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    VERWENDUNG VON CYCLISCHEN CARBONATEN IN EPOXIDHARZZUSAMMENSETZUNGEN
    45.
    发明公开
    VERWENDUNG VON CYCLISCHEN CARBONATEN IN EPOXIDHARZZUSAMMENSETZUNGEN 有权
    环状碳酸酯的在环氧树脂中使用

    公开(公告)号：EP2582740A1

    公开(公告)日：2013-04-24

    申请号：EP11726123.0

    申请日：2011-06-14

    Applicant: BASF SE

    Inventor： KLOPSCH, Rainer ,  LANVER, Andreas ,  KAFFEE, Achim ,  EBEL, Klaus ,  YU, Miran

    IPC: C08G59/40 ,  C08L63/00

    CPC classification number: C08G59/4007 ,  C08K5/06 ,  C08L63/00

    Abstract: The invention relates to the use of cyclic carbonates of formula I or mixtures thereof in epoxy resin compositions, and epoxy resin compositions that contain such cyclic carbonates. In said formula R
    1 and R
    2 represent, independently of one another, hydrogen, C
    1 -C
    6 -alkyl, C
    1 -C
    4 -alkoxy-C
    1 -C
    4 -alkyl, C
    5 -C
    6 -cycloalkyl, phenyl, phenyl-C
    1 -C
    4 -alkyl, C
    2 -C
    6 -alkenyl or C
    2 -C
    6 -alkinyl, or R
    1 and R
    2 together represent a C
    3 -C
    11 -alkylene group; R
    3 and R
    4 represent, independently of one another, hydrogen, C
    1 -C
    6 -alkyl, C
    1 -C
    4 -alkoxy-C
    1 -C
    4 -alkyl, C
    5 -C
    6 -cycloalkyl, phenyl, phenyl-C
    1 -C
    4 -alkyl, C
    2 -C
    6 -alkenyl or C
    2 -C
    6 -alkinyl, or R
    3 and R
    4 together represent a C
    4 -C
    6 -alkylene group; or mixtures thereof, as an additive in epoxy resin compositions.

    VERFAHREN ZUR HERSTELLUNG HYDROXY-SUBSTITUIERTER AROMATISCHER ALDEHYDE
    46.
    发明公开
    VERFAHREN ZUR HERSTELLUNG HYDROXY-SUBSTITUIERTER AROMATISCHER ALDEHYDE 有权
    VERFAHREN ZUR HERSTELLUNG HYDROXY-SUBSTITERERTER AROMATISCHER ALDEHYDE

    公开(公告)号：EP2552880A1

    公开(公告)日：2013-02-06

    申请号：EP11710524.7

    申请日：2011-03-29

    Applicant: BASF SE

    Inventor： EBEL, Klaus ,  RÜDENAUER, Stefan

    IPC: C07C45/67 ,  C07C47/565 ,  C07C47/575 ,  C07C47/58

    CPC classification number: C07C45/673 ,  Y02P20/582 ,  C07C47/58 ,  C07C47/565 ,  C07C47/575

    Abstract: The present invention accordingly provides a process for preparing aldehydes of the formula (I) in which one, two or all three radicals of the group R
    1 , R
    3 and R
    5 denote hydroxyl, and the radical or radicals of the group R
    1 , R
    3 and R
    5 that do not denote hydroxyl are, independently of one another, hydrogen, C
    1 -C
    8 alkyl or C
    6 -C
    14 aryl, and R
    2 and R
    4 independently of one another are hydrogen, C
    1 -C
    8 alkyl, C
    1 -C
    8 alkoxy or C
    6 -C
    14 aryl, the process being characterized in that an aldehyde of the formula (II) in which one, two or all three radicals of the group R'
    1 , R'
    3 and R'
    5 denote C
    1 -C
    8 alkoxy, and the radical or radicals of the group R'
    1 , R'
    3 and R'
    5 that do not denote C
    1 -C
    8 alkoxy are, independently of one another, hydrogen, C
    1 -C
    8 alkyl or C
    6 -C
    14 aryl, and R
    2 and R
    4 have the definitions indicated under formula (I), is reacted at elevated temperature and elevated pressure in the presence of (C
    1 -C
    4 alkyl)
    2 -amine, and the reaction product of the formula (I) is subsequently isolated.

    Abstract translation: 因此，本发明提供了制备式（I）的醛的方法，其中R1，R3和R5基团中的一个，两个或全部三个基团表示羟基，R1，R3和R5基团的基团或基团 不表示羟基彼此独立地为氢，C1-C8烷基或C6-C14芳基，R2和R4彼此独立地为氢，C1-C8烷基，C1-C8烷氧基或C6-C14芳基， 方法的特征在于式（II）的醛，其中R 1，R 3和R 5基团中的一个，两个或全部三个基团表示C 1 -C 8烷氧基，以及基团的基团或基团 不表示C1-C8烷氧基的R'1，R'3和R'5彼此独立地为氢，C1-C8烷基或C6-C14芳基，R2和R4具有式（I ）在升高的温度和升高的压力下在（C 1 -C 4烷基）2-胺的存在下反应，随后分离式（I）的反应产物。

    VERFAHREN ZUR HERSTELLUNG M- ODER P-SUBSTITUIERTER PHENYLALKANOLE DURCH ALKYLIERUNG
    47.
    发明公开
    VERFAHREN ZUR HERSTELLUNG M- ODER P-SUBSTITUIERTER PHENYLALKANOLE DURCH ALKYLIERUNG 有权
    过程为生产或M-P-取代的苯基链烷醇烷基化

    公开(公告)号：EP2490992A1

    公开(公告)日：2012-08-29

    申请号：EP10765445.1

    申请日：2010-10-14

    Applicant: BASF SE

    Inventor： LANVER, Andreas ,  EBEL, Klaus ,  BECK, Karl ,  PELZER, Ralf ,  BOTZEM, Jörg ,  GRIESBACH, Ulrich

    IPC: C07C29/32 ,  C07C29/56 ,  C07C33/20 ,  C07C45/29 ,  C07C47/228

    CPC classification number: C07C29/32 ,  C07C29/56 ,  C07C45/29 ,  C07C33/20 ,  C07C47/228

    Abstract: The invention provides a process for preparing m- or p-substituted phenylalkanols of the formula (I) in which R
    1 is m- or p-bonded to the phenyl ring and is C
    1 -C
    5 -alkyl, and R
    2 , R
    3, R
    4 and R
    5 are each independently hydrogen or methyl, which is characterized in that an unsubstituted phenylalkanol of the formula (II) in which R
    2 , R
    3 , R
    4 and R
    5 are each as defined for formula (I) is alkylated together with a C
    1 -C
    5 -alkyl halide of the formula (III) R
    1 Hal (III), in which R
    1 is as defined for formula (I) and Hal is halogen, in the presence of a Friedel-Crafts catalyst, to give an m- or p-alkyl-substituted phenylalkanol of the formula (I), then the reaction mixture is worked up and the desired m- or p-alkyl-substituted phenylalkanol of the formula (I) is removed, the remaining by-products formed are returned to the reaction mixture and these are isomerized in the presence of a Friedel-Crafts catalyst to give the desired m- or p- alkyl-substituted phenylalkanol. The m- or p-alkyl-substituted phenylalkanols of the formula (I) can be used to form, by oxidation or dehydrogenation, as products of value, the corresponding aldehydes, which are of interest as fragrances and aroma chemicals.

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