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    REACTOR AND PROCESS
    11.
    发明公开
    REACTOR AND PROCESS 审中-公开
    反应器和方法

    公开(公告)号：EP1713721A2

    公开(公告)日：2006-10-25

    申请号：EP04768928.6

    申请日：2004-10-18

    申请人： Phoenix Chemicals Limited

    发明人： WARR, Antony, John ,  PROCTOR, Lee David

    IPC分类号： C01B21/09 ,  C01C1/16 ,  B01J12/00

    CPC分类号： C01C1/164 ,  B01J4/002 ,  B01J4/02 ,  B01J19/24 ,  C01B21/091

    摘要： The invention relates to a process for the production of chloramine comprising supplying a first reagent stream comprising chlorine gas and a second reagent stream comprising ammonia gas to a reaction zone maintained at a temperature of less than 275° C and configured to allow expansion of the first and second reagent streams in the reaction zone to an extent sufficient to generate chloramine as a gas and ammonium chloride as a free falling solid. The invention also provides a chemical reactor suitable for operating this process.

    PLANT FOR THE PRODUCTION OF MONOCHLORAMINE AND PROCESS THEREOF
    12.
    发明公开
    PLANT FOR THE PRODUCTION OF MONOCHLORAMINE AND PROCESS THEREOF 审中-公开
    安格尔ZER HERSTELLUNG VON MONOCHLORAMIN UND VERFAHRENDAFÜR

    公开(公告)号：EP3015424A1

    公开(公告)日：2016-05-04

    申请号：EP15191748.1

    申请日：2015-10-27

    申请人： Acel S.r.l.

    发明人： GATTI, Marco ,  CAUZZI, Daniele Alessandro

    IPC分类号： C01B21/09 ,  B01J14/00 ,  C02F1/76

    CPC分类号： C01B21/091 ,  C02F1/76

    摘要： A process for the production of monochloramine characterized in that it provides for drawing a portion of water intended for the user and exclusively using said portion for preparing the monochloramine solution. The portion intended for the reaction of formation of monochloramine is subjected to a treatment on osmotic membrane, obtaining osmotized water. Subsequently, there is the reaction of said water with reagents in a reactor. In the reaction step, inside the reactor, the osmotized water enters from a first orifice (C) by means of a solenoid valve with micrometric regulation (EV1). Inside the same reactor, the base chemical products enter by means of the respective orifices A and B. The base chemical products enter due to the action of metering pumps (e.g. peristaltic pumps). The system is managed by PLC.

    摘要翻译： 一种用于生产一氯胺的方法，其特征在于它提供了一部分用于使用者的水并且专门使用所述部分来制备一氯胺溶液。 用于形成一氯胺的反应部分在渗透膜上进行处理，得到渗透水。 随后，在反应器中存在所述水与试剂的反应。 在反应步骤中，在反应器内，渗透水通过具有微量调节（EV1）的电磁阀从第一孔口（C）进入。 在同一反应器内，基础化学产品通过相应的孔A和B进入。基础化学品由于计量泵（例如蠕动泵）的作用而进入。 该系统由PLC管理。

    METHOD AND APPARATUS FOR MONITORING AND CONTROLLING EXOTHERMIC AND ENDOTHERMIC CHEMICAL REACTIONS
    13.
    发明公开
    METHOD AND APPARATUS FOR MONITORING AND CONTROLLING EXOTHERMIC AND ENDOTHERMIC CHEMICAL REACTIONS 审中-公开
    方法和仪器监测和控制吸热放热化学反应

    公开(公告)号：EP2906339A2

    公开(公告)日：2015-08-19

    申请号：EP13774012.2

    申请日：2013-09-24

    申请人： Buckman Laboratories International, Inc

    发明人： MCNEEL, Thomas E. ,  CLARK, Richard A. ,  LUSK, JR., Richard D.

    IPC分类号： B01J19/00 ,  B01J14/00 ,  C01B21/09

    CPC分类号： C01B21/091 ,  B01J14/00 ,  B01J19/0013 ,  B01J2219/00063 ,  B01J2219/00164 ,  B01J2219/00198 ,  B01J2219/00202 ,  B01J2219/00213 ,  B01J2219/0022 ,  B01J2219/00225 ,  B01J2219/00231

    摘要： A method of controlling an exothermic or endothermic chemical reaction is provided. The method involves measuring a temperature of a first reactant flowing at a first flow rate, contacting the first reactant with a second reactant flowing at a second flow rate to form a reaction product, measuring the temperature of the reaction product, and determining the temperature difference between the temperature of the first reactant and the temperature of the reaction product. The method can further involve adjusting the flow rate of at least one of the first reactant and the second reactant, or shutting down flow, based on the temperature difference. An apparatus to carry out the method is also provided. The method and apparatus can be useful in controlling many different reactions, including the reaction of sodium hypochlorite and ammonia to form monochloramine.

    摘要翻译： 提供放热或吸热化学反应的控制的方法。 该方法包括测量在第一流速流动的第一反应物的温度，接触，以第二流速流动的第二反应物的第一反应物以形成反应产物，测定上述反应生成物的温度，并且确定性采矿的温度差 第一反应物的温度和反应产物的温度之间。 该方法可包括进一步的调节第一和第二反应物反应物中的至少一个的流量，或关闭流，基于所述温度差。 因此，提供给执行该方法的装置。 该方法和装置可以在控制许多不同的反应，包括次氯酸钠和氨的反应以形成单氯胺是有用的。

    PRODUCTION OF GASEOUS CHLORAMINE
    15.
    发明公开
    PRODUCTION OF GASEOUS CHLORAMINE 审中-公开
    气态氯胺的生产

    公开(公告)号：EP1560789A2

    公开(公告)日：2005-08-10

    申请号：EP03783616.0

    申请日：2003-11-14

    申请人： Bristol-Myers Squibb Company

    发明人： TUMMALA, Srinivas ,  LEUNG, Shun, Wang ,  LO, Ehrlic, T. ,  ALVAREZ, Mario Moisés

    IPC分类号： C01B21/083

    CPC分类号： C01C1/164 ,  B01J4/001 ,  B01J12/00 ,  B01J2219/0254 ,  B01J2219/0286 ,  C01B21/091

    摘要： A process and reactor for the gas-phase reaction of commercially available gases in the presence of an inert carrier gas to from product gas. The reactor (10) has an outer shell tube (12) and an inner tube (16), both of which feed reaction chamber (18). At last one first commercially available fed gas is fed to outré tube (12) via first inlet (13). One or more inert gases is fed to outer tube (12) via second inlet (14). In the case of chloramines gas formation, chlorine gas reacts with ammonia. Gas at reaction zone (20) in reaction chamber (18), which is heated by one or more heating elements (22). The product gas stream exits reaction chamber (18) via discharge tube (26).

    摘要翻译： 用于在惰性载气存在下使市售气体与产物气体进行气相反应的方法和反应器。 反应器（10）具有外壳管（12）和内管（16），两者都进料反应室（18）。 最后一个可商购的进料气体经由第一入口（13）被输送到出口管（12）。 一种或多种惰性气体通过第二入口（14）供给到外管（12）。 在氯胺气体形成的情况下，氯气与氨反应。 在反应室（18）中的反应区（20）处的气体由一个或多个加热元件（22）加热。 产物气流通过排放管（26）离开反应室（18）。

    Improved process for preparing hydrazines
    17.
    发明公开
    Improved process for preparing hydrazines 失效
    Verfahren zur Herstellung von Hydrazinen。

    公开(公告)号：EP0134259A1

    公开(公告)日：1985-03-20

    申请号：EP83107623.7

    申请日：1983-08-02

    申请人： Osborg, Hans

    发明人： Osborg, Hans

    IPC分类号： C07C241/02 ,  C01B21/16 ,  C01B21/09

    CPC分类号： C01B21/091 ,  C01B21/16 ,  C07C241/02 ,  C07C243/14 ,  C07C243/40

    摘要： Anhydrous hydrazine and hydrocarbyl-substituted hydrazines are efficiently prepared according to a three-step procedure, comprising a first step wherein ammonia, a primary or secondary amine, an alkali metal amide, an alkaline earth metal amide, a hydrocarbyl-substituted alkali metal amide or a hydrocarbyl-substituted alkaline earth metal amide is reacted with a chlorinating agent to produce the corresponding chloramine without co-production of an amine hydrochloride salt; a second step wherein the chloramine is reacted with a tertiary amine to produce a tertiary hydrazinium chloride; and a final step wherein the tertiary hydrazinium chloride is reacted with an alkali metal amide or an alkaline earth metal amide under anhydrous conditions to produce the desired product.

    摘要翻译： 无水肼和烃基取代的肼根据三步法有效制备，包括第一步，其中氨，伯或仲胺，碱金属氨化物，碱土金属酰胺，烃基取代的碱金属酰胺或 烃基取代的碱土金属酰胺与氯化剂反应生成相应的氯胺而不共同制备胺盐酸盐; 第二步，其中氯胺与叔胺反应产生叔氯化铵氯化铵; 和最后一步，其中叔无水氯化铵在无水条件下与碱金属氨化物或碱土金属酰胺反应以产生所需产物。