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    PROCESS FOR PREPARING A HALOGENATED POLYMER AND DEVICE FOR THE IMPLEMENTATION THEREOF
    14.
    发明公开
    PROCESS FOR PREPARING A HALOGENATED POLYMER AND DEVICE FOR THE IMPLEMENTATION THEREOF 审中-公开
    制备卤化聚合物的方法及其实施方法

    公开(公告)号：EP2513167A1

    公开(公告)日：2012-10-24

    申请号：EP10787798.7

    申请日：2010-12-13

    申请人： SOLVAY SA

    发明人： DE FRANCISCO, Manuel ,  CLAEYS, Ivan

    IPC分类号： C08F14/00 ,  B01J3/00

    CPC分类号： B01J19/242 ,  B01J3/008 ,  B01J2219/00006 ,  B01J2219/00094 ,  B01J2219/00108 ,  B01J2219/0011 ,  B01J2219/00162 ,  C08F2/04 ,  C08F14/00 ,  C08F14/06 ,  Y02P20/544 ,  C08F2/20

    摘要： Continuous process for preparing a halogenated polymer comprising a step of polymerization of at least one halogenated monomer in a medium comprising carbon dioxide in the liquid or supercritical state (L/SC-CO2), in at least one pressurized reactor, said process comprising at least : - (1) an expansion of the suspension resulting from the reactor; - (2) a separation of the expanded suspension resulting from the reactor into a first stream, containing the solid phase comprising the halogenated polymer and into a liquid, gaseous or supercritical second stream, which is a mixture Of CO2 and of monomer not converted to polymer; and the recovery of this first stream and of this second stream; - (3) an optional reheating, applied to the expanded suspension, before or after its separation into first and second streams, with optional recovery of the cold energy generated by the expansion; - (4) a recompression of the second stream and the optional cooling thereof in order to recycle it, at a plurality of points, to the reactor feed, with a fresh monomer make-up and, possibly, a CO2 make-up; - (5) a final step of degassing the halogenated polymer, optionally in combination with a continuous technique of forming the polymer into granules. Device for implementing the process.

    摘要翻译： 用于制备卤化聚合物的连续方法，其包括在至少一个加压反应器中在包含液态或超临界态（L / SC-CO 2）的二氧化碳的介质中聚合至少一种卤代单体的步骤，所述方法包括在 至少：（1）由反应器产生的悬浮液的膨胀; - （2）将由反应器产生的膨胀悬浮液分离成含有包含卤化聚合物的固相的第一物流和分离成液体，气体或超临界第二物流，该第二物流是CO 2和未转化的单体的混合物 聚合物; 并回收这第一股流和这第二股流; - （3）在分离成第一和第二物流之前或之后，对膨胀的悬浮液进行任选的再加热，同时可任意回收由膨胀产生的冷能; - （4）第二物流的再压缩和其任选的冷却以便在多个点处将其再循环至反应器进料，其中新鲜的单体化妆品和可能的CO 2补充物; - （5）将卤化聚合物脱气的最后步骤，任选地与将聚合物形成颗粒的连续技术组合。 实施过程的设备。

    Continuous polymerization apparatus and process for producing polymer composition
    16.
    发明公开
    Continuous polymerization apparatus and process for producing polymer composition 审中-公开
    聚合物聚合物和聚合物聚合物

    公开(公告)号：EP2481477A1

    公开(公告)日：2012-08-01

    申请号：EP12152511.7

    申请日：2012-01-25

    申请人： Sumitomo Chemical Company, Limited

    发明人： Sumida, Masakazu ,  Yamazaki, Kazuhiro ,  Sato, Yoshinori ,  Wake, Takao

    IPC分类号： B01J19/00 ,  B01J19/18 ,  C08F20/18 ,  C08F2/01 ,  C08F2/02

    CPC分类号： B01J19/0013 ,  B01J19/0033 ,  B01J19/006 ,  B01J19/0066 ,  B01J19/1856 ,  B01J2219/00094 ,  B01J2219/00159 ,  B01J2219/00189 ,  B01J2219/002 ,  B01J2219/00213 ,  B01J2219/00231 ,  B01J2219/00238 ,  C08F2/001 ,  C08F2/01 ,  C08F2/04

    摘要： The present invention is directed to provide a novel continuous polymerization apparatus which is able to more efficiently produce a polymer composition having a variety of properties.
    In a continuous polymerization apparatus at least two reactors (10, 20) of a complete mixing type are used. Each of the reactors (10, 20) is provided with a supply port (11a, 21a) and an effluent port (11b, 21b); the respective supply ports (11a, 21a) of the two reactors (10, 20) are commonly connected to a supply source (1, 3) of a raw material monomer and a polymerization initiator; a flow control valve (8) is installed on a raw material supply line (9) for supplying a mixture comprising the raw material monomer and the polymerization initiator from the supply source (1, 3) of the raw material monomer and the polymerization initiator to the respective supply ports (11a, 21a) of the two reactors (10, 20); and the respective effluent ports (11b, 21b) of the two reactors (10, 20) are connected to a common effluent line (27).

    摘要翻译： 本发明旨在提供一种能够更有效地制备具有多种性质的聚合物组合物的新型连续聚合装置。 在连续聚合装置中，使用至少两个完全混合型的反应器（10,20）。 每个反应器（10,20）设置有供给口（11a，21a）和排出口（11b，21b）; 两个反应器（10,20）的供给口（11a，21a）共同连接到原料单体和聚合引发剂的供给源（1,3） 将原料单体和聚合引发剂的混合物从原料单体和聚合引发剂的供给源（1,3）供给到原料供给管线（9）上的流量控制阀（8） 两个反应器（10,20）的各个供应口（11a，21a）; 并且两个反应器（10,20）的各个流出物端口（11b，21b）连接到共同的流出物管线（27）。