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    PROCESS FOR PRODUCING POLYVALENT GLYCIDYL COMPOUND
    2.
    发明公开
    PROCESS FOR PRODUCING POLYVALENT GLYCIDYL COMPOUND 审中-公开

    公开(公告)号：EP3219708A4

    公开(公告)日：2018-05-23

    申请号：EP15859225

    申请日：2015-10-28

    申请人： SHOWA DENKO KK

    发明人： YAMASHITA CHIKA ,  ISHIBASHI YOSHITAKA

    IPC分类号： C07D301/12 ,  C07D301/03 ,  C07D303/12 ,  C07D303/28

    CPC分类号： C07D301/12 ,  C07D301/03 ,  C07D303/12 ,  C07D303/28

    摘要： Provided is a process for safely producing, in a high yield, a high-purity polyvalent glycidyl compound from a compound having one or more 2-alkenyl ether groups and two or more 2-alkenyl groups in the molecule, by using a hydrogen peroxide aqueous solution as an oxidizing agent to oxidize the 2-alkenyl ether groups and the 2-alkenyl groups. A 2-alkenyl ether compound having, in the molecule, two or more (un)substituted 2-alkenyl groups and one or more (un)substituted 2-alkenyl ether groups is oxidized using a hydrogen peroxide aqueous solution as an oxidizing agent in the presence of a tungsten compound and a quaternary ammonium salt as catalysts and of phosphoric acid as a co-catalyst, while controlling the pH of the reaction solution to 1.0-4.0 using an acid other than phosphoric acid. During the oxidation, the step of adding the hydrogen peroxide aqueous solution to the reaction solution and the step of adding the acid other than phosphoric acid thereto are alternately repeated at intervals two or more times.

    INTEGRATED PROCESS FOR MAKING PROPENE OXIDE FROM PROPANE
    6.
    发明公开
    INTEGRATED PROCESS FOR MAKING PROPENE OXIDE FROM PROPANE 审中-公开
    由丙烷制备丙烯氧化物的综合方法

    公开(公告)号：EP3246323A1

    公开(公告)日：2017-11-22

    申请号：EP16169840.2

    申请日：2016-05-17

    申请人： Evonik Degussa GmbH ,  ThyssenKrupp Industrial Solutions AG

    发明人： WIEDERHOLD, Holger ,  BOLZ, David ,  THIELE, Georg Friedrich

    IPC分类号： C07D301/12

    CPC分类号： C07D301/12 ,  Y02P20/125

    摘要： The integrated process comprises a step a) of dehydrogenating propane providing a stream S1 comprising propane and propene; a step b) of separating stream S1 in at least one rectification column, providing an overhead product stream S2 comprising more than 99 % by weight propene, a side stream S3 comprising from 90 to 98 % by weight propene and a bottoms product stream S4 enriched in propane; a step c) of reacting propene with hydrogen peroxide in the presence of an epoxidation catalyst using propene in molar excess; and a step d) of separating non-reacted propene and propene oxide from the reaction mixture of step c) providing a propene oxide product and a stream S5 comprising propene and propane; wherein stream S3 is passed to step c), stream S5 is recycled to step b) and stream S4 is recycled to step a).

    摘要翻译： 该整合方法包括丙烷脱氢步骤a），提供包含丙烷和丙烯的物流S1; 在至少一个精馏塔中分离物流S1的步骤b），提供包含大于99重量％丙烯的塔顶产物物流S2，包含90-98重量％丙烯的侧物流S3和富集的底部产物物流S4 在丙烷中; 在环氧化催化剂存在下使用摩尔过量的丙烯使丙烯与过氧化氢反应的步骤c）; 和从步骤c）的反应混合物中分离未反应的丙烯和氧化丙烯以提供氧化丙烯产物和包含丙烯和丙烷的料流S5的步骤d） 其中流S3进入步骤c），流S5再循环至步骤b），并且流S4循环至步骤a）。

    PART-STREAM DISTILLATION
    8.
    发明公开
    PART-STREAM DISTILLATION 审中-公开
    部分蒸馏

    公开(公告)号：EP3212627A1

    公开(公告)日：2017-09-06

    申请号：EP15786922.3

    申请日：2015-10-27

    申请人： BASF SE ,  Dow Global Technologies LLC

    发明人： RIEDEL, Dominic ,  TELES, Joaquim, Henrique ,  SEELIG, Bianca ,  KAMPE, Philip ,  WEBER, Markus ,  SCHRÖDER, Alexander ,  URBANCZYK, Daniel ,  WEIDENBACH, Meinolf ,  MÜLLER, Ulrich ,  WITZL, Werner ,  PARVULESCU, Andrei-Nicolae ,  BÄR, Holger

    IPC分类号： C07D301/12

    CPC分类号： C07D301/12

    摘要： A continuous process for the preparation of propylene oxide, comprising (a) reacting propene with hydrogen peroxide in a reaction apparatus in the presence of acetonitrile as solvent, obtaining a stream SO containing propylene oxide, acetonitrile, water, at least one further component B wherein the normal boiling point of the at least one component B is higher than the normal boiling point of acetonitrile; (b) separating propylene oxide from SO, obtaining a stream SI containing acetonitrile, water and the at least one further component B; (c) dividing S1 into two streams S2 and S3; (d) subjecting S3 to a vapor-liquid fractionation in a first fractionation unit, obtaining a vapor fraction stream S4 a being depleted, relative to S3, of at least one of the at least one component B and obtaining a liquid bottoms stream S4b, and subjecting at least part of the vapor fraction stream S4 a to a vapor-liquid fractionation in a second fractionation unit, obtaining a vapor fraction stream S4c and a liquid bottoms stream S4 being depleted, relative to S4a, of at least one of the at least one component B; (e) recycling at least a portion of S4, optionally after work-up, to (a).

    摘要翻译： 一种制备环氧丙烷的连续方法，包括（a）在乙腈作为溶剂存在下，在反应装置中使丙烯与过氧化氢反应，获得含有环氧丙烷，乙腈，水，至少一种另外的组分B的物流SO，其中 至少一种组分B的标准沸点高于乙腈的标准沸点; （b）从SO中分离氧化丙烯，获得含有乙腈，水和至少一种其他组分B的料流S1; （c）将S1分成两个流S2和S3; （d）使S3在第一分馏单元中进行气液分馏，获得至少一种组分B中的至少一种的相对于S3被耗尽的蒸气分馏流S4a，并获得液体底部料流S4b， 并且使至少部分蒸气馏分流S4a在第二分馏单元中经受蒸气 - 液体分馏，获得相对于S4a而言至少一个蒸气馏分流S4c和液体底部物流S4被耗尽 至少一个组件B; （e）可选地在后处理之后，将至少一部分S4再循环至（a）。

    OLEFIN OXIDATION METHOD, AND REACTION APPARATUS AND SYSTEM
    9.
    发明公开
    OLEFIN OXIDATION METHOD, AND REACTION APPARATUS AND SYSTEM 审中-公开
    烯烃氧化方法，以及反应设备和系统

    公开(公告)号：EP3202764A1

    公开(公告)日：2017-08-09

    申请号：EP15845790.3

    申请日：2015-09-29

    申请人： China Petroleum & Chemical Corporation ,  Research Institute Of Petroleum Processing, Sinopec

    发明人： SHI, Chunfeng ,  LONG, Jun ,  ZHU, Bin ,  LIN, Min

    IPC分类号： C07D303/04 ,  C07D301/12 ,  C07D301/19

    CPC分类号： C07D301/12 ,  C07D301/19 ,  C07D303/04

    摘要： This invention discloses an olefin oxidation process, including a step of under olefin oxidation conditions, successively passing a reaction feed from the No.1 catalyst bed through the No.n catalyst bed, wherein if the apparent velocity of each of the reaction materials passing from the No.1 catalyst bed through the No.n catalyst bed is respectively named as v 1 to v n , and if m represents any integer in the region [2, n], the relationship v m-1 m holds. The process according to this invention is capable of extending the service life of the catalyst, especially the single-pass service life thereof, and at the same time, suppressing any side-reaction over a prolonged period of time. This invention further discloses a fixed-bed reaction apparatus and a system for olefin oxidation.

    摘要翻译： 本发明公开了一种烯烃氧化方法，包括在烯烃氧化条件下的步骤，将来自第一催化剂床的反应进料依次通过第n催化剂床，其中如果每种反应物料的表观速度从 通过第n个催化剂床的第1催化剂床分别命名为v1至vn，并且如果m表示区域[2，n]中的任何整数，则关系vm-1

    PROCESS FOR EPOXIDATION AND CATALYST TO BE USED THEREIN
    10.
    发明公开
    PROCESS FOR EPOXIDATION AND CATALYST TO BE USED THEREIN 审中-公开
    在其中使用的环氧化和催化剂的方法

    公开(公告)号：EP3202494A1

    公开(公告)日：2017-08-09

    申请号：EP17155785.3

    申请日：2003-09-16

    申请人： BASF SE

    发明人： MUELLER, Ulrich ,  KRUG, Georg ,  BAßler, Peter ,  GÖBBEL, Hans-Georg ,  RUDOLF, Peter ,  TELES, Joaquim Henrique

    IPC分类号： B01J29/89 ,  B01J37/10 ,  C07D301/12

    CPC分类号： C07D301/19 ,  B01J29/89 ,  B01J37/10 ,  B01J2229/36 ,  B01J2229/40 ,  C07D301/12 ,  Y02P20/125

    摘要： The present invention relates to a process for treating a solid material containing at least one zeolite and being at least partly crystalline or treating a shaped body obtained from said solid material wherein said solid material or shaped body is brought in contact with a composition containing water after at least one of the following steps of an integrated process for producing a solid material or a shaped body containing at least one zeolite: (i) after step (II) of separating the at least partly crystalline solid material from its mother liquor or (ii) after step (S) of shaping said solid material into a shaped body or (iii) after a step (C) of calcining said solid material or said shaped body. The present invention furthermore relates to the solid material obtainable by the inventive process and the shaped body obtainable by the inventive process. The present invention also relates to the use of the solid material or the shaped body as mentioned above as a catalyst in chemical reactions, in particular in reactions of compounds containing at least one C-C double bond with at least one hydroperoxide

    摘要翻译： 本发明涉及一种处理含有至少一种沸石并至少部分结晶的固体材料或处理由所述固体材料获得的成形体的方法，其中所述固体材料或成形体与含水的组合物接触后 （i）在将至少部分结晶的固体材料从其母液中分离出来或（ii）将至少部分结晶的固体材料从其母液中分离出来的步骤（II）之后， ）在将所述固体材料成形为成形体的步骤（S）之后或（iii）在煅烧所述固体材料或所述成形体的步骤（C）之后）。 本发明还涉及通过本发明方法可获得的固体材料和可通过本发明方法获得的成型体。 本发明还涉及如上所述的固体材料或成型体作为化学反应中的催化剂的用途，特别是在含有至少一个C-C双键的化合物与至少一种氢过氧化物