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    PROCESS FOR THE PREPARATION OR REACTIVATION OF CARBON MONOXIDE HYDROGENATION CATALYST
    6.
    发明申请
    PROCESS FOR THE PREPARATION OR REACTIVATION OF CARBON MONOXIDE HYDROGENATION CATALYST 审中-公开
    一氧化碳氢化催化剂的制备或反应方法

    公开(公告)号：WO01026811A1

    公开(公告)日：2001-04-19

    申请号：PCT/US2000/027716

    申请日：2000-10-06

    IPC: B01J38/00 ,  B01J23/75 ,  B01J23/94 ,  B01J29/90 ,  B01J37/06 ,  B01J38/10 ,  B01J38/50 ,  B01J38/66 ,  C07C1/04 ,  C10G2/00

    CPC classification number: C10G2/332 ,  B01J29/90 ,  B01J37/06 ,  B01J38/50 ,  B01J38/66 ,  C07C1/0445 ,  C07C1/045 ,  C07C2529/08 ,  C07C2529/18 ,  C07C2529/70 ,  C07C2529/83 ,  C07C2529/85 ,  Y02P20/584

    Abstract: A process for the preparation of a catalyst useful for conducting carbon monoxide hydrogenation reactions, especially Fischer-Tropsch reactions. The steps of the process begin with the activation, or reactivation, of a deactivated catalyst, or with the preparation and activation of a fresh catalyst. In accordance with the latter, the steps of the process comprise, first contacting, in one or more steps, a powder or preformed, particulate refractory inorganic support with a liquid, or solution in which there is dispersed or dissolved a compound, or salt of a catalytically active metal, or metals, to impregnate and deposit the metal, or metals, upon the support, or powder. The metal, or metals, impregnated support is calcined following each impregnation step to form oxides of the deposited metal, or metals. The calcined catalyst precursor is then treated with a solution of a chelating compound, preferably a poly-or multidentate chelating compound, sufficient to complex with, extract and remove a portion of the oxides of the metal, or metals. The catalyst is activated by reduction; suitably by contact with hydrogen. In the activation, or reactivation of a deactivated catalyst, the catalyst is first treated with the chelating compound to extract a portion of the oxides of the metal, or metals, and the catalyst is then reduced. In either event, the activated or reactivated catalyst has high activity, or high C5+ selectivity, or both high activity and C5+ selectivity in conducting carbon monoxide hydrogenation reactions. The productivity of the process is increased.

    Abstract translation: 一种制备可用于进行一氧化碳氢化反应，特别是费 - 托反应的催化剂的方法。 该方法的步骤开始于失活催化剂的活化或再活化，或与新鲜催化剂的制备和活化。 根据后者，该方法的步骤包括：首先在一个或多个步骤中将粉末或预成型的颗粒状耐火无机载体与液体或溶液分散或溶解的化合物或其盐 催化活性金属或金属，以将金属或金属浸渍并沉积在载体或粉末上。 在每个浸渍步骤之后煅烧金属或金属浸渍的载体以形成沉积的金属或金属的氧化物。 然后将煅烧的催化剂前体用螯合化合物，优选多齿螯合化合物的溶液处理，该溶液足以与金属或金属的一部分氧化物复合，提取和除去。 催化剂通过还原活化; 适当地通过与氢接触。 在失活的催化剂的活化或再活化中，催化剂首先用螯合化合物处理以提取一部分金属或金属的氧化物，然后还原催化剂。 在任一情况下，活化或再活化的催化剂在进行一氧化碳氢化反应时具有高活性或高C5 +选择性，或高活性和C5 +选择性。 该过程的生产率增加。

    DETERGENT ALKYLATION CATALYST REGENERATION EFFLUENT RECYCLE
    7.
    发明申请
    DETERGENT ALKYLATION CATALYST REGENERATION EFFLUENT RECYCLE 审中-公开
    洗涤剂烷基化催化剂再生剂回收利用

    公开(公告)号：WO2017200751A1

    公开(公告)日：2017-11-23

    申请号：PCT/US2017/030963

    申请日：2017-05-04

    Applicant: UOP LLC

    Inventor： SOHN, Stephen W. ,  LUEBKE, Charles P. ,  PIEPER, Jeffrey L.

    IPC: B01J38/50 ,  C07C2/66 ,  C07C15/107

    Abstract: A process for the regeneration of a catalyst is presented. The catalyst is in a reactor for use in benzene alkylation, and periodically needs to be regenerated. The reactor is taken off-line, and a regenerant is passed through the reactor, producing an effluent stream. A portion of the effluent stream is recycled through the reactor without passing through a clean-up process.

    Abstract translation: 给出了催化剂再生的方法。 催化剂在用于苯烷基化的反应器中，并且需要定期进行再生。 将反应器离线，再生剂通过反应器，产生流出物流。 一部分流出物流通过反应器再循环而不经过清理过程。

    METHODS, SYSTEMS AND APPARATUSES FOR FISCHER-TROPSCH CATALYST REGENERATION
    8.
    发明申请
    METHODS, SYSTEMS AND APPARATUSES FOR FISCHER-TROPSCH CATALYST REGENERATION 审中-公开
    FISCHER-TROPSCH催化剂再生的方法，系统和装置

    公开(公告)号：WO2014144855A3

    公开(公告)日：2014-12-24

    申请号：PCT/US2014029442

    申请日：2014-03-14

    Applicant: INGA JUAN R ,  GI GASIFICATION INTERNATIONAL LUXEMBOURG S A

    Inventor： INGA JUAN R

    IPC: B01J38/50 ,  B01J38/56 ,  C07C27/26 ,  C10G2/00

    CPC classification number: B01J38/50 ,  B01J23/74 ,  B01J23/94 ,  B01J38/10 ,  B01J38/12 ,  B01J38/48 ,  B01J38/56 ,  C10G2/332 ,  C10G2/34 ,  C10G2300/70

    Abstract: Systems, methods and apparatuses for regenerating a Fischer-Tropsch ("FT") catalyst that is to be regenerated with a first wash fluid comprising at least one hydrocarbon and contacting the washed FT catalyst with a gas comprising hydrogen, method of regenerating a Fischer-Tropsch ("'FT") catalyst that is at least partially spent through having been utilized to produce FT hydrocarbons via FT synthesis in an FT reactor. The method includes the steps of washing the FT catalyst to be regenerated with a first wash fluid. The FT catalyst to be regenerated comprises pores, and at least a fraction of the pores contain a first mixture of hydrocarbons, The first wash fluid comprises at least one hydrocarbon, and the average molecular weight of the at least one hydrocarbon of the first wash fluid is less than the average molecular weight of the hydrocarbons in the first mixture of hydrocarbons.

    Abstract translation: 用于再生含有至少一种烃的第一洗涤流体并使经洗涤的FT催化剂与包含氢的气体接触的Fischer-Trop（“FT”）催化剂再生的系统，方法和装置， Tropsch（“'FT”）催化剂，其通过在FT反应器中通过FT合成被用于生产FT烃的至少部分消耗。 该方法包括用第一洗涤流体洗涤待再生的FT催化剂的步骤。 待再生的FT催化剂包含孔，并且孔的至少一部分含有烃的第一混合物。第一洗涤流体包含至少一种烃，并且第一洗涤流体的至少一种烃的平均分子量 小于烃的第一混合物中烃的平均分子量。

    METHOD FOR REGENERATING TITANOSILICATE CATALYSTS
    9.
    发明申请
    METHOD FOR REGENERATING TITANOSILICATE CATALYSTS 审中-公开
    重新制备钛酸酯催化剂的方法

    公开(公告)号：WO2011115234A1

    公开(公告)日：2011-09-22

    申请号：PCT/JP2011/056491

    申请日：2011-03-11

    Applicant: SUMITOMO CHEMICAL COMPANY, LIMITED ,  KAWABATA, Tomonori ,  YOSHIOKA, Masato

    Inventor： KAWABATA, Tomonori ,  YOSHIOKA, Masato

    IPC: B01J29/90 ,  B01J29/89 ,  B01J38/50 ,  C07D303/04

    CPC classification number: B01J29/90 ,  B01J29/89 ,  B01J38/50

    Abstract: A method for regenerating a titanosilicate catalyst, comprising a step of mixing a titanosilicate having reduced catalytic ability with a cyclic secondary amine, and a method for producing an oxirane compound, which comprises a step of reacting hydrogen peroxide with a C2-C12 compound having a carbon-carbon double bond, in the presence of a titanosilicate catalyst obtained by the regeneration method.

    Abstract translation: 一种再生钛硅酸盐催化剂的方法，包括将具有降低的催化能力的钛硅酸盐与环状仲胺混合的步骤和环氧乙烷化合物的制备方法，该方法包括使过氧化氢与具有 在通过再生方法获得的钛硅酸盐催化剂的存在下，碳 - 碳双键。

    A REACTIVE DISTILLATION ALKYLATION PROCESS INCLUDING IN SITU CATALYST REGENERATION
    10.
    发明申请
    A REACTIVE DISTILLATION ALKYLATION PROCESS INCLUDING IN SITU CATALYST REGENERATION 审中-公开
    包括催化剂再生的反应性蒸馏碱化方法

    公开(公告)号：WO2003076074A1

    公开(公告)日：2003-09-18

    申请号：PCT/US2003/001432

    申请日：2003-01-16

    Applicant: SASOL NORTH AMERICA INC.

    Inventor： WINDER, Barry, J. ,  WHARRY, Donald, L. ,  SCHELL, John, R. ,  BROWN, Mary, J. ,  MURRAY, Joy, L. ,  HOWE, Richard, C. ,  SORENSON, Wayne, L. ,  SZURA, Daniel, P. ,  GATES, Frank

    IPC: B01J38/50

    CPC classification number: B01J29/90 ,  B01D3/009 ,  C07C2/66 ,  Y02P20/127 ,  Y02P20/584

    Abstract: A unified process which couples a unique in-situ catalyst regeneration process with a continuous reactive distillation under pressure for the alkylation of light aromatic hydrocarbons such as benzene with C 2 -C 30 olefins using a solid acid alkylation catalyst supported in the reflux zone (21) of a distillation column (section A). Periodic regeneration of the catalyst (sections E, F and G) is carried out with a countercurrent injection of a C 4 -C 16 paraffin (35) below the benzene rectification zone at the top of the column, but above the catalyst zone while the aromatic hydrocarbon reaction feedstock (17) is injected continuously at a point above a rectification zone at the base of the column where the aromatic compound is separated from the paraffin and by-products washed from the catalyst. The use of the C 4 -C 16 paraffin with the aromatic at a mole fraction in the range of 40 to 90% enables a regeneration temperature of about 175 - 250°C. to be achieved and maintained by adjusting the column pressure and aromatic reflux rate. Significantly lower pressures, on the order of 125 to 370 psig, are required to achieve regeneration temperature than would be otherwise required with the use only of the aromatic hydrocarbon to dilute and wash the by-products from the catalyst surfaces.

    Abstract translation: 将独特的原位催化剂再生过程与压力下的连续反应蒸馏相结合的方法，用于使用在C 2 -C 30烯烃的回流区（21）中负载的固体酸烷基化催化剂烷基化轻质芳烃如C 2 -C 30烯烃 蒸馏塔（A部分）。 催化剂（部分E，F和G）的定期再生通过在塔顶部但在催化剂区上方的苯精馏区下面的C4-C16石蜡（35）逆流注入来进行，而芳族烃 将反应原料（17）连续注入塔的底部的精馏区上方，其中芳族化合物与石蜡分离，副产物从催化剂中洗脱。 使用具有40至90％摩尔分数的芳族化合物的C 4 -C 16石蜡使得能够通过调节柱压力和芳族回流速率来实现和维持约175-250℃的再生温度。 需要显着降低约125至370psig的压力以实现再生温度，而不是仅使用芳烃从催化剂表面稀释和洗涤副产物所需的压力。

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