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公开(公告)号：WO2016114177A1
公开(公告)日：2016-07-21
申请号：PCT/JP2016/050146
申请日：2016-01-05
Applicant: 昭和電工株式会社
Abstract: 本発明の金属酸化物粒子の製造方法は、予熱された金属塩化物含有ガスに、金属塩化物を含まない予熱された第１ガスを第１合流地点で合流させて第１合流ガスとし、第１合流ガスに、金属塩化物を含まない予熱された第２ガスを、第１合流地点よりも下流側に離れた第２合流地点で合流させて第２合流ガスとする工程を含み、金属塩化物含有ガス及び第１ガスの両方とも酸素、水蒸気を含有せず、第２ガスは少なくとも酸素を含有しており、第１ガスの予熱温度を、金属塩化物含有ガスの予熱温度以上の温度として合流させて、予熱された金属塩化物含有ガスを加熱し、第２ガスの予熱温度を、第１合流ガスの温度以上の温度として第１合流ガスと合流させて、第２合流地点から下流側において第１合流ガスを加熱することを特徴とする。
Abstract translation: 该金属氧化物粒子的制造方法的特征在于，在第一接合点将预热的不含金属氯化物的第一气体与预热的含有金属氯化物的气体接合，形成第一汇合气体，将预热后的第二气体 不含有金属氯化物的第一汇合气体在第一汇合点的下游的第二汇合点被接合到第一汇流气体中，从而形成第二汇流气体。 这种金属氧化物颗粒的制造方法的特征还在于：含金属氯化物的气体和第一气体不含有氧和水蒸汽; 第二气体至少含有氧气; 通过将第一气体接合而加热预热的含金属氯化物气体，同时将第一气体的预热温度设定为含有金属氯化物的气体的预热温度以上的温度; 并且通过将第二气体接合到第一汇流气体中，在第二汇合点的下游将第一汇流气体加热，同时将第二气体的预热温度设定为等于或高于第一汇合气体的温度的温度 。
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公开(公告)号：WO2011111848A3
公开(公告)日：2011-09-15
申请号：PCT/JP2011/055864
申请日：2011-03-07
Applicant: NATIONAL UNIVERSITY CORPORATION HOKKAIDO UNIVERSITY , SHOWA DENKO K.K. , OHTANI Bunsho , SUGISHITA Noriyuki , KURODA Yasushi
Inventor： OHTANI Bunsho , SUGISHITA Noriyuki , KURODA Yasushi
Abstract: There is provided a method and an apparatus for producing metal oxide particles, which produce metal oxide particles having a high photocatalytic activity with high yield. The method for producing metal oxide particles of the invention is characterized by including combining, in a reaction tube, a preheated metal chloride-containing gas with a preheated first gas which does not contain the metal chloride at a first junction to obtain a first combined gas, and combining the first combined gas with a preheated second gas which does not contain the metal chloride, at a second junction which is further downstream of the first junction, to obtain a second combined gas, wherein at least one of the metal chloride-containing gas and the first gas contains oxygen, and wherein the preheated metal chloride-containing gas is further heated in a region between the first junction and the second junction (referred to as first reaction zone), by combining the first gas with the metal chloride-containing gas at the first junction while setting the preheat temperature of the first gas at a temperature equal to or higher than the preheat temperature of the metal chloride-containing gas, and the first combined gas is further heated in a region downstream of the second junction by combining the second gas with the first combined gas at the second junction while setting the preheat temperature of the second gas at a temperature equal to or higher than the temperature of the first combined gas.
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3.发明申请
公开(公告)号：WO2009011528A3
公开(公告)日：2009-01-22
申请号：PCT/KR2008/004115
申请日：2008-07-11
Applicant: KIM, Jong-Hoon
Inventor： KIM, Jong-Hoon
IPC: C01B13/22
Abstract: The present invention relates to a preparation method of metal oxide, and more specifically to a preparation method of metal oxide comprising the steps of : a) dissolving metal halide in a solvent; b) adding and reacting water or metal hydroxide having strong basicity; c) adding base to the reaction solution and then raising a temperature thereof to form the metal oxide -carbon complex; d) stopping the reaction by inputting a large amount of water or metal hydroxide and raising the temperature thereof; and e) obtaining the metal oxide-carbon complex by a separation and a cleaning.
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公开(公告)号：WO2011111848A2
公开(公告)日：2011-09-15
申请号：PCT/JP2011055864
申请日：2011-03-07
Applicant: UNIV HOKKAIDO NAT UNIV CORP , SHOWA DENKO KK , OHTANI BUNSHO , SUGISHITA NORIYUKI , KURODA YASUSHI
Inventor： OHTANI BUNSHO , SUGISHITA NORIYUKI , KURODA YASUSHI
IPC: C01B13/22
CPC classification number: C01B13/22 , C01G1/02 , C01G23/07 , C01P2002/30 , C01P2004/03 , C01P2006/12 , C01P2006/90
Abstract: There is provided a method and an apparatus for producing metal oxide particles, which produce metal oxide particles having a high photocatalytic activity with high yield. The method for producing metal oxide particles of the invention is characterized by including combining, in a reaction tube, a preheated metal chloride-containing gas with a preheated first gas which does not contain the metal chloride at a first junction to obtain a first combined gas, and combining the first combined gas with a preheated second gas which does not contain the metal chloride, at a second junction which is further downstream of the first junction, to obtain a second combined gas, wherein at least one of the metal chloride-containing gas and the first gas contains oxygen, and wherein the preheated metal chloride-containing gas is further heated in a region between the first junction and the second junction (referred to as first reaction zone), by combining the first gas with the metal chloride-containing gas at the first junction while setting the preheat temperature of the first gas at a temperature equal to or higher than the preheat temperature of the metal chloride-containing gas, and the first combined gas is further heated in a region downstream of the second junction by combining the second gas with the first combined gas at the second junction while setting the preheat temperature of the second gas at a temperature equal to or higher than the temperature of the first combined gas.
Abstract translation: 提供了一种生产金属氧化物颗粒的方法和设备，其以高产率生产具有高光催化活性的金属氧化物颗粒。 本发明的金属氧化物粒子的制造方法的特征在于，在反应管中，将预热的含金属氯化物的气体与在第一接合处不含有金属氯化物的预热的第一气体组合，得到第一组合气体 并且在第二结合处将第一组合气体与不含金属氯化物的预热的第二气体组合，以获得第二组合气体，其中至少一种含金属氯化物的 气体，第一气体含有氧，并且其中预热的含金属氯化物的气体在第一接合点和第二接合点（称为第一反应区域）之间的区域中进一步加热，通过将第一气体与金属氯化物 - 在将第一气体的预热温度设定为等于或高于金属氯化物c的预热温度的温度的同时， 通过在第二连接处组合第二气体与第一组合气体，将第一组合气体在第二接合点的下游区域进一步加热，同时将第二气体的预热温度设定在等于或高于 第一组合气体的温度。
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公开(公告)号：WO2011024617A1
公开(公告)日：2011-03-03
申请号：PCT/JP2010/063117
申请日：2010-08-03
Applicant: 国立大学法人北海道大学 , 昭和電工株式会社 , 大谷 文章 , 杉下 紀之 , 黒田 靖
CPC classification number: C01G23/07 , B01J21/063 , B01J35/002 , B01J35/004 , B01J35/1014 , B01J37/088 , B01J37/14 , B01J37/349 , C01B13/22 , C01G23/00 , C01G23/047 , C01P2002/72 , C01P2004/03 , C01P2006/12 , C01P2006/80
Abstract: 光触媒活性の高い金属酸化物粒子を製造する金属酸化物粒子の製造方法及びその製造装置を提供することを目的とする。 反応管（１１）内で、金属塩化物を含む反応ガスと前記金属塩化物を含まない酸化性ガスとを予熱してから、前記反応ガスと前記酸化性ガスとからなる合流ガスを、その合流地点（５ｂ）よりも下流側に離れた本加熱領域（Ａ）で本加熱する金属酸化物粒子の製造方法であって、前記合流ガスが合流地点（５ｂ）から本加熱領域（Ａ）の上流端（Ａ１）に達するまでの時間を２５ミリ秒未満とする金属酸化物粒子の製造方法を用いることにより、上記課題を解決できる。
Abstract translation: 公开了一种用于制备具有高光催化活性的金属氧化物颗粒的金属氧化物颗粒的制备方法及其制备装置。 金属氧化物粒子的制造方法包括在反应管（11）中预热含有金属氯化物的反应气体和不含上述金属氯化物的氧化气体，然后实际加热包含上述反应物 气体和上述氧化气体在比气体的组合部位（5b）更下游的单独的实际加热区域（A）中; 其中上述组合气体从组合部位（5b）到达实际加热区域（A）的上游端（A1）的时间小于25毫秒。
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Patent Agency Ranking6.发明申请
公开(公告)号：WO2004052778A3
公开(公告)日：2004-11-18
申请号：PCT/CA0301881
申请日：2003-12-01
Applicant: TEKNA PLASMA SYSTEMS INC , BOULOS MAHER I , JUREWICZ JERZY W , NESSIM CHRISTINE A ABDEL MESSI
Inventor： BOULOS MAHER I , JUREWICZ JERZY W , NESSIM CHRISTINE A ABDEL MESSI
IPC: C01B13/14 , B01J19/08 , B01J19/12 , C01B13/20 , C01B13/22 , C01B13/28 , C01B13/30 , C01G23/07 , C09C1/36 , C22B4/00 , C22B4/08 , C22B34/12
CPC classification number: B82Y30/00 , B01J19/088 , B01J19/129 , B01J2219/0871 , B01J2219/0875 , B01J2219/0879 , B01J2219/0894 , C01B13/30 , C01G23/07 , C01G23/075 , C01P2002/50 , C01P2002/52 , C01P2002/72 , C01P2004/64 , C01P2006/12 , C09C1/36 , C09C1/3607 , C09C1/3669 , C22B4/005 , C22B4/08 , C22B34/129
Abstract: A process and apparatus for the synthesis of metal oxide nanopowder from a metal compound vapour is presented. In particular a process and apparatus for the synthesis of Ti02 nanopowder from TiCl4 is disclosed. The metal compound vapour is reacted with an oxidizing gas in electrically induced RF frequency plasma thus forming a metal oxide vapour. The metal oxide vapour is rapidly cooled using a highly turbulent gas quench zone which quickly halts the particle growth process, yielding a substantial reduction in the size of metal oxide particles formed compared with known processes. The metal compound vapour can also react with a doping agent to create a doped metal oxide nanopowder. Additionally, a process and apparatus for the inline synthesis of a coated metal oxide is disclosed wherein the metal oxide particles are coated with a surface agent after being cooled in a highly turbulent gas quench zone.
Abstract translation: 提出了一种从金属化合物蒸气合成金属氧化物纳米粉末的方法和装置。 公开了一种用于从TiCl4合成TiO 2纳米粉末的方法和装置。 金属化合物蒸汽与电感RF频率等离子体中的氧化气体反应，从而形成金属氧化物蒸气。 使用快速停止颗粒生长过程的高度湍流气体骤冷区快速冷却金属氧化物蒸汽，与已知方法相比，形成金属氧化物颗粒的尺寸显着减小。 金属化合物蒸汽也可以与掺杂剂反应以产生掺杂的金属氧化物纳米粉末。 此外，公开了一种用于在线合成涂覆的金属氧化物的方法和装置，其中在高度湍流的气体骤冷区域中冷却之后，金属氧化物颗粒被表面剂涂覆。
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7.发明申请PREPARATION METHOD OF METAL OXIDE FROM METAL HALIDE BY DEHYDRO HALOGENATION WITH BASE AND METAL OXIDE PREPARED THEREFROM 审中-公开由金属卤化物制备金属氧化物用脱氢卤化法制备碱金属氧化物和由此制备的金属氧化物
公开(公告)号：WO2009011528A2
公开(公告)日：2009-01-22
申请号：PCT/KR2008004115
申请日：2008-07-11
Applicant: KIM JONG-HOON
Inventor： KIM JONG-HOON
IPC: C01B13/22
CPC classification number: C01B13/32 , B82Y30/00 , C01F7/02 , C01G49/04 , C01G49/06 , C01P2002/72 , C01P2002/85 , C01P2004/04 , C01P2004/64
Abstract: The present invention relates to a preparation method of metal oxide, and more specifically to a preparation method of metal oxide comprising the steps of : a) dissolving metal halide in a solvent; b) adding and reacting water or metal hydroxide having strong basicity; c) adding base to the reaction solution and then raising a temperature thereof to form the metal oxide -carbon complex; d) stopping the reaction by inputting a large amount of water or metal hydroxide and raising the temperature thereof; and e) obtaining the metal oxide-carbon complex by a separation and a cleaning.
Abstract translation: 本发明涉及一种金属氧化物的制备方法，更具体地涉及金属氧化物的制备方法，该方法包括以下步骤：a）将金属卤化物溶解在溶剂中; b）加入具有强碱性的水或金属氢氧化物并进行反应; c）向反应溶液中加入碱，然后升高其温度以形成金属氧化物 - 碳络合物; d）通过输入大量的水或金属氢氧化物并升高其温度来停止反应; 和e）通过分离和清洁获得金属氧化物 - 碳络合物。
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公开(公告)号：WO2007050682A3
公开(公告)日：2008-01-24
申请号：PCT/US2006041627
申请日：2006-10-26
Applicant: DU PONT , SUBRAMANIAN NARAYANAN SANKARA , BERNARD RICHARD P , HSU YUNG-HSING SAMSON , MUSICK CHARLES DAVID , OGUNDE KUNLE , TILTON JAMES NELSON
Inventor： SUBRAMANIAN NARAYANAN SANKARA , BERNARD RICHARD P , HSU YUNG-HSING SAMSON , MUSICK CHARLES DAVID , OGUNDE KUNLE , TILTON JAMES NELSON
CPC classification number: C01G23/07 , C01G23/075 , C01P2004/61 , C09C1/3607
Abstract: This disclosure relates to a process for producing titanium dioxide, comprising: a) providing a quantity of liquid titanium tetrahalide for reacting with an oxygen-containing gas; b) vaporizing a first portion of the liquid titanium tetrahalide and reacting the titanium tetrahalide vapor and the oxygen-containing gas, in a first stage of a reaction zone, the reaction zone temperature ranging from at least about 650°C to form a reaction product at least containing titanium dioxide and oxygen-containing gas and passing the reaction product, more typically in the vapor phase, to at least one additional stage of the reaction zone; and c) charging at least one additional portion of the liquid titanium tetrahalide to the at least one additional stage of the reaction zone to cool the titanium dioxide and to react with the oxygen-containing gas to form additional titanium dioxide. This process results in a high conversion to titanium dioxide and formation of titanium dioxide powders having improved particle size and size distribution.
Abstract translation: 本公开涉及一种生产二氧化钛的方法，包括：a）提供一定数量的四卤化钛用于与含氧气体反应; b）蒸发液态四卤化钛的第一部分并使四卤化钛蒸气和含氧气体在反应区的第一阶段中反应，反应区温度为至少约650℃，形成反应产物 至少含有二氧化钛和含氧气体，并将反应产物，更典型地在气相中送至反应区的至少一个附加阶段; 和c）将至少另外一部分液体四卤化钛装入至该反应区的至少一个附加阶段以冷却二氧化钛并与含氧气体反应以形成另外的二氧化钛。 该方法导致二氧化钛的高转化率和具有改进的粒度和尺寸分布的二氧化钛粉末的形成。
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9.发明申请METHOD FOR THE CONTROL OF THE COMPOSITION AND PHYSICAL PROPERTIES OF SOLID URANIUM OXIDES 审中-公开控制固体氧化铀的组成和物理性质的方法
公开(公告)号：WO98031632A1
公开(公告)日：1998-07-23
申请号：PCT/US1998/000346
申请日：1998-01-14
IPC: C01G43/01 , C01G43/025 , C01B13/22
CPC classification number: C01G43/01 , C01G43/025 , Y02P20/129
Abstract: The present invention provides a method for varying and controlling the chemical composition and physical properties of the uranium oxide solids produced by the thermal conversion of UF6. The method allows the production of predominantly UO2, U3O8, or UO3 interchangeably from the same reactor simply by controlling the hydrogen and oxygen contents of the feed relative to uranium. The temperature profile of the thermal reactor is established by specifying the preheat of the feed prior to mixing, the feed composition, and the reactor wall temperature to thus vary and control the physical properties of the resulting solids according to the end use of the uranium product.
Abstract translation: 本发明提供了一种用于改变和控制由UF6的热转化产生的氧化铀固体的化学组成和物理性质的方法。 该方法允许主要通过相对于铀控制进料的氢和氧含量从相同的反应器互换地生产UO2，U3O8或UO3。 热反应器的温度曲线是通过在混合之前指定进料的预热，进料组成和反应器壁温度来确定的，从而根据铀产品的最终用途改变和控制所得固体的物理性能 。
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10.发明申请NONAQUEOUS CHLORINE DIOXIDE-GENERATING COMPOSITIONS AND METHODS RELATED THERETO 审中-公开不产生二氧化氯的组合物及其相关方法
公开(公告)号：WO2010096300A2
公开(公告)日：2010-08-26
申请号：PCT/US2010023575
申请日：2010-02-09
Applicant: BASF CATALYSTS LLC , HRATKO LINDA , SPERONELLO BARRY KEVEN
Inventor： HRATKO LINDA , SPERONELLO BARRY KEVEN
CPC classification number: C01B11/023 , C01B11/024
Abstract: A method for generating chlorine dioxide is disclosed in which chlorine dioxide generation is activated with a dry polar material. A system for generating chlorine dioxide is also disclosed, as well as compositions useful in the system and method.
Abstract translation: 公开了一种产生二氧化氯的方法，其中二氧化氯的产生用干燥的极性物质活化。 还公开了用于产生二氧化氯的系统，以及用于该系统和方法的组合物。
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