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    PROCESS FOR PRODUCING ALKYLENE OXIDE
    71.
    发明授权
    PROCESS FOR PRODUCING ALKYLENE OXIDE 有权
    用于生产亚

    公开(公告)号：EP1654242B1

    公开(公告)日：2010-09-08

    申请号：EP04756272.3

    申请日：2004-06-28

    申请人： Shell Internationale Research Maatschappij B.V.

    发明人： MURRAY, Brendan, Dermot ,  VAPORCIYAN, Garo, Garbis

    IPC分类号： C07D301/19

    CPC分类号： C07D301/19 ,  Y02P20/127

    摘要： A process for preparing an alkylene oxide, which process comprises: (i) oxidizing an alkylebenzene to obtain a stream comprising alkylbenzene hydroperoxide; (ii) contacting at least part of the alkylbenzene hydroperoxide obtained in step (i) with an olefin to obtain a product stream comprising an alkylene oxide; (iii) separating alkylene oxide compound from the product stream of step (ii) to obtain (a) a residual product stream comprising alkylphenyl alcohol, and (b) alkylene oxide; (iv) feeding at least a part of the residual product stream comprising alkylphenyl alcohol to a reactor having a catalytic distillation zone, and concurrently in the reactor: (a) contacting the residual product stream comprising alkylphenyl alcohol with hydrogen in the catalytic distillation zone to convert the alkylphenyl alcohol in the residual product stream to alkylbenzene and from a reaction mixture; and, (b) separating alkylbenze from the reaction mixture by fraction distillation; (v) withdrawing a stream comprising alkybenzene and having a reduced concentration of alkylphenyl alcohol than the feed stream from the reactor at a position upper from the catalytic reaction zone; withdrawing from the reactor at a position lower than the catalytic distillation zone a bottom stream comprising dimer(s) of alkylbenzene; alkylbenze; and. (viii) recycling at least a part of the alkylbenzene produced from (iv)(b) and/or (vi) to step (i).

    PROCESS FOR PREPARING AN ALKYLENE OXIDE
    73.
    发明公开
    PROCESS FOR PREPARING AN ALKYLENE OXIDE 审中-公开
    用于生产亚

    公开(公告)号：EP1727606A1

    公开(公告)日：2006-12-06

    申请号：EP05717143.1

    申请日：2005-03-24

    申请人： Shell Internationale Research Maatschappij B.V.

    发明人： HEISZWOLF, Gerhard Johan ,  DE VRIES, Enno Boelo

    IPC分类号： B01D17/04 ,  C07D301/32

    CPC分类号： C07D301/19 ,  C07D301/32

    摘要： Process for preparing an alkylene oxide, which process comprises: (a) oxidation of an organic compound to obtain reaction product containing organic hydroperoxide, (b) washing at least part of the organic hydroperoxide containing reaction product with a basic aqueous solution, (c) separating the mixture obtained in step (b) into a hydrocarbonaceous phase and an aqueous phase, (d) washing at least part of the hydrocarbonaceous phase obtained in step (c) with water, (e) separating the mixture obtained in step (d) into a hydrocarbonaceous phase and an aqueous phase, and (f) contacting at least part of the hydrocarbonaceous phase' obtained in step (e) with an alkene and catalyst to obtain an alkylene oxide, in which process the separation of hydrocarbonaceous phase and aqueous phase of step (c) and/or (e) is carried out with the help of a coalescer containing polypropylene fibers.

    PROCESS FOR PREPARING ORGANIC HYDROPEROXIDES
    74.
    发明授权
    PROCESS FOR PREPARING ORGANIC HYDROPEROXIDES 有权
    制备有机氢氧化物的方法

    公开(公告)号：EP1440058B1

    公开(公告)日：2006-11-15

    申请号：EP02779377.7

    申请日：2002-09-19

    申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.

    发明人： DU CAUZE DE NAZELLE, Gerard ,  FOONG, Wan, Shi ,  GARRITSEN, Tjeerd, Willem ,  JUNE, Raymond, Lawrence ,  OTHMAN, Mohammad, Azmi, Bin ,  SCHOUTEN, Eduardus, Petrus, Simon

    IPC分类号： C07C407/00 ,  C07C409/08 ,  C07D301/19

    CPC分类号： C07D301/19 ,  C07C15/40 ,  C07C407/00 ,  C07C407/003 ,  C07C409/08

    摘要： A process for preparing organic hydroperoxides, which process comprises:(a) oxidation of an organic compound to obtain reaction product containing organic hydroperoxide,(b) contacting at least part of the organic hydroperoxide containing reaction product with a basic aqueous solution,(c) separating hydrocarbonaceous phase containing organic hydroperoxide from aqueous phase,(d) contacting at least part of the separated hydrocarbonaceous phase containing organic hydroperoxide with an aqueous solution comprising wastewater, and(e) separating the hydrocarbonaceous phase containing organic hydroperoxide from the aqueous phase.The invention further relates to a process for preparing an oxirane compounds with the help of this process, and a to a process for preparing an alkenyl aryl with the help of this process.

    摘要翻译： 一种制备有机氢过氧化物的方法，该方法包括：（a）氧化有机化合物以获得含有机氢过氧化物的反应产物，（b）使至少部分含有机氢过氧化物的反应产物与碱性水溶液接触，（c） （d）使至少部分含有机氢过氧化物的分离的烃相与包含废水的水溶液接触，和（e）将含有有机氢过氧化物的烃相从水相中分离出来。发明内容本发明涉及一种含有有机氢过氧化物的含烃相， 进一步涉及借助于该方法制备环氧乙烷化合物的方法，以及借助于该方法制备烯基芳基的方法。

    VERFAHREN ZUR HERSTELLUNG EINES EPOXIDS
    77.
    发明授权
    VERFAHREN ZUR HERSTELLUNG EINES EPOXIDS 有权
    用于生产环氧

    公开(公告)号：EP1377562B1

    公开(公告)日：2005-11-09

    申请号：EP02716731.1

    申请日：2002-02-06

    申请人： BASF Aktiengesellschaft

    发明人： TELES, Joaquim, Henrique ,  REHFINGER, Alwin ,  BERG, Anne ,  RUDOLF, Peter ,  RIEBER, Norbert ,  BASSLER, Peter

    IPC分类号： C07D301/12 ,  C07D303/04

    CPC分类号： C07D301/19 ,  C07D301/12 ,  C07D301/32

    摘要： The invention relates to a method for the epoxidation of an organic compound comprising at least one C-C double bond, using hydrogen peroxide in the presence of at least one catalytically active compound and at least one solvent. Said method is characterised in that a product mixture containing α-hydroperoxy alcohols is reduced using at least one reductant. The invention also relates to a method for the epoxidation of an organic compound comprising at least one C-C double bond, using hydrogen peroxide in the presence of at least one catalytically active compound and at least one solvent, characterised in that said method comprises at least the following steps: (i) an organic compound comprising at least one C-C double bond is reacted with hydrogen peroxide in the presence of at least one catalytically active compound and at least one solvent to obtain a product mixture P1 containing α-hydroperoxy alcohols; (ii) an epoxide that has been obtained by the reaction in step (i) is separated from P1 or P1', together with the non-converted organic compound comprising at least one C-C double bond, to obtain a product mixture P2 or P2', P2 containing the α-hydroperoxy alcohols that have occurred as by-products in the reaction in step (i) and P2' being substantially devoid of α-hydroperoxy alcohols. (iii) at least one reductant is added to P1 and/or P2, whereby the α-hydroperoxy alcohols are converted into corresponding glycols, obtained in a product mixture P1' or P3.

    PROCESS FOR PRODUCING PROPYLENE OXIDE
    80.
    发明公开
    PROCESS FOR PRODUCING PROPYLENE OXIDE 有权
    用于生产丙烯

    公开(公告)号：EP1266895A4

    公开(公告)日：2004-09-01

    申请号：EP01912509

    申请日：2001-03-19

    申请人： SUMITOMO CHEMICAL CO

    发明人： OKU NORIAKI ,  OMAE TOSHIKAZU

    IPC分类号： C07D301/19 ,  C07D303/04

    CPC分类号： C07D301/19

    摘要： A process for producing propylene oxide, which comprises steps described below, wherein isopropylbenzene hydroperoxide supplied to an epoxidation step has not undergone a heat history including heating at a temperature not lower than the temperature (t DEG C) represented by the following equation(1), t ( DEG C) = 150 -0.8 x W W: content (% by weight) of isopropylbenzene hydroperoxide in a solution containing isopropylbenzene hydroperoxide: oxidation step; a step in which isopropylbenzene is oxidized to obtain isopropylbenzene hydroperoxide, epoxidation step; a step in which isopropylbenzene hydroperoxide obtained in the oxidation step is reacted with propylene to obtain propylene oxide and cumyl alcohol, and hydrogenolysis step; a step in which cumyl alcohol obtained in the epoxidation step is subjected to hydrogenolysis to obtain isopropylbenzene, and said isopropylbenzene is recycled to the oxidation step as a raw material for the oxidation step.