚合物或聚合物/二氧化硅混合中空纳米球。

    PROCESS FOR PREPARING FUNCTIONALIZED HOLLOW SILICA PARTICLES HAVING LOW POROSITY USING WATER-BASED SILICA PRECURSORS
    8.
    发明申请
    PROCESS FOR PREPARING FUNCTIONALIZED HOLLOW SILICA PARTICLES HAVING LOW POROSITY USING WATER-BASED SILICA PRECURSORS 审中-公开
    使用水基二氧化硅前驱体制备具有低孔隙率的功能性中空二氧化硅颗粒的方法

    公开(公告)号：WO2015138159A1

    公开(公告)日：2015-09-17

    申请号：PCT/US2015/017907

    申请日：2015-02-27

    Applicant: E I DU PONT DE NEMOURS AND COMPANY

    Inventor： LASIO, Jelena ,  LEE, Hau-Nan ,  RAGHAVANPILLAI, Anilkumar ,  CATIVO, Ma Helen

    IPC: C09C1/30 ,  C01B33/12 ,  C01B33/149 ,  C08F2/10 ,  C08F8/50

    CPC classification number: C09C1/3054 ,  C01B33/12 ,  C01B33/149 ,  C01B33/18 ,  C01P2004/34 ,  C01P2004/62 ,  C01P2004/64 ,  C08F2/22 ,  C08F220/14 ,  C08F265/04 ,  C09C1/3063 ,  C09C1/3081 ,  C08F230/08 ,  C08F220/34 ,  C08F2230/085 ,  C08F2222/1013

    Abstract: The disclosure provides a process for preparing the functionalized hollow silica particles comprises: providing a core-shell silica particle comprising a template core particle and a silica treatment, wherein the core-shell silica particle has an outer surface; and wherein the silica treatment is prepared using a water-based silica precursor; creating a functionalized surface on the core-shell silica particle, wherein the functionalized surface is prepared using sulfonic acid, phosphonic esters, carboxylic acid, amines, epoxides, or boronic acids, and removing the template core particle to form a functionalized hollow silica particle. These inorganic hollow particles are useful as hiding or opacifying agents in coating and molding compositions. They are also useful as photonic band gap or thermal insulation materials.

    Abstract translation: 本发明提供了制备官能化中空二氧化硅颗粒的方法，包括：提供包含模板核心颗粒和二氧化硅处理的核 - 壳二氧化硅颗粒，其中核 - 壳二氧化硅颗粒具有外表面; 并且其中所述二氧化硅处理是使用水基二氧化硅前体制备的; 在核 - 壳二氧化硅颗粒上形成功能化表面，其中功能化表面使用磺酸，膦酸酯，羧酸，胺，环氧化物或硼酸制备，并除去模板核心颗粒以形成官能化的中空二氧化硅颗粒。 这些无机中空颗粒可用作涂料和模塑组合物中的隐藏剂或不透明剂。 它们也可用作光子带隙或保温材料。

    COATING COMPOSITIONS COMPRISING FUNCTIONALIZED HOLLOW SILICA PARTICLES WITH LOW POROSITY
    10.
    发明申请
    COATING COMPOSITIONS COMPRISING FUNCTIONALIZED HOLLOW SILICA PARTICLES WITH LOW POROSITY 审中-公开
    具有低功能性功能的中空二氧化硅颗粒的涂料组合物

    公开(公告)号：WO2015138144A1

    公开(公告)日：2015-09-17

    申请号：PCT/US2015/017815

    申请日：2015-02-26

    Applicant: E I DU PONT DE NEMOURS AND COMPANY

    Inventor： LASIO, Jelena

    IPC: C08K3/36 ,  C09D175/04 ,  C08K7/26 ,  C08K9/06

    CPC classification number: C08K3/36 ,  C08G18/36 ,  C08G18/7621 ,  C08K7/26 ,  C08K9/06 ,  C09D175/04 ,  C08L25/04 ,  C08K9/04

    Abstract: The disclosure provides a coating composition comprising functionalized hollow silica particles, wherein the functionalized hollow silica particles are prepared by a process comprising: providing a core-shell silica particle comprising a template core particle and a silica treatment, wherein the core-shell silica particle has an outer surface; and wherein the silica treatment is prepared using a solvent-based silica precursor; creating a functionalized surface on the core-shell silica particle, wherein the functionalized surface is prepared using sulfonic acid, phosphonic esters, carboxylic acid, amines, epoxides, or boronic acids, and removing the template core particle to form a functionalized hollow silica particle. These coating compositions comprise inorganic hollow particles which are useful as hiding or opacifying agents.

    Abstract translation: 本发明提供了包含官能化中空二氧化硅颗粒的涂料组合物，其中所述官能化中空二氧化硅颗粒通过包括以下方法制备的方法包括：提供包含模板核心颗粒和二氧化硅处理的核 - 壳二氧化硅颗粒，其中所述核 - 壳二氧化硅颗粒具有 外表面 并且其中所述二氧化硅处理是使用溶剂基二氧化硅前体制备的; 在核 - 壳二氧化硅颗粒上形成功能化表面，其中功能化表面使用磺酸，膦酸酯，羧酸，胺，环氧化物或硼酸制备，并除去模板核心颗粒以形成官能化的中空二氧化硅颗粒。 这些涂料组合物包含可用作遮盖剂或不透明剂的无机中空颗粒。

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