Invention Grant
- Patent Title: Nanocomposites containing silica nanoparticles and dispersant, composites, articles, and methods of making same
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Application No.: US14911058Application Date: 2014-08-12
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Publication No.: US10442914B2Publication Date: 2019-10-15
- Inventor: Peter D. Condo , Jeremy O. Swanson , James E. Thorson , Kristin L. Thunhorst
- Applicant: 3M INNOVATIVE PROPERTIES COMPANY
- Applicant Address: US MN St. Paul
- Assignee: 3M Innovative Properties Company
- Current Assignee: 3M Innovative Properties Company
- Current Assignee Address: US MN St. Paul
- Agent Adrian L. Pishko
- International Application: PCT/US2014/050661 WO 20140812
- International Announcement: WO2015/023640 WO 20150219
- Main IPC: C08K9/04
- IPC: C08K9/04 ; C09D7/40 ; C08J5/24 ; C08K9/06 ; C08J5/00 ; C08K7/00 ; C08K7/18 ; C08K7/28 ; C08L63/00 ; C08K3/36 ; C09D7/20

Abstract:
A nanocomposite is provided including silica nanoparticles and a dispersant dispersed in a curable resin or a curing agent, where the nanocomposite contains less than 2% by weight solvent. The silica nanoparticles include nonspherical silica nanoparticles and/or spherical pyrogenic silica nanoparticles. A composite is also provided including from about 4 to 70 weight percent of silica nanoparticles, and a dispersant, dispersed in a cured resin, and a filler embedded in the cured resin. Optionally, the composite further contains a curing agent. Further, a method of preparing a nanoparticle-containing curable resin system is provided including mixing from 10 to 70 weight percent of aggregated silica nanoparticles with a curable resin and a dispersant to form a mixture. The mixture contains less than 2% by weight solvent. The method also includes milling the mixture in an immersion mill containing milling media to form a milled resin system including silica nanoparticles dispersed in the curable resin.
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