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    SYNTHESIS OF HIGH ACTIVITY LARGE CRYSTAL ZSM-5
    3.
    发明公开
    SYNTHESIS OF HIGH ACTIVITY LARGE CRYSTAL ZSM-5 有权
    合成高活性GROSSKRISTALLINEM ZSM-5的

    公开(公告)号：EP2785645A1

    公开(公告)日：2014-10-08

    申请号：EP12795305.7

    申请日：2012-11-27

    申请人： ExxonMobil Research and Engineering Company

    发明人： LAI, Wenyih, Frank ,  HAMILTON, Merci, A.

    IPC分类号： C01B39/38 ,  C07C6/12

    CPC分类号： B01J29/40 ,  B01J35/023 ,  B01J2229/123 ,  B01J2229/32 ,  C01B39/38 ,  C07C6/123 ,  C07C2529/40 ,  Y02P20/52 ,  C07C15/08

    摘要： In a process for preparing a high activity, large crystal ZSM-5 type zeolite in the absence of a template, a reaction mixture can be prepared comprising water, a silica source having a surface area less than 150 m
    2 /g, an alumina source, seeds, a source of an oxide of an alkali metal, M, and a source of gluconic acid or salt thereof, Q, wherein the mixture has a SiO
    2 /A1
    2 O
    3 molar ratio ≤40. The reaction mixture can be heated to a crystallization temperature from about 100°C to 200°C for a time sufficient for crystals of ZSM-5 to form. Crystals of ZSM-5 can then be recovered from the reaction mixture which crystals can have a SiO
    2 /A1
    2 O
    3 molar ratio ≤40 and a majority of which crystals can have at least one crystalline dimension of at least about 2 μm.

    IMPROVED LIQUID PHASE ALKYLATION PROCESS
    5.
    发明公开
    IMPROVED LIQUID PHASE ALKYLATION PROCESS 审中-公开
    改进的液相烷基化工艺

    公开(公告)号：EP2755913A1

    公开(公告)日：2014-07-23

    申请号：EP12751717.5

    申请日：2012-08-24

    申请人： ExxonMobil Chemical Patents Inc.

    发明人： VINCENT, Matthew, J. ,  HELTON, Terry, E. ,  JOHNSON, Ivy, D.

    IPC分类号： C01B39/48

    CPC分类号： C01B39/48 ,  B01J29/70 ,  B01J29/74 ,  B01J29/76 ,  B01J29/78 ,  B01J2229/186 ,  B01J2229/42 ,  C07C2/66 ,  C07C2529/70 ,  Y02P20/52 ,  C07C15/073 ,  C07C15/085

    摘要： The present invention provides an improved method for manufacturing high quality porous crystalline MCM-56 material. It also relates to the MCM-56 material manufactured by the improved method, catalyst compositions comprising same and use thereof in a process for catalytic conversion of hydrocarbon compounds. One such conversion process involves production of monoalkylated aromatic compounds, particularly ethylbenzene and cumene, by the liquid or partial liquid phase alkylation of alkylatable aromatic compound, particularly benzene.

    摘要翻译： 本发明提供了一种生产单烷基化芳族化合物的方法，该方法包括在有效的烷基化条件下在催化剂组合物存在下使可烷基化的芳族化合物与烷基化剂接触的步骤，所述催化剂组合物包含通过种子合成生产的MCM-56晶体 方法和粘合剂，使得催化剂组合物中的晶体/粘合剂重量比从20/80至约80/20。

    METHOD FOR PREDICTING HAZE IN LUBRICANT BASE STOCKS
    8.
    发明公开
    METHOD FOR PREDICTING HAZE IN LUBRICANT BASE STOCKS 审中-公开
    VERFAHREN ZUR VORHERSAGE DERTRÜBUNGVON SCHMIERMITTELBASISSTOFFEN

    公开(公告)号：EP2734830A1

    公开(公告)日：2014-05-28

    申请号：EP12748293.3

    申请日：2012-07-20

    申请人： ExxonMobil Research and Engineering Company

    发明人： KANVINDE, Atul, G. ,  BAKER, jR., Charles, L. ,  RIZZO, John, T. ,  LANE, Janet, L. ,  SAEGER, Roland, B.

    IPC分类号： G01N21/03 ,  G01N21/51 ,  G01N33/28

    CPC分类号： G01N21/0332 ,  G01N21/53 ,  G01N33/2888

    摘要： The invention is a technique for predicting future haze formation in dewaxed, petroleum-derived, lubricant base stocks and, by extension, products made from such base stocks. In general, the technique measures the changes in light scattering caused by the formation and disappearance of wax crystals in a dilute test sample of neat base stock, over the course of a temperature profile. The data obtained is then compared to a previously formulated historical correlation of measurements taken using light scattering data to haze potential. The technique focuses on haze disappearance temperature as a reference point, as opposed to total wax formation. The technique also uses a solvent to accelerate the formation of wax crystals in the test sample. The technique provides a robust early warning system that allows refineries to rapidly and accurately determine the long term haze potential of a base stock production prior to release. The technique can be performed in real time, typically in less than an hour.

    摘要翻译： 本发明是用于预测脱蜡，石油衍生的润滑剂基础油以及由这些基础油制成的产品的未来雾度形成的技术。 通常，该技术测量在温度曲线过程中在纯基础油的稀释试样中蜡晶体的形成和消失引起的光散射变化。 然后将获得的数据与使用光散射数据到雾度电位进行的测量的先前制定的历史相关性进行比较。 该技术的重点是雾霾消失温度作为参考点，而不是总蜡形成。 该技术还使用溶剂来加速测试样品中蜡晶体的形成。 该技术提供了一个强大的预警系统，允许炼油厂在发布前快速，准确地确定基础油生产的长期雾度潜力。 该技术可以实时执行，通常在不到一个小时内完成。

    CYCLOHEXYLBENZENE HYDROPEROXIDE COMPOSITIONS
    10.
    发明公开
    CYCLOHEXYLBENZENE HYDROPEROXIDE COMPOSITIONS 审中-公开
    CYCLOHEXYLBENZOL-HYDROPEROXID-ZUSAMMENSETZUNGEN

    公开(公告)号：EP2616435A1

    公开(公告)日：2013-07-24

    申请号：EP11751724.3

    申请日：2011-08-16

    申请人： Exxonmobil Chemical Patents Inc. A Corporation Of The State Of Delaware

    发明人： KUECHLER, Keith, H. ,  BENITEZ, Francisco, M.

    IPC分类号： C07C409/14 ,  C07C13/28

    CPC分类号： C07C407/00 ,  C07C2/74 ,  C07C37/08 ,  C07C37/86 ,  C07C45/53 ,  C07C45/85 ,  C07C2601/14 ,  C07C409/14 ,  C07C39/04 ,  C07C49/403 ,  C07C13/28

    摘要： In a process for producing phenol and cyclohexanone, a feed comprising cyclohexylbenzene is oxidized to produce an oxidation reaction product comprising cyclohexyl-1-phenyl-1-hydroperoxide. At least a portion of the oxidation reaction product is then cleaved to produce a cleavage reaction product comprising phenol, cyclohexanone, and at least one contaminant. At least a portion of the cleavage reaction product is contacted with an acidic material to convert at least a portion of the at least one contaminant to a converted contaminant and thereby produce a modified reaction product. The oxidation reaction product may have at least 50 wt% of cyclohexylbenzene, no greater than 80 wt% of cyclohexyl-1-phenyl-1-hydroperoxide, and 0.1 wt% to 10 wt% of another hydroperoxide.

    摘要翻译： 在生产苯酚和环己酮的方法中，将包含环己基苯的进料氧化以产生包含环己基-1-苯基-1-氢过氧化物的氧化反应产物。 然后将至少一部分氧化反应产物切割以产生包含苯酚，环己酮和至少一种污染物的裂解反应产物。 裂解反应产物的至少一部分与酸性物质接触以将至少一部分至少一种污染物转化为转化的污染物，从而产生改性的反应产物。 氧化反应产物可以具有至少50重量％的环己基苯，不大于80重量％的环己基-1-苯基-1-氢过氧化物和0.1重量％至10重量％的其它氢过氧化物。