发明授权
- 专利标题: Joint production method and device for aziridine, piperazine and triethylenediamine
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申请号: US15105883申请日: 2014-09-05
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公开(公告)号: US09850250B2公开(公告)日: 2017-12-26
- 发明人: Jianming Yang , Suning Mei , Qinwei Yu , Feng Hui , Jun Yuan , Wei Wang , Yani Li , Weiqiang Wang , Jian Lu
- 申请人: XI'AN MODERN CHEMISTRY RESEARCH INSTITUTE
- 申请人地址: CN Shaanxi
- 专利权人: XI'AN MODERN CHEMISTRY RESEARCH INSTITUTE
- 当前专利权人: XI'AN MODERN CHEMISTRY RESEARCH INSTITUTE
- 当前专利权人地址: CN Shaanxi
- 代理机构: Seed IP Law Group LLP
- 优先权: CN201310698872 20131218
- 国际申请: PCT/CN2014/086019 WO 20140905
- 国际公布: WO2015/090085 WO 20150625
- 主分类号: C07D487/08
- IPC分类号: C07D487/08 ; C07D203/02 ; C07D295/023 ; B01J27/18 ; B01J21/02 ; B01J21/06 ; B01J19/00 ; B01J31/02
摘要:
Disclosed are a joint production method and device for aziridine, piperazine and triethylenediamine. The method comprises: reaction 1, preparing piperazine and triethylenediamine by taking ethanol amine as a raw material under the existence of a cyclamine catalyst; reaction 2, preparing aziridine by taking the ethanol amine as the raw material under the existence of a catalyst B; and taking heat released in the reaction 1 as a heat source of heat absorption in the reaction 2. The device comprises a reactor 1 for carrying out the reaction 1 and the heat exchange between reaction materials of the reaction 1 and the raw material of the reaction 2 and a reactor 2 for carrying out the reaction 2. According to the present invention, the same raw material, namely the ethanol amine is adopted, aziridine, piperazine and triethylenediamine can be produced in a joint manner, the heat released in the reaction 1 is used for preheating materials in the reaction 2, so that heat coupling between the reactions is implemented, energy conservation is facilitated and competitiveness of the device is improved.
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